JP2014508046A - 研磨物品用のイミド架橋したバインダー - Google Patents
研磨物品用のイミド架橋したバインダー Download PDFInfo
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- JP2014508046A JP2014508046A JP2013547714A JP2013547714A JP2014508046A JP 2014508046 A JP2014508046 A JP 2014508046A JP 2013547714 A JP2013547714 A JP 2013547714A JP 2013547714 A JP2013547714 A JP 2013547714A JP 2014508046 A JP2014508046 A JP 2014508046A
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- Prior art keywords
- binder
- abrasive article
- abrasive
- article
- polymer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000006061 abrasive grain Substances 0.000 claims abstract description 32
- 150000008065 acid anhydrides Chemical class 0.000 claims abstract description 27
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- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000000203 mixture Substances 0.000 claims description 67
- 238000009472 formulation Methods 0.000 claims description 53
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- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 claims description 3
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- MTPVUVINMAGMJL-UHFFFAOYSA-N trimethyl(1,1,2,2,2-pentafluoroethyl)silane Chemical compound C[Si](C)(C)C(F)(F)C(F)(F)F MTPVUVINMAGMJL-UHFFFAOYSA-N 0.000 claims description 3
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- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 description 9
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- 239000002981 blocking agent Substances 0.000 description 8
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 description 7
- 230000008901 benefit Effects 0.000 description 7
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- 229920001577 copolymer Polymers 0.000 description 7
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 description 7
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- AMJYHMCHKZQLAY-UHFFFAOYSA-N tris(2-isocyanatophenoxy)-sulfanylidene-$l^{5}-phosphane Chemical compound O=C=NC1=CC=CC=C1OP(=S)(OC=1C(=CC=CC=1)N=C=O)OC1=CC=CC=C1N=C=O AMJYHMCHKZQLAY-UHFFFAOYSA-N 0.000 description 1
- 150000003673 urethanes Chemical class 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 239000004636 vulcanized rubber Substances 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24D—TOOLS FOR GRINDING, BUFFING OR SHARPENING
- B24D3/00—Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents
- B24D3/02—Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent
- B24D3/20—Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent and being essentially organic
- B24D3/28—Resins or natural or synthetic macromolecular compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24D—TOOLS FOR GRINDING, BUFFING OR SHARPENING
- B24D11/00—Constructional features of flexible abrasive materials; Special features in the manufacture of such materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24D—TOOLS FOR GRINDING, BUFFING OR SHARPENING
- B24D18/00—Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/62—Polymers of compounds having carbon-to-carbon double bonds
- C08G18/6216—Polymers of alpha-beta ethylenically unsaturated carboxylic acids or of derivatives thereof
- C08G18/622—Polymers of esters of alpha-beta ethylenically unsaturated carboxylic acids
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
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- Health & Medical Sciences (AREA)
- Polymers & Plastics (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polishing Bodies And Polishing Tools (AREA)
- Polyurethanes Or Polyureas (AREA)
- Laminated Bodies (AREA)
Abstract
Description
バインダー配合物サンプルを調製し、ケーニッヒ振子硬度を試験する。
対照サンプル1:メチルエチルケトン(MEK)中の13.5%固形分溶液のメチレンジアニリンを、アジプレン(Adiprene)BL−16(ケムチュラChemtura)及びアジプレンBL−40(ケムチュラ)のそれぞれが51.3gのジアミンに対して35.0g及び15.0gの比率である混合物に添加する。その溶液をガラス板上に4ミルの湿潤厚で注型し、250°Fで20.5時間乾燥させる。
ナイロン繊維からなる嵩高い不織布サンプル(500デニール2.5”及び200デニール2”の1:1ブレンド)が、4.4ポンド/リームの重量のバインダー及び35.6ポンド/リームの重量の繊維を使用して調製される。補助結合剤は、39部のハイカー(Hycar)26138、0.2部のトリトンX−100、1.5部のメラミン樹脂、及び59.3部の水からなり、生産ライン上で硬化させ、11”×11”四方に切断する。予備上引き接着剤層は270ポンド/リームの粒体及び20ポンド/リームのバインダーg数を含有して調製される。粒体内容物は70%のA2−60及び30%のハイパル(HiPal)60からなる。予備上引き接着剤層を325°Fで10分乾燥する。次いで上引き接着剤層を450ポンド/リームのコーティング重量で適用し、260°Fで6時間、続いて210°Fで14時間乾燥させる。ポリウレタン−イミドサンプルを、同じ補助結合剤、粒体パーセント及び粒体組成で、並びに同じ架橋条件を用いて調製する。それぞれのバインダーの組成を下記の表2及び表3に一覧にする。
Claims (41)
- 繊維性基材と、
前記繊維性基材の上に付着されたバインダーであって、ブロック化イソシアネート成分と酸無水物成分とから誘導されたイミド架橋したウレタン成分を含むバインダーと、
前記バインダーと接触した砥粒と
を含む研磨物品。 - 第1のバインダーと共に固定された繊維を含む不織布の繊維性基材と、
前記不織布の繊維性基材の上に付着され、かつ第2のバインダーで前記不織布の基材に固定された砥粒と、
ブロック化イソシアネート成分と酸無水物成分とから誘導されたイミド架橋したウレタン成分を含む第2バインダーと
を含む研磨物品。 - 研磨物品を形成する方法であって、
不織布を含む繊維基材を分配することと、
前記不織布の繊維性基材を、ブロック化イソシアネート成分及び酸無水物架橋剤を含むバインダー配合物でコーティングすることと、
砥粒を付着させ、前記バインダー配合物に接触させることと、
前記バインダー配合物を硬化させ、イミド架橋したウレタンバインダーを形成することと
を含む、研磨物品形成方法。 - 加工物品を研磨する方法であって、
研磨物品を加工物品の表面に接触させることと、
前記研磨物品を前記表面と接触させながら前記加工物に対して移動させることとを含み、前記研磨物品が、
繊維性基材と
前記繊維性基材の上に付着され、ブロック化イソシアネート成分と酸無水物成分都から誘導されたイミド架橋したウレタンを含むバインダーと、
前記バインダーと接触した砥粒とを含む、方法。 - 前記ブロック化イソシアネート成分がポリエーテルブロックを含む、請求項1〜4のいずれか一項に記載の研磨物品又は方法。
- 前記ブロック化イソシアネート成分がポリエステル−エーテルブロックを含む、請求項1〜5のいずれか一項に記載の研磨物品又は方法。
- 前記酸無水物成分が無水マレイン酸変性ポリマーである、請求項1〜6のいずれか一項に記載の研磨物品又は方法。
- 前記無水マレイン酸変性ポリマーが、スチレン系ポリマー、ポリオレフィン、ジエンエラストマー、ビニルエーテルポリマー、エチレン−酢酸ビニルコポリマー、アクリル系ポリマー、ポリエーテル、ポリエステル、シリコーン、又はこれらの組み合わせ、を含む、請求項1〜7のいずれか一項に記載の研磨物品又は方法。
- 前記無水マレイン酸変性ポリマーがシリコーンを含む、請求項1〜8のいずれか一項に記載の研磨物品又は方法。
- 前記無水マレイン酸変性ポリマーがスチレン系ポリマーを含む、請求項1〜9のいずれか一項に記載の研磨物品又は方法。
- 前記無水マレイン酸変性ポリマーがアクリル系ポリマーを含む、請求項1〜10のいずれか一項に記載の研磨物品又は方法。
- 前記バインダーが下引き接着剤層を形成する、請求項1〜11のいずれか一項に記載の研磨物品又は方法。
- 前記バインダーが上引き接着剤層を形成する、請求項1〜12のいずれか一項に記載の研磨物品又は方法。
- 前記バインダーが超上引き接着剤層を形成する、請求項1〜13のいずれか一項に記載の研磨物品又は方法。
- 前記砥粒が、シリカ、アルミナ(溶融した又は焼結した)、ジルコニア、ジルコニア/アルミナ酸化物、炭化ケイ素、ガーネット、ダイヤモンド、立方晶窒化ホウ素、窒化ケイ素、セリア、二酸化チタン、二ホウ化チタン、炭化ホウ素、酸化錫、炭化タングステン、炭化チタン、酸化鉄、クロミア、フリント、エメリー、それらの任意の組み合わせ、を含む、請求項1〜14のいずれか一項に記載の研磨物品又は方法。
- 前記砥粒が0.1ミクロン〜1500ミクロンの範囲にある平均粒径を有する、請求項1〜15のいずれか一項に記載の研磨物品又は方法。
- 前記バインダーがアンチローディング剤を更に含む、請求項1〜16のいずれか一項に記載の研磨物品又は方法。
- 前記アンチローディング剤がステアリン酸金属塩である、請求項1〜17のいずれか一項に記載の研磨物品又は方法。
- 前記バインダーが粘度調整剤を更に含む、請求項1〜18のいずれか一項に記載の研磨物品又は方法。
- 前記バインダーが懸濁剤を更に含む、請求項1〜19のいずれか一項に記載の研磨物品又は方法。
- 前記繊維性基材又は繊維性材料が不織布である、請求項1〜20のいずれか一項に記載の研磨物品又は方法。
- 前記繊維性基材又は不織布繊維性材料が第2のバインダーによって接合された繊維を含む、請求項1〜21のいずれか一項に記載の研磨物品又は方法。
- 前記繊維が無機繊維を含む、請求項1〜22のいずれか一項に記載の研磨物品又は方法。
- 前記繊維がポリマー繊維を含む、請求項1〜23のいずれか一項に記載の研磨物品又は方法。
- 前記ポリマー繊維がポリアミドを含む、請求項1〜24のいずれか一項に記載の研磨物品又は方法。
- 前記第2のバインダーがアクリル樹脂、ポリウレタン、酢酸ビニル、又はそれらの任意の組み合わせを含む、請求項2及び請求項22〜25のいずれか一項に記載の研磨物品又は方法。
- 前記バインダーが0.5MPa〜20MPaの範囲内の貯蔵弾性率を有する、請求項1〜26のいずれか一項に記載の研磨物品又は方法。
- 前記バインダーが200℃で少なくとも60%のTMAプローブ深さを有する、請求項1〜27のいずれか一項に記載の研磨物品又は方法。
- 前記バインダーが少なくとも−20℃のガラス転移温度を有する、請求項1〜28のいずれか一項に記載の研磨物品又は方法。
- 前記バインダーが15回振動〜160回振動の範囲のケーニッヒ振子硬度を有する、請求項1〜29のいずれか一項に記載の研磨物品又は方法。
- 前記バインダーが少なくとも200%の伸度を有する、請求項1〜30のいずれか一項に記載の研磨物品又は方法。
- 前記バインダーが20kgf/mm2〜80kgf/mm2の範囲のヌープ硬度を有する、請求項1〜31のいずれか一項に記載の研磨物品又は方法。
- 前記研磨物品が砥石車の形状である、請求項1〜32のいずれか一項に記載の研磨物品又は方法。
- 前記研磨物品がフラップの形状である、請求項1〜33のいずれか一項に記載の研磨物品又は方法。
- 前記研磨物品がベルトの形状である、請求項1〜34のいずれか一項に記載の研磨物品又は方法。
- 前記バインダー配合物及び前記砥粒を含むスラリーを形成することを更に含み、前記不織布繊維性材料を前記スラリーでコーティングすることによって、コーティングすることと付着させることとが同時に生じる、請求項3に記載の方法。
- コーティングすることが付着させることの前に起こる、請求項3又は36に記載の方法。
- 前記バインダー配合物を硬化させた後に、研磨物品が前記基材から成形されることを更に含む、請求項3、36、及び37のいずれか一項に記載の方法。
- 繊維性材料をランダムに付着させ、前記繊維性材料を第2のバインダーでコーティングすることによって基材を形成することを更に含む、請求項3及び36〜38のいずれか一項に記載の方法。
- 前記付着された砥粒を覆って第2のバインダー配合物をコーティングし、前記第2のバインダー配合物を硬化させることを更に含む、請求項3及び36〜39のいずれか一項に記載の方法。
- 前記第2のバインダー配合物が、ブロック化イソシアネート成分及び酸無水物架橋剤を含む、請求項3及び36〜40のいずれか一項に記載の方法。
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- 2011-12-30 BR BR112013016300-3A patent/BR112013016300B1/pt active IP Right Grant
- 2011-12-30 WO PCT/US2011/068248 patent/WO2012092618A2/en active Application Filing
- 2011-12-30 JP JP2013547714A patent/JP5735134B2/ja active Active
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WO2015152383A1 (ja) * | 2014-04-04 | 2015-10-08 | 株式会社フジミインコーポレーテッド | 硬質材料の研磨用組成物 |
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KR20180042290A (ko) * | 2015-08-21 | 2018-04-25 | 아우구스트 뤼게베르크 게엠베하 운트 코. 카게 | 연삭 공구 및 이러한 유형의 연삭 공구를 제조하기 위한 방법 |
JP2018528866A (ja) * | 2015-08-21 | 2018-10-04 | アウグスト リュッゲベルク ゲーエムベーハー ウント コンパニー カーゲー | 研磨工具及びこの種の研磨工具の製造方法 |
AU2015407196B2 (en) * | 2015-08-21 | 2021-11-04 | August Rüggeberg Gmbh & Co. Kg | Abrasive tool and method for producing an abrasive tool of this kind |
KR102340572B1 (ko) | 2015-08-21 | 2021-12-17 | 아우구스트 뤼게베르크 게엠베하 운트 코. 카게 | 연삭 공구 및 이러한 유형의 연삭 공구를 제조하기 위한 방법 |
US11273535B2 (en) | 2015-08-21 | 2022-03-15 | Pferd Milwaukee Brush Company, Inc. | Abrasive tool and method for producing an abrasive tool of this kind |
JP2020519468A (ja) * | 2017-05-12 | 2020-07-02 | スリーエム イノベイティブ プロパティズ カンパニー | 研磨物品中の四面体研磨粒子 |
JP2021508607A (ja) * | 2017-12-29 | 2021-03-11 | サンーゴバン アブレイシブズ,インコーポレイティド | 研磨バフ物品 |
JP7204756B2 (ja) | 2017-12-29 | 2023-01-16 | サンーゴバン アブレイシブズ,インコーポレイティド | 研磨バフ物品 |
Also Published As
Publication number | Publication date |
---|---|
MX349734B (es) | 2017-08-10 |
EP2658684A2 (en) | 2013-11-06 |
KR20130105895A (ko) | 2013-09-26 |
US20120167478A1 (en) | 2012-07-05 |
WO2012092618A2 (en) | 2012-07-05 |
CN103338901A (zh) | 2013-10-02 |
JP5735134B2 (ja) | 2015-06-17 |
MX2013007550A (es) | 2013-08-21 |
BR112013016300B1 (pt) | 2021-01-05 |
WO2012092618A3 (en) | 2012-11-08 |
CN103338901B (zh) | 2017-12-15 |
BR112013016300A2 (pt) | 2016-10-04 |
EP2658684A4 (en) | 2017-09-27 |
CA2823374A1 (en) | 2012-07-05 |
CA2823374C (en) | 2016-04-05 |
KR101571668B1 (ko) | 2015-11-25 |
US8992643B2 (en) | 2015-03-31 |
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