JP2016510328A - フローシステムを用いた5−ニトロテトラゾレートを調製するための簡易な方法 - Google Patents
フローシステムを用いた5−ニトロテトラゾレートを調製するための簡易な方法 Download PDFInfo
- Publication number
- JP2016510328A JP2016510328A JP2015553911A JP2015553911A JP2016510328A JP 2016510328 A JP2016510328 A JP 2016510328A JP 2015553911 A JP2015553911 A JP 2015553911A JP 2015553911 A JP2015553911 A JP 2015553911A JP 2016510328 A JP2016510328 A JP 2016510328A
- Authority
- JP
- Japan
- Prior art keywords
- acid
- zone
- reaction
- flow system
- continuous flow
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D257/00—Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms
- C07D257/02—Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms not condensed with other rings
- C07D257/04—Five-membered rings
- C07D257/06—Five-membered rings with nitrogen atoms directly attached to the ring carbon atom
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201361755167P | 2013-01-22 | 2013-01-22 | |
US61/755,167 | 2013-01-22 | ||
PCT/US2014/012472 WO2014116654A1 (en) | 2013-01-22 | 2014-01-22 | Facile method for preparation of 5-nitrotetrazolates using a flow system |
Publications (1)
Publication Number | Publication Date |
---|---|
JP2016510328A true JP2016510328A (ja) | 2016-04-07 |
Family
ID=51208193
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2015553911A Pending JP2016510328A (ja) | 2013-01-22 | 2014-01-22 | フローシステムを用いた5−ニトロテトラゾレートを調製するための簡易な方法 |
Country Status (9)
Country | Link |
---|---|
US (1) | US9670168B2 (es) |
EP (1) | EP2948435B1 (es) |
JP (1) | JP2016510328A (es) |
AU (1) | AU2014209562A1 (es) |
CA (1) | CA2897068C (es) |
ES (1) | ES2649740T3 (es) |
MX (1) | MX359795B (es) |
WO (1) | WO2014116654A1 (es) |
ZA (1) | ZA201504901B (es) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
MX359795B (es) | 2013-01-22 | 2018-10-10 | Pacific Scient Energetic Materials Co | Método fácil para la preparación de 5-nitrotetrazolatos usando un sistema de flujo. |
US9598380B2 (en) | 2014-06-12 | 2017-03-21 | Sri International | Facile method for preparation of 5-nitrotetrazolates using a batch system |
US9718791B2 (en) | 2015-01-16 | 2017-08-01 | Pacific Scientific Energetic Materials Company | Facile method for preparation of sodium 5-nitrotetrazolate using a flow system |
WO2018093447A2 (en) | 2016-09-07 | 2018-05-24 | Pacific Scientific Energetic Materials Company | Purification of flow sodium 5- nitrotetrazolate solutions with copper modified cation exchange resin |
US10947204B1 (en) * | 2019-10-17 | 2021-03-16 | U.S. Government As Represented By The Secretary Of The Army | Method for preparing sodium nitrotetrazolate using cation exchange resin |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2066954A (en) | 1931-07-10 | 1937-01-05 | Herz Edmund Von | C-nitrotetrazole compounds |
US3054800A (en) | 1949-09-17 | 1962-09-18 | Harry P Burchfield | 3, 5-dinitro-1, 2, 4-triazoles and process for preparing same |
US3111524A (en) | 1957-05-06 | 1963-11-19 | Richard H Wiley | Preparation of 3, 5-dinitro-1, 2, 4-triazole |
GB1519796A (en) | 1975-11-11 | 1978-08-02 | Secr Defence | Production of 5-nitotetrazole salts |
US4093623A (en) | 1977-05-05 | 1978-06-06 | The United States Of America As Represented By The Secretary Of The Navy | Method of preparing the acid copper salt of 5-nitrotetrazole |
US4552598A (en) | 1984-05-17 | 1985-11-12 | The United States Of America As Represented By The United States Department Of Energy | Ethylenediamine salt of 5-nitrotetrazole and preparation |
US6375871B1 (en) | 1998-06-18 | 2002-04-23 | 3M Innovative Properties Company | Methods of manufacturing microfluidic articles |
US6167910B1 (en) | 1998-01-20 | 2001-01-02 | Caliper Technologies Corp. | Multi-layer microfluidic devices |
US6749814B1 (en) | 1999-03-03 | 2004-06-15 | Symyx Technologies, Inc. | Chemical processing microsystems comprising parallel flow microreactors and methods for using same |
DE19949551C2 (de) | 1999-10-14 | 2001-12-13 | Agilent Technologies Inc | Mikrofluidischer Mikrochip, Energieversorgungseinrichtung und Verfahren zum Betrieb eines mikrofluidischen Mikrochips |
DE50100960D1 (de) | 2000-02-09 | 2003-12-18 | Clariant Internat Ltd Muttenz | Verfahren zur herstellung von azofarbmitteln in mikroreaktoren |
DE10032019A1 (de) | 2000-07-01 | 2002-01-10 | Clariant Gmbh | Verfahren zur Herstellung von Disazokondensationspigmenten in Mikroreaktoren |
GB0126281D0 (en) | 2001-11-01 | 2002-01-02 | Astrazeneca Ab | A chemical reactor |
DE602005024824D1 (de) * | 2004-09-08 | 2010-12-30 | Pacific Scient Energetic Materials Co | Verfahren zur herstellung von substituierten tetrazolen aus aminotetrazolen |
MX359795B (es) | 2013-01-22 | 2018-10-10 | Pacific Scient Energetic Materials Co | Método fácil para la preparación de 5-nitrotetrazolatos usando un sistema de flujo. |
US9598380B2 (en) | 2014-06-12 | 2017-03-21 | Sri International | Facile method for preparation of 5-nitrotetrazolates using a batch system |
-
2014
- 2014-01-22 MX MX2015009173A patent/MX359795B/es active IP Right Grant
- 2014-01-22 JP JP2015553911A patent/JP2016510328A/ja active Pending
- 2014-01-22 CA CA2897068A patent/CA2897068C/en active Active
- 2014-01-22 EP EP14743596.0A patent/EP2948435B1/en not_active Not-in-force
- 2014-01-22 WO PCT/US2014/012472 patent/WO2014116654A1/en active Application Filing
- 2014-01-22 ES ES14743596.0T patent/ES2649740T3/es active Active
- 2014-01-22 US US14/160,998 patent/US9670168B2/en active Active
- 2014-01-22 AU AU2014209562A patent/AU2014209562A1/en not_active Abandoned
-
2015
- 2015-07-08 ZA ZA2015/04901A patent/ZA201504901B/en unknown
Also Published As
Publication number | Publication date |
---|---|
MX359795B (es) | 2018-10-10 |
US20140206885A1 (en) | 2014-07-24 |
AU2014209562A1 (en) | 2015-08-20 |
EP2948435A1 (en) | 2015-12-02 |
CA2897068C (en) | 2019-09-03 |
WO2014116654A1 (en) | 2014-07-31 |
ES2649740T3 (es) | 2018-01-15 |
US9670168B2 (en) | 2017-06-06 |
EP2948435A4 (en) | 2016-06-08 |
MX2015009173A (es) | 2016-02-18 |
CA2897068A1 (en) | 2014-07-31 |
ZA201504901B (en) | 2016-07-27 |
EP2948435B1 (en) | 2017-08-30 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US9598380B2 (en) | Facile method for preparation of 5-nitrotetrazolates using a batch system | |
US9670168B2 (en) | Facile method for preparation of 5-nitrotetrazolates using a flow system | |
ES2836201T3 (es) | Proceso para la preparación de ácidos 4-alcoxi-3-hidroxipicolínicos | |
CN107663160A (zh) | 一种4‑氯苯肼盐的连续流合成工艺 | |
JP2010235370A (ja) | ビス(フルオロスルホニル)イミドの製造方法 | |
CN103370301A (zh) | 制备尼可地尔的方法 | |
JP5525515B2 (ja) | 2−ハロ−4−ニトロイミダゾール及びその中間体の製造方法 | |
US20150239910A1 (en) | Method for preparation of a lead-free primary explosive | |
JP5497052B2 (ja) | モノニトロベンゼンを製造するための断熱的方法 | |
US9718791B2 (en) | Facile method for preparation of sodium 5-nitrotetrazolate using a flow system | |
JP5444453B2 (ja) | ビス(フルオロスルホニル)イミドの製造方法 | |
Mittal et al. | Highly scalable and inherently safer preparation of di, tri and tetra nitrate esters using continuous flow chemistry | |
CN105418432A (zh) | 一种硝酸异辛酯的生产方法 | |
TW201538474A (zh) | 使用流動反應器的酮基丙二酸化合物的連續製造方法 | |
US8415513B2 (en) | Continuous process of preparing bromopicrin | |
CA3204883C (en) | Flow synthesis of rdx | |
JP5560136B2 (ja) | ビス(フルオロスルホニル)イミドの製造方法 | |
CN112358404B (zh) | 一种2-氯-6-甲基苯胺的制备方法 | |
US10947204B1 (en) | Method for preparing sodium nitrotetrazolate using cation exchange resin | |
WO2023180688A1 (en) | A method of producing explosive hmx by flow synthesis | |
WO2020119507A1 (zh) | 一种连续制备5-氰二醇的方法 | |
JPH10298147A (ja) | 芳香族基体の連続的ジニトロ化方法 | |
JP2004217526A (ja) | 2−アミノトロポンの製造方法 | |
CN115536587A (zh) | 一种用微通道硝化制备西地那非中间体的方法 | |
Li et al. | Synthesis and crystal structure of 1-methoxymethyl-3, 4, 5-trinitropyrazole |