JP2015517999A - バイオベースアクリル酸の粗及び氷アクリル酸への精製 - Google Patents

バイオベースアクリル酸の粗及び氷アクリル酸への精製 Download PDF

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Publication number
JP2015517999A
JP2015517999A JP2015505902A JP2015505902A JP2015517999A JP 2015517999 A JP2015517999 A JP 2015517999A JP 2015505902 A JP2015505902 A JP 2015505902A JP 2015505902 A JP2015505902 A JP 2015505902A JP 2015517999 A JP2015517999 A JP 2015517999A
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Japan
Prior art keywords
acrylic acid
acid
composition
another embodiment
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2015505902A
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English (en)
Japanese (ja)
Inventor
エレン ゴドルースキー ジェイン
エレン ゴドルースキー ジェイン
ビラロボス リンゴーズ ジャネット
ビラロボス リンゴーズ ジャネット
エステバン ヴェラスケス ジュアン
エステバン ヴェラスケス ジュアン
イオアニス コリアス ディミトリス
イオアニス コリアス ディミトリス
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Procter and Gamble Co
Original Assignee
Procter and Gamble Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US13/760,505 external-priority patent/US20130274518A1/en
Application filed by Procter and Gamble Co filed Critical Procter and Gamble Co
Publication of JP2015517999A publication Critical patent/JP2015517999A/ja
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/16—Phosphorus; Compounds thereof containing oxygen, i.e. acids, anhydrides and their derivates with N, S, B or halogens without carriers or on carriers based on C, Si, Al or Zr; also salts of Si, Al and Zr
    • B01J27/18—Phosphorus; Compounds thereof containing oxygen, i.e. acids, anhydrides and their derivates with N, S, B or halogens without carriers or on carriers based on C, Si, Al or Zr; also salts of Si, Al and Zr with metals other than Al or Zr
    • B01J27/1802—Salts or mixtures of anhydrides with compounds of other metals than V, Nb, Ta, Cr, Mo, W, Mn, Tc, Re, e.g. phosphates, thiophosphates
    • B01J27/1806—Salts or mixtures of anhydrides with compounds of other metals than V, Nb, Ta, Cr, Mo, W, Mn, Tc, Re, e.g. phosphates, thiophosphates with alkaline or alkaline earth metals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
    • C07C51/377—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by splitting-off hydrogen or functional groups; by hydrogenolysis of functional groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C07C51/46—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by azeotropic distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03—Monocarboxylic acids
    • C07C57/04—Acrylic acid; Methacrylic acid

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
JP2015505902A 2012-04-11 2013-04-11 バイオベースアクリル酸の粗及び氷アクリル酸への精製 Pending JP2015517999A (ja)

Applications Claiming Priority (9)

Application Number Priority Date Filing Date Title
US201261623054P 2012-04-11 2012-04-11
US61/623,054 2012-04-11
US13/760,505 US20130274518A1 (en) 2012-04-11 2013-02-06 Purification Of Bio Based Acrylic Acid To Crude And Glacial Acrylic Acid
US13/760,505 2013-02-06
US13/835,187 US9926256B2 (en) 2012-04-11 2013-03-15 Catalytic conversion of lactic acid to acrylic acid
US13/838,823 2013-03-15
US13/835,187 2013-03-15
US13/838,823 US20130274520A1 (en) 2012-04-11 2013-03-15 Purification Of Bio Based Acrylic Acid To Crude And Glacial Acrylic Acid
PCT/US2013/036158 WO2013155292A2 (en) 2012-04-11 2013-04-11 Purification of bio-based acrylic acid to crude and glacial acrylic acid

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2017001292A Division JP2017101046A (ja) 2012-04-11 2017-01-06 バイオベースアクリル酸の粗及び氷アクリル酸への精製

Publications (1)

Publication Number Publication Date
JP2015517999A true JP2015517999A (ja) 2015-06-25

Family

ID=49325676

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2015505902A Pending JP2015517999A (ja) 2012-04-11 2013-04-11 バイオベースアクリル酸の粗及び氷アクリル酸への精製
JP2017001292A Pending JP2017101046A (ja) 2012-04-11 2017-01-06 バイオベースアクリル酸の粗及び氷アクリル酸への精製

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2017001292A Pending JP2017101046A (ja) 2012-04-11 2017-01-06 バイオベースアクリル酸の粗及び氷アクリル酸への精製

Country Status (12)

Country Link
US (2) US20130274520A1 (https=)
EP (1) EP2836475B1 (https=)
JP (2) JP2015517999A (https=)
AU (1) AU2013245853B2 (https=)
BR (1) BR112014025188B1 (https=)
CA (1) CA2870314C (https=)
IN (1) IN2014DN08551A (https=)
MX (1) MX380544B (https=)
MY (1) MY164790A (https=)
RU (1) RU2599640C2 (https=)
SG (2) SG11201406509YA (https=)
WO (1) WO2013155292A2 (https=)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2018528209A (ja) * 2015-08-28 2018-09-27 ザ プロクター アンド ギャンブル カンパニー ヒドロキシプロピオン酸及びその誘導体の触媒的脱水
JP2023546421A (ja) * 2020-10-16 2023-11-02 エルジー・ケム・リミテッド 乳酸気化方法、乳酸気化装置、およびアクリル酸の製造方法

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* Cited by examiner, † Cited by third party
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BR112016008445B1 (pt) * 2013-10-16 2022-03-15 The Procter & Gamble Company Catalisador para produzir ácido acrílico biobaseado e seus derivados e método para fabricar o mesmo
WO2016026761A1 (en) * 2014-08-18 2016-02-25 Basf Se Process for preparing acrylic acid by dehydration of 3-hydroxypropionic acid
EP3012244A1 (en) 2014-10-24 2016-04-27 Sulzer Chemtech AG Process and apparatus for purification of acrylic acid
AU2016316922B2 (en) 2015-08-28 2019-05-02 The Procter & Gamble Company Catalysts for the dehydration of hydroxypropionic acid and its derivatives
DE102016114555A1 (de) 2016-08-05 2018-02-08 Thyssenkrupp Ag Prozess zur Herstellung von Acrylsäure aus einer wässrigen 3-Hydroxypropanol-Lösung
US9890102B1 (en) 2016-11-03 2018-02-13 The Procter & Gamble Company Method of making acrylic acid from hydroxypropionic acid
KR102721330B1 (ko) * 2020-12-03 2024-10-23 주식회사 엘지화학 아크릴산 제조방법
FR3125064B1 (fr) 2021-07-09 2024-07-12 Snf Sa Procédé biologique d’obtention de monomères comprenant une insaturation éthylénique par bioconversion d’un composé biosourcé comprenant au moins une fonction nitrile

Citations (5)

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JPH09227445A (ja) * 1996-01-12 1997-09-02 Basf Ag アクリル酸及びそのエステルを製造する方法及び装置
WO2005095320A1 (en) * 2004-04-02 2005-10-13 Ciba Specialty Chemicals Water Treatments Limited Preparation of acrylic acid derivatives from alpha or beta-hydroxy carboxylic acids
JP2010501526A (ja) * 2006-08-22 2010-01-21 エボニック・シュトックハウゼン・ゲーエムベーハー ヒドロキシプロピオン酸からの晶析により精製されるアクリル酸の調製方法及びそれに使用する装置
WO2011052178A1 (ja) * 2009-10-29 2011-05-05 株式会社サンギ 不飽和カルボン酸および／またはその誘導体の合成方法
JP2011225533A (ja) * 2010-03-31 2011-11-10 Nippon Shokubai Co Ltd アクリル酸およびその重合体の製造方法

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US4973841A (en) 1990-02-02 1990-11-27 Genus, Inc. Precision ultra-sensitive trace detector for carbon-14 when it is at concentration close to that present in recent organic materials
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FR2736912B1 (fr) 1995-07-18 1997-08-22 Atochem Elf Sa Procede de purification de l'acide acrylique obtenu par oxydation catalytique du propylene
US5661299A (en) 1996-06-25 1997-08-26 High Voltage Engineering Europa B.V. Miniature AMS detector for ultrasensitive detection of individual carbon-14 and tritium atoms
DE19829477A1 (de) 1998-07-01 2000-01-05 Basf Ag Verfahren zur Reinigung von Acrylsäure oder Methacrylsäure durch Kristallisation und Destillation
DE19832962A1 (de) * 1998-07-22 2000-01-27 Basf Ag Reinigung von Acrylsäure durch Kristallisation mittels Vakuumverdampfung
JP4960562B2 (ja) * 2000-04-11 2012-06-27 ビーエーエスエフ ソシエタス・ヨーロピア 粗製アクリル酸溶融物の精製法
BR0206396A (pt) * 2001-01-12 2004-02-10 Degussa Processo contìnuo para preparação e purificação de ácido (met)acrìlico
DE10138150A1 (de) 2001-08-03 2003-02-13 Basf Ag Verfahren zur Herstellung wasserabsorbierender Harze
US20030146081A1 (en) * 2002-01-08 2003-08-07 Salvador Aldrett Acrylic acid recovery utilizing ethyl acrylate and selected co-solvents
FR2897058B1 (fr) * 2006-02-07 2008-04-18 Arkema Sa Procede de preparation d'acroleine
EP2114852B1 (de) * 2007-01-26 2015-09-23 Basf Se Verfahren zur herstellung von acrylsäure
JP5489726B2 (ja) * 2007-01-26 2014-05-14 ビーエーエスエフ ソシエタス・ヨーロピア アクリル酸の製造方法
JP4822559B2 (ja) * 2007-09-19 2011-11-24 ローム アンド ハース カンパニー （メタ）アクリル酸生成物流からのプロピオン酸の選択的減少のための改良された方法
WO2009155086A2 (en) 2008-05-30 2009-12-23 E. I. Du Pont De Nemours And Company Renewably resourced chemicals and intermediates
JP2010163383A (ja) * 2009-01-14 2010-07-29 Toagosei Co Ltd アクリル酸の精製方法
JP2010180171A (ja) * 2009-02-06 2010-08-19 Nippon Shokubai Co Ltd アクリル酸の製造方法
MY152961A (en) * 2009-05-15 2014-12-15 Nippon Catalytic Chem Ind Process for producing (meth)acrylic acid
FR2948365B1 (fr) * 2009-07-22 2011-09-09 Arkema France Procede de fabrication d'acide acrylique bio-ressource a partir de glycerol
CN103080328B (zh) * 2010-09-07 2015-06-10 麦兰特公司 乳酸和乳酸酯的催化脱水
US9029596B2 (en) * 2010-12-28 2015-05-12 Nippon Shokubai Co., Ltd. Methods for producing acrylic acid and/or ester thereof and polymer of the acrylic acid and/or ester thereof
US10106484B2 (en) * 2012-04-11 2018-10-23 The Procter & Gamble Company Catalysts for the conversion of hydroxypropionic acid or its derivatives to acrylic acid or its derivatives

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09227445A (ja) * 1996-01-12 1997-09-02 Basf Ag アクリル酸及びそのエステルを製造する方法及び装置
WO2005095320A1 (en) * 2004-04-02 2005-10-13 Ciba Specialty Chemicals Water Treatments Limited Preparation of acrylic acid derivatives from alpha or beta-hydroxy carboxylic acids
JP2010501526A (ja) * 2006-08-22 2010-01-21 エボニック・シュトックハウゼン・ゲーエムベーハー ヒドロキシプロピオン酸からの晶析により精製されるアクリル酸の調製方法及びそれに使用する装置
WO2011052178A1 (ja) * 2009-10-29 2011-05-05 株式会社サンギ 不飽和カルボン酸および／またはその誘導体の合成方法
JP2011225533A (ja) * 2010-03-31 2011-11-10 Nippon Shokubai Co Ltd アクリル酸およびその重合体の製造方法

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2018528209A (ja) * 2015-08-28 2018-09-27 ザ プロクター アンド ギャンブル カンパニー ヒドロキシプロピオン酸及びその誘導体の触媒的脱水
JP2023546421A (ja) * 2020-10-16 2023-11-02 エルジー・ケム・リミテッド 乳酸気化方法、乳酸気化装置、およびアクリル酸の製造方法
JP7618792B2 (ja) 2020-10-16 2025-01-21 エルジー・ケム・リミテッド 乳酸気化方法、乳酸気化装置、およびアクリル酸の製造方法
JP2025039724A (ja) * 2020-10-16 2025-03-21 エルジー・ケム・リミテッド 乳酸気化方法、乳酸気化装置、およびアクリル酸の製造方法

Also Published As

Publication number Publication date
AU2013245853B2 (en) 2016-06-02
SG11201406509YA (en) 2014-11-27
WO2013155292A4 (en) 2014-01-23
US20130274520A1 (en) 2013-10-17
MX380544B (es) 2025-03-12
RU2599640C2 (ru) 2016-10-10
EP2836475A2 (en) 2015-02-18
CA2870314C (en) 2018-01-02
IN2014DN08551A (https=) 2015-05-15
SG10201703949YA (en) 2017-06-29
WO2013155292A2 (en) 2013-10-17
CA2870314A1 (en) 2013-10-17
MY164790A (en) 2018-01-30
RU2014139950A (ru) 2016-04-20
AU2013245853A1 (en) 2014-10-30
EP2836475B1 (en) 2021-05-26
CN104220410A (zh) 2014-12-17
US20150329462A1 (en) 2015-11-19
MX2014012303A (es) 2014-11-10
WO2013155292A3 (en) 2013-12-05
BR112014025188B1 (pt) 2020-02-04
JP2017101046A (ja) 2017-06-08

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