JP2016510328A - フローシステムを用いた５−ニトロテトラゾレートを調製するための簡易な方法 - Google Patents

フローシステムを用いた５−ニトロテトラゾレートを調製するための簡易な方法 Download PDF

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Publication number
JP2016510328A
JP2016510328A JP2015553911A JP2015553911A JP2016510328A JP 2016510328 A JP2016510328 A JP 2016510328A JP 2015553911 A JP2015553911 A JP 2015553911A JP 2015553911 A JP2015553911 A JP 2015553911A JP 2016510328 A JP2016510328 A JP 2016510328A
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Prior art keywords
acid
zone
reaction
flow system
continuous flow
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JP2015553911A
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English (en)
Japanese (ja)
Inventor
ジョン ダブリュー． フロナバーガー，
ジョン ダブリュー． フロナバーガー，
マイケル ディー． ウィリアムズ，
マイケル ディー． ウィリアムズ，
ジョン ジー ブラッグ，
ジョン ジー ブラッグ，
Original Assignee
パシフィック・サイエンティフィック・エナジェティック・マテリアルズ・カンパニー
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Publication of JP2016510328A publication Critical patent/JP2016510328A/ja
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D257/00—Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms
    • C07D257/02—Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms not condensed with other rings
    • C07D257/04—Five-membered rings
    • C07D257/06—Five-membered rings with nitrogen atoms directly attached to the ring carbon atom

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
JP2015553911A 2013-01-22 2014-01-22 フローシステムを用いた５−ニトロテトラゾレートを調製するための簡易な方法 Pending JP2016510328A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201361755167P 2013-01-22 2013-01-22
US61/755,167 2013-01-22
PCT/US2014/012472 WO2014116654A1 (en) 2013-01-22 2014-01-22 Facile method for preparation of 5-nitrotetrazolates using a flow system

Publications (1)

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JP2016510328A true JP2016510328A (ja) 2016-04-07

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JP2015553911A Pending JP2016510328A (ja) 2013-01-22 2014-01-22 フローシステムを用いた５−ニトロテトラゾレートを調製するための簡易な方法

Country Status (9)

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US (1) US9670168B2 (es)
EP (1) EP2948435B1 (es)
JP (1) JP2016510328A (es)
AU (1) AU2014209562A1 (es)
CA (1) CA2897068C (es)
ES (1) ES2649740T3 (es)
MX (1) MX359795B (es)
WO (1) WO2014116654A1 (es)
ZA (1) ZA201504901B (es)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MX359795B (es) 2013-01-22 2018-10-10 Pacific Scient Energetic Materials Co Método fácil para la preparación de 5-nitrotetrazolatos usando un sistema de flujo.
US9598380B2 (en) 2014-06-12 2017-03-21 Sri International Facile method for preparation of 5-nitrotetrazolates using a batch system
US9718791B2 (en) 2015-01-16 2017-08-01 Pacific Scientific Energetic Materials Company Facile method for preparation of sodium 5-nitrotetrazolate using a flow system
WO2018093447A2 (en) 2016-09-07 2018-05-24 Pacific Scientific Energetic Materials Company Purification of flow sodium 5- nitrotetrazolate solutions with copper modified cation exchange resin
US10947204B1 (en) * 2019-10-17 2021-03-16 U.S. Government As Represented By The Secretary Of The Army Method for preparing sodium nitrotetrazolate using cation exchange resin

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2066954A (en) 1931-07-10 1937-01-05 Herz Edmund Von C-nitrotetrazole compounds
US3054800A (en) 1949-09-17 1962-09-18 Harry P Burchfield 3, 5-dinitro-1, 2, 4-triazoles and process for preparing same
US3111524A (en) 1957-05-06 1963-11-19 Richard H Wiley Preparation of 3, 5-dinitro-1, 2, 4-triazole
GB1519796A (en) 1975-11-11 1978-08-02 Secr Defence Production of 5-nitotetrazole salts
US4093623A (en) 1977-05-05 1978-06-06 The United States Of America As Represented By The Secretary Of The Navy Method of preparing the acid copper salt of 5-nitrotetrazole
US4552598A (en) 1984-05-17 1985-11-12 The United States Of America As Represented By The United States Department Of Energy Ethylenediamine salt of 5-nitrotetrazole and preparation
US6375871B1 (en) 1998-06-18 2002-04-23 3M Innovative Properties Company Methods of manufacturing microfluidic articles
US6167910B1 (en) 1998-01-20 2001-01-02 Caliper Technologies Corp. Multi-layer microfluidic devices
US6749814B1 (en) 1999-03-03 2004-06-15 Symyx Technologies, Inc. Chemical processing microsystems comprising parallel flow microreactors and methods for using same
DE19949551C2 (de) 1999-10-14 2001-12-13 Agilent Technologies Inc Mikrofluidischer Mikrochip, Energieversorgungseinrichtung und Verfahren zum Betrieb eines mikrofluidischen Mikrochips
DE50100960D1 (de) 2000-02-09 2003-12-18 Clariant Internat Ltd Muttenz Verfahren zur herstellung von azofarbmitteln in mikroreaktoren
DE10032019A1 (de) 2000-07-01 2002-01-10 Clariant Gmbh Verfahren zur Herstellung von Disazokondensationspigmenten in Mikroreaktoren
GB0126281D0 (en) 2001-11-01 2002-01-02 Astrazeneca Ab A chemical reactor
DE602005024824D1 (de) * 2004-09-08 2010-12-30 Pacific Scient Energetic Materials Co Verfahren zur herstellung von substituierten tetrazolen aus aminotetrazolen
MX359795B (es) 2013-01-22 2018-10-10 Pacific Scient Energetic Materials Co Método fácil para la preparación de 5-nitrotetrazolatos usando un sistema de flujo.
US9598380B2 (en) 2014-06-12 2017-03-21 Sri International Facile method for preparation of 5-nitrotetrazolates using a batch system

Also Published As

Publication number Publication date
MX359795B (es) 2018-10-10
US20140206885A1 (en) 2014-07-24
AU2014209562A1 (en) 2015-08-20
EP2948435A1 (en) 2015-12-02
CA2897068C (en) 2019-09-03
WO2014116654A1 (en) 2014-07-31
ES2649740T3 (es) 2018-01-15
US9670168B2 (en) 2017-06-06
EP2948435A4 (en) 2016-06-08
MX2015009173A (es) 2016-02-18
CA2897068A1 (en) 2014-07-31
ZA201504901B (en) 2016-07-27
EP2948435B1 (en) 2017-08-30

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