JP2016520411A - 非中空の多孔性粒子を製造するための噴霧熱分解中でのスラリーの使用方法 - Google Patents

非中空の多孔性粒子を製造するための噴霧熱分解中でのスラリーの使用方法 Download PDF

Info

Publication number
JP2016520411A
JP2016520411A JP2016502203A JP2016502203A JP2016520411A JP 2016520411 A JP2016520411 A JP 2016520411A JP 2016502203 A JP2016502203 A JP 2016502203A JP 2016502203 A JP2016502203 A JP 2016502203A JP 2016520411 A JP2016520411 A JP 2016520411A
Authority
JP
Japan
Prior art keywords
particles
metal oxide
solid phase
range
average
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2016502203A
Other languages
English (en)
Japanese (ja)
Other versions
JP2016520411A5 (enExample
Inventor
エルハシド ドロル
エルハシド ドロル
アクセルボーム リチャード
アクセルボーム リチャード
レンゲル ミクロス
レンゲル ミクロス
モーラー ウィリアム
モーラー ウィリアム
アトラス ガル
アトラス ガル
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Washington University in St Louis WUSTL
X Tend Energy LLC
Original Assignee
Washington University in St Louis WUSTL
X Tend Energy LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Washington University in St Louis WUSTL, X Tend Energy LLC filed Critical Washington University in St Louis WUSTL
Publication of JP2016520411A publication Critical patent/JP2016520411A/ja
Publication of JP2016520411A5 publication Critical patent/JP2016520411A5/ja
Pending legal-status Critical Current

Links

Images

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/02Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00Lithium compounds
    • C01D15/02Oxides; Hydroxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G1/00Methods of preparing compounds of metals not covered by subclasses C01B, C01C, C01D, or C01F, in general
    • C01G1/02Oxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/40Complex oxides containing nickel and at least one other metal element
    • C01G53/42Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • C01G53/44Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
    • C01G53/50Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (MnO2)n-, e.g. Li(NixMn1-x)O2 or Li(MyNixMn1-x-y)O2
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • H01M10/0525Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00Compounds of manganese
    • C01G45/12Complex oxides containing manganese and at least one other metal element
    • C01G45/1221Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof
    • C01G45/1228Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof of the type (MnO2)-, e.g. LiMnO2 or Li(MxMn1-x)O2
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00Compounds of manganese
    • C01G45/12Complex oxides containing manganese and at least one other metal element
    • C01G45/1221Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof
    • C01G45/125Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof of the type (MnO3)n-, e.g. CaMnO3
    • C01G45/1257Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof of the type (MnO3)n-, e.g. CaMnO3 containing lithium, e.g. Li2MnO3 or Li2(MxMn1-x)O3
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00Compounds of cobalt
    • C01G51/40Complex oxides containing cobalt and at least one other metal element
    • C01G51/42Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00Compounds of cobalt
    • C01G51/40Complex oxides containing cobalt and at least one other metal element
    • C01G51/42Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2
    • C01G51/44Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2 containing manganese
    • C01G51/50Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2 containing manganese of the type (MnO2)n-, e.g. Li(CoxMn1-x)O2 or Li(MyCoxMn1-x-y)O2
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00Compounds of cobalt
    • C01G51/40Complex oxides containing cobalt and at least one other metal element
    • C01G51/42Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2
    • C01G51/44Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2 containing manganese
    • C01G51/56Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2 containing manganese of the type (MnO3)2-, e.g. Li2(CoxMn1-x)O3 or Li2(MyCoxMn1-x-y)O3
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/40Complex oxides containing nickel and at least one other metal element
    • C01G53/42Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/40Complex oxides containing nickel and at least one other metal element
    • C01G53/42Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • C01G53/44Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
    • C01G53/56Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (MnO3)2-, e.g. Li2(NixMn1-x)O3 or Li2(MyNixMn1-x-y)O3
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/30Three-dimensional structures
    • C01P2002/32Three-dimensional structures spinel-type (AB2O4)
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/50Solid solutions
    • C01P2002/52Solid solutions containing elements as dopants
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/03Particle morphology depicted by an image obtained by SEM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/30Particle morphology extending in three dimensions
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/30Particle morphology extending in three dimensions
    • C01P2004/45Aggregated particles or particles with an intergrown morphology
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/80Particles consisting of a mixture of two or more inorganic phases
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/80Particles consisting of a mixture of two or more inorganic phases
    • C01P2004/82Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/11Powder tap density
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/16Pore diameter
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Glanulating (AREA)
  • Mechanical Engineering (AREA)
JP2016502203A 2013-03-13 2014-03-13 非中空の多孔性粒子を製造するための噴霧熱分解中でのスラリーの使用方法 Pending JP2016520411A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201361780059P 2013-03-13 2013-03-13
US61/780,059 2013-03-13
PCT/US2014/026641 WO2014160445A1 (en) 2013-03-13 2014-03-13 Method for the use of slurries in spray pyrolysis for the production of non-hollow, porous particles

Publications (2)

Publication Number Publication Date
JP2016520411A true JP2016520411A (ja) 2016-07-14
JP2016520411A5 JP2016520411A5 (enExample) 2017-04-13

Family

ID=51625427

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2016502203A Pending JP2016520411A (ja) 2013-03-13 2014-03-13 非中空の多孔性粒子を製造するための噴霧熱分解中でのスラリーの使用方法

Country Status (5)

Country Link
US (2) US9748567B2 (enExample)
EP (1) EP2969170A4 (enExample)
JP (1) JP2016520411A (enExample)
KR (1) KR20150132375A (enExample)
WO (1) WO2014160445A1 (enExample)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016018645A (ja) * 2014-07-07 2016-02-01 大陽日酸株式会社 リチウムイオン二次電池用正極材及びその製造方法
KR101993149B1 (ko) * 2018-10-31 2019-09-30 주황윤 제강분진으로부터 황산아연분말을 제조하는 방법

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2017027439A1 (en) * 2015-08-07 2017-02-16 Yangchuan Xing Synthesis of deep eutectic solvent chemical precursors and their use in the production of metal oxides
FR3043572B1 (fr) 2015-11-12 2020-05-15 Pylote Materiaux thermiquement isolants integrant des particules inorganiques spheriques et creuses
JP6871235B2 (ja) * 2016-04-01 2021-05-12 デンカ株式会社 チタン酸バリウム質粉末及びその製造方法、用途
KR102242799B1 (ko) 2017-01-09 2021-04-21 에보니크 오퍼레이션즈 게엠베하 분무 열분해에 의해 금속 산화물을 제조하는 방법
KR20190112809A (ko) * 2017-02-09 2019-10-07 와커 헤미 아게 리튬 이온 배터리의 애노드 재료를 위한 규소 입자
EP3424883A1 (de) 2017-07-05 2019-01-09 Evonik Degussa GmbH Sprühverdampfung eines flüssigen rohstoffes zur herstellung von siliciumdioxid und metalloxiden
EP3495321A1 (de) 2017-12-07 2019-06-12 Evonik Degussa GmbH Herstellung von pulverförmigen, porösen kristallinen metallsilikaten mittels flammensprühpyrolyse
CN110918047B (zh) * 2018-09-20 2021-04-20 比亚迪股份有限公司 一种锂铝复合材料及其制备方法和从含锂卤水中富集锂离子的方法
CN113165905B (zh) * 2018-12-19 2023-12-29 托普索公司 锂正极活性材料
US20210399298A1 (en) * 2018-12-19 2021-12-23 Haldor Topsøe A/S Lithium positive electrode active material
GB201901061D0 (en) * 2019-01-25 2019-03-13 Ceramic Powder Tech As Process
CN110935394B (zh) * 2019-11-05 2021-07-30 南京清大迈特新材料有限公司 一种微纳粉体精细加工方法及装置
CN112520792A (zh) * 2021-01-30 2021-03-19 浙江博瓦德新材料科技有限公司 一种镍沉淀物回用制备氧化亚镍的方法
CN116351419B (zh) * 2023-03-02 2024-12-24 中科合成油技术股份有限公司 一种重质含碳原料浆态床加氢铁基催化剂及其制备方法
WO2025096857A1 (en) * 2023-11-03 2025-05-08 Stratus Materials Inc. Systems and methods for preparing electrode materials via aerosol decomposition
CN117987921A (zh) * 2023-12-29 2024-05-07 华友新能源科技(衢州)有限公司 金属氧化物前驱体及其制备方法和应用
CN119215904A (zh) * 2024-09-05 2024-12-31 宁波中科远东催化工程技术有限公司 火焰喷雾热解制备绿色甲醇合成用催化剂的方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04298234A (ja) * 1990-12-11 1992-10-22 W R Grace & Co 多孔質チタニア球
JP2000340226A (ja) * 1999-05-26 2000-12-08 Kawasaki Steel Corp リチウムマンガン複合酸化物粒子およびその製造方法
US20120282522A1 (en) * 2011-05-02 2012-11-08 Washington University Spray Pyrolysis Synthesis of Mesoporous Positive Electrode Materials for High Energy Lithium-Ion Batteries

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5958361A (en) * 1993-03-19 1999-09-28 Regents Of The University Of Michigan Ultrafine metal oxide powders by flame spray pyrolysis
US6338809B1 (en) 1997-02-24 2002-01-15 Superior Micropowders Llc Aerosol method and apparatus, particulate products, and electronic devices made therefrom
US6268014B1 (en) 1997-10-02 2001-07-31 Chris Eberspacher Method for forming solar cell materials from particulars
US7704483B2 (en) 2005-04-29 2010-04-27 Cabot Corporation High surface area tetragonal zirconia and processes for synthesizing same
US20120128577A1 (en) 2010-10-06 2012-05-24 Blue Juice, Inc. Metal oxide synthesis
WO2012155196A1 (en) * 2011-05-13 2012-11-22 University Of Wollongong Spray pyrolysis method for in situ production of graphene oxide based composites

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04298234A (ja) * 1990-12-11 1992-10-22 W R Grace & Co 多孔質チタニア球
JP2000340226A (ja) * 1999-05-26 2000-12-08 Kawasaki Steel Corp リチウムマンガン複合酸化物粒子およびその製造方法
US20120282522A1 (en) * 2011-05-02 2012-11-08 Washington University Spray Pyrolysis Synthesis of Mesoporous Positive Electrode Materials for High Energy Lithium-Ion Batteries

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016018645A (ja) * 2014-07-07 2016-02-01 大陽日酸株式会社 リチウムイオン二次電池用正極材及びその製造方法
KR101993149B1 (ko) * 2018-10-31 2019-09-30 주황윤 제강분진으로부터 황산아연분말을 제조하는 방법

Also Published As

Publication number Publication date
EP2969170A4 (en) 2016-09-07
US9748567B2 (en) 2017-08-29
EP2969170A1 (en) 2016-01-20
KR20150132375A (ko) 2015-11-25
US20160049652A1 (en) 2016-02-18
WO2014160445A1 (en) 2014-10-02
US20170324088A1 (en) 2017-11-09
US10490814B2 (en) 2019-11-26

Similar Documents

Publication Publication Date Title
US10490814B2 (en) Method for the use of slurries in spray pyrolysis for the production of non-hollow, porous particles
JP7539358B2 (ja) 改善されたリチウム金属酸化物カソード材料及びそれらの作製方法
JP4894969B1 (ja) ニッケルマンガン複合水酸化物粒子とその製造方法、非水系電解質二次電池用正極活物質とその製造方法、ならびに、非水系電解質二次電池
JP4915488B1 (ja) ニッケルマンガン複合水酸化物粒子とその製造方法、非水系電解質二次電池用正極活物質とその製造方法、および非水系電解質二次電池
JP6519202B2 (ja) チタン酸リチウム粉末、及び活物質材料、並びにそれを用いた蓄電デバイス
JP6287771B2 (ja) 非水系電解質二次電池用正極活物質、その製造方法及びそれを用いた非水系電解質二次電池
JP2005347134A (ja) リチウムイオン二次電池用正極活物質の製造方法
JPWO2018003929A1 (ja) 蓄電デバイスの電極用チタン酸リチウム粉末および活物質材料、並びにそれを用いた電極シートおよび蓄電デバイス
US20220352500A1 (en) Electrode Mixture and Electrode Layer and Solid-State Battery Employing Same
JP5364523B2 (ja) オリビン型ケイ酸mリチウムの合成方法およびリチウムイオン二次電池
JP7135354B2 (ja) 非水系電解質二次電池用正極活物質前駆体、非水系電解質二次電池用正極活物質前駆体の製造方法、非水系電解質二次電池用正極活物質の製造方法
JP2025074304A (ja) 非水電解質二次電池用正極活物質及びその製造方法
JP5634828B2 (ja) スピネル型リチウム・マンガン系複合酸化物粒子の製造方法ならびに用途
KR101510528B1 (ko) 분무건조 공정에 의한 응집체 구조의 리튬 이차 전지용 전극활물질 분말의 제조방법 및 이로부터 제조된 전극활물질 분말
JP7068637B1 (ja) リチウムイオン二次電池用正極活物質、及びこれを用いたリチウムイオン二次電池
JP7338133B2 (ja) 非水系電解質二次電池用正極活物質前駆体、非水系電解質二次電池用正極活物質前駆体の製造方法、非水系電解質二次電池用正極活物質の製造方法
TW201803803A (zh) 磷酸釩鋰的製造方法
JP2020057474A (ja) リチウムイオン二次電池用正極活物質およびその製造方法、リチウムイオン二次電池正極用スラリー組成物、リチウムイオン二次電池用正極、並びに、リチウムイオン二次電池
JP2005257171A (ja) 焼成容器、及びリチウム二次電池電極材料用リチウム遷移金属複合酸化物の製造方法
JP2020161455A (ja) リチウムイオン二次電池用正極材料、リチウムイオン二次電池用正極、リチウムイオン二次電池
JP2019021422A (ja) 非水系電解質二次電池用正極活物質前駆体、非水系電解質二次電池用正極活物質、非水系電解質二次電池用正極活物質前駆体の製造方法、非水系電解質二次電池用正極活物質の製造方法
JP2002003220A (ja) リチウムイオン二次電池用正極材料、これを用いた正極及び電池
CN115347161B (zh) 正极材料及其制备方法和锂离子电池
RU2818523C2 (ru) Смешанный оксид лития и переходного металла, покрытый полученными пирогенным способом оксидами, содержащими цирконий
JP2002053321A (ja) リチウムマンガン複合酸化物及びその製造方法、並びにその用途

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20151013

A529 Written submission of copy of amendment under article 34 pct

Free format text: JAPANESE INTERMEDIATE CODE: A529

Effective date: 20151013

A711 Notification of change in applicant

Free format text: JAPANESE INTERMEDIATE CODE: A711

Effective date: 20170214

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A821

Effective date: 20170214

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20170309

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20170309

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20180227

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20180305

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20181015