JP2015038017A5 - - Google Patents
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- Publication number
- JP2015038017A5 JP2015038017A5 JP2014145632A JP2014145632A JP2015038017A5 JP 2015038017 A5 JP2015038017 A5 JP 2015038017A5 JP 2014145632 A JP2014145632 A JP 2014145632A JP 2014145632 A JP2014145632 A JP 2014145632A JP 2015038017 A5 JP2015038017 A5 JP 2015038017A5
- Authority
- JP
- Japan
- Prior art keywords
- graphite
- metal salt
- raw material
- producing
- exfoliated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 16
- 229910002804 graphite Inorganic materials 0.000 claims 15
- 239000010439 graphite Substances 0.000 claims 15
- 238000004519 manufacturing process Methods 0.000 claims 6
- -1 alkali metal salt Chemical class 0.000 claims 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- 239000002994 raw material Substances 0.000 claims 3
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims 2
- 206010040844 Skin exfoliation Diseases 0.000 claims 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims 2
- 229910052783 alkali metal Inorganic materials 0.000 claims 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims 2
- 239000003792 electrolyte Substances 0.000 claims 2
- 229910021389 graphene Inorganic materials 0.000 claims 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims 1
- 238000005452 bending Methods 0.000 claims 1
- 239000001110 calcium chloride Substances 0.000 claims 1
- 229910001628 calcium chloride Inorganic materials 0.000 claims 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims 1
- 239000000920 calcium hydroxide Substances 0.000 claims 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims 1
- 238000007598 dipping method Methods 0.000 claims 1
- 238000004299 exfoliation Methods 0.000 claims 1
- 229910001629 magnesium chloride Inorganic materials 0.000 claims 1
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims 1
- 239000000347 magnesium hydroxide Substances 0.000 claims 1
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 239000001103 potassium chloride Substances 0.000 claims 1
- 235000011164 potassium chloride Nutrition 0.000 claims 1
- 239000011780 sodium chloride Substances 0.000 claims 1
- 238000009210 therapy by ultrasound Methods 0.000 claims 1
- 238000001238 wet grinding Methods 0.000 claims 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2014145632A JP6493903B2 (ja) | 2013-07-18 | 2014-07-16 | 二次黒鉛の製造方法、薄片化黒鉛の製造方法、二次黒鉛及び薄片化黒鉛 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2013149538 | 2013-07-18 | ||
| JP2013149538 | 2013-07-18 | ||
| JP2014145632A JP6493903B2 (ja) | 2013-07-18 | 2014-07-16 | 二次黒鉛の製造方法、薄片化黒鉛の製造方法、二次黒鉛及び薄片化黒鉛 |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2018200704A Division JP6818266B2 (ja) | 2013-07-18 | 2018-10-25 | 二次黒鉛の製造方法、薄片化黒鉛の製造方法、二次黒鉛及び薄片化黒鉛 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015038017A JP2015038017A (ja) | 2015-02-26 |
| JP2015038017A5 true JP2015038017A5 (enExample) | 2017-08-03 |
| JP6493903B2 JP6493903B2 (ja) | 2019-04-03 |
Family
ID=52631398
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014145632A Active JP6493903B2 (ja) | 2013-07-18 | 2014-07-16 | 二次黒鉛の製造方法、薄片化黒鉛の製造方法、二次黒鉛及び薄片化黒鉛 |
| JP2018200704A Expired - Fee Related JP6818266B2 (ja) | 2013-07-18 | 2018-10-25 | 二次黒鉛の製造方法、薄片化黒鉛の製造方法、二次黒鉛及び薄片化黒鉛 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2018200704A Expired - Fee Related JP6818266B2 (ja) | 2013-07-18 | 2018-10-25 | 二次黒鉛の製造方法、薄片化黒鉛の製造方法、二次黒鉛及び薄片化黒鉛 |
Country Status (1)
| Country | Link |
|---|---|
| JP (2) | JP6493903B2 (enExample) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101785374B1 (ko) * | 2015-07-31 | 2017-10-17 | 가천대학교 산학협력단 | 전기화학적 전처리 및 전단 유동 박리를 이용한 비산화 그래핀 제조 방법 및 장치 |
| US10381646B2 (en) | 2015-12-24 | 2019-08-13 | Semiconductor Energy Laboratory Co., Ltd. | Secondary battery, graphene oxide, and manufacturing method thereof |
| KR102068258B1 (ko) * | 2016-03-30 | 2020-01-20 | 주식회사 엘지화학 | 그래핀의 제조 방법 |
| CN106006693B (zh) * | 2016-05-17 | 2017-07-07 | 西北工业大学 | 一种高稳定性氢氧化钙/石墨烯纳米复合材料及制备方法 |
| KR101996811B1 (ko) * | 2017-05-25 | 2019-07-08 | 한국과학기술원 | 전기화학적 박리를 통한 고품질 그래핀 플레이크의 제조 방법 및 그래핀 플레이크의 분산 용액 |
| CN108117065B (zh) * | 2017-12-14 | 2020-04-17 | 北京化工大学 | 一种采用交替电流剥离制备石墨烯的方法 |
| CN108821278A (zh) * | 2018-08-21 | 2018-11-16 | 大同新成新材料股份有限公司 | 一种利用石墨烯复合材料制备膨胀石墨的方法 |
| CN110282616A (zh) * | 2019-06-29 | 2019-09-27 | 天津大学 | 复合模板制备三维石墨烯多级网络材料的方法 |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004181383A (ja) * | 2002-12-04 | 2004-07-02 | Nippon Telegr & Teleph Corp <Ntt> | 水素貯蔵用炭素材料 |
| JP4804272B2 (ja) * | 2006-08-26 | 2011-11-02 | 正義 梅野 | 単結晶グラファイト膜の製造方法 |
| US8524067B2 (en) * | 2007-07-27 | 2013-09-03 | Nanotek Instruments, Inc. | Electrochemical method of producing nano-scaled graphene platelets |
| KR101344493B1 (ko) * | 2007-12-17 | 2013-12-24 | 삼성전자주식회사 | 단결정 그라펜 시트 및 그의 제조방법 |
| KR101456905B1 (ko) * | 2010-02-19 | 2014-10-31 | 가부시키가이샤 인큐베이션 얼라이언스 | 탄소 재료 및 그 제조 방법 |
| JP2012020915A (ja) * | 2010-07-16 | 2012-02-02 | Masayoshi Umeno | 透明導電膜の形成方法及び透明導電膜 |
| JP2013067549A (ja) * | 2011-09-06 | 2013-04-18 | Waseda Univ | 薄膜の形成方法 |
| JP2013112542A (ja) * | 2011-11-25 | 2013-06-10 | Sekisui Chem Co Ltd | 層間物質挿入黒鉛及び薄片化黒鉛の製造方法 |
| US8734683B2 (en) * | 2011-11-29 | 2014-05-27 | Xerox Corporation | Graphene nano-sheets and methods for making the same |
-
2014
- 2014-07-16 JP JP2014145632A patent/JP6493903B2/ja active Active
-
2018
- 2018-10-25 JP JP2018200704A patent/JP6818266B2/ja not_active Expired - Fee Related
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