JP2014505779A - 潤滑組成物およびドライブライン装置を潤滑する方法 - Google Patents
潤滑組成物およびドライブライン装置を潤滑する方法 Download PDFInfo
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- JP2014505779A JP2014505779A JP2013554561A JP2013554561A JP2014505779A JP 2014505779 A JP2014505779 A JP 2014505779A JP 2013554561 A JP2013554561 A JP 2013554561A JP 2013554561 A JP2013554561 A JP 2013554561A JP 2014505779 A JP2014505779 A JP 2014505779A
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- 238000000034 method Methods 0.000 title claims abstract description 24
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- 125000001183 hydrocarbyl group Chemical group 0.000 claims abstract description 55
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- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 claims description 3
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- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims description 2
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- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 claims description 2
- KUNSUQLRTQLHQQ-UHFFFAOYSA-N copper tin Chemical compound [Cu].[Sn] KUNSUQLRTQLHQQ-UHFFFAOYSA-N 0.000 claims description 2
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- 150000002431 hydrogen Chemical class 0.000 claims 1
- 125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 claims 1
- 150000003892 tartrate salts Chemical class 0.000 claims 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 48
- 235000019198 oils Nutrition 0.000 description 39
- 150000001412 amines Chemical class 0.000 description 31
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- 230000005540 biological transmission Effects 0.000 description 22
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- 235000014113 dietary fatty acids Nutrition 0.000 description 19
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- BIGYLAKFCGVRAN-UHFFFAOYSA-N 1,3,4-thiadiazolidine-2,5-dithione Chemical compound S=C1NNC(=S)S1 BIGYLAKFCGVRAN-UHFFFAOYSA-N 0.000 description 13
- 150000001336 alkenes Chemical class 0.000 description 13
- 239000000314 lubricant Substances 0.000 description 12
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- 239000004094 surface-active agent Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000010689 synthetic lubricating oil Substances 0.000 description 1
- 229940042055 systemic antimycotics triazole derivative Drugs 0.000 description 1
- 150000003899 tartaric acid esters Chemical class 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- YBRBMKDOPFTVDT-UHFFFAOYSA-N tert-butylamine Chemical compound CC(C)(C)N YBRBMKDOPFTVDT-UHFFFAOYSA-N 0.000 description 1
- DHZWALZKPWZSMA-UHFFFAOYSA-N tetradecyl oleate Natural products CCCCCCCCCCCCCCOC(=O)CCCCCCCC=CCCCCCCCC DHZWALZKPWZSMA-UHFFFAOYSA-N 0.000 description 1
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 1
- RYYWUUFWQRZTIU-UHFFFAOYSA-K thiophosphate Chemical compound [O-]P([O-])([O-])=S RYYWUUFWQRZTIU-UHFFFAOYSA-K 0.000 description 1
- IMFACGCPASFAPR-UHFFFAOYSA-N tributylamine Chemical compound CCCCN(CCCC)CCCC IMFACGCPASFAPR-UHFFFAOYSA-N 0.000 description 1
- ABVVEAHYODGCLZ-UHFFFAOYSA-N tridecan-1-amine Chemical compound CCCCCCCCCCCCCN ABVVEAHYODGCLZ-UHFFFAOYSA-N 0.000 description 1
- SWZDQOUHBYYPJD-UHFFFAOYSA-N tridodecylamine Chemical compound CCCCCCCCCCCCN(CCCCCCCCCCCC)CCCCCCCCCCCC SWZDQOUHBYYPJD-UHFFFAOYSA-N 0.000 description 1
- 150000005691 triesters Chemical class 0.000 description 1
- LENZDBCJOHFCAS-UHFFFAOYSA-N tris Chemical compound OCC(N)(CO)CO LENZDBCJOHFCAS-UHFFFAOYSA-N 0.000 description 1
- MBYLVOKEDDQJDY-UHFFFAOYSA-N tris(2-aminoethyl)amine Chemical compound NCCN(CCN)CCN MBYLVOKEDDQJDY-UHFFFAOYSA-N 0.000 description 1
- KJIOQYGWTQBHNH-UHFFFAOYSA-N undecanol Chemical compound CCCCCCCCCCCO KJIOQYGWTQBHNH-UHFFFAOYSA-N 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 239000003981 vehicle Substances 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- LPEBYPDZMWMCLZ-CVBJKYQLSA-L zinc;(z)-octadec-9-enoate Chemical compound [Zn+2].CCCCCCCC\C=C/CCCCCCCC([O-])=O.CCCCCCCC\C=C/CCCCCCCC([O-])=O LPEBYPDZMWMCLZ-CVBJKYQLSA-L 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
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Abstract
Description
清浄剤は、過塩基化清浄剤、非過塩基化清浄剤またはそれらの混合物であってよい。
本発明の非ホウ素化分散剤は、スクシンイミド分散剤、マンニッヒ分散剤、スクシンアミド分散剤、ポリオレフィンコハク酸のエステル、アミドもしくはエステルアミド、またはそれらの混合物であってよい。一実施形態では、非ホウ素化分散剤は、スクシンイミド分散剤であってよい。
本発明は、ヒドロキシカルボン酸に由来する化合物を含有する潤滑組成物を提供する。
ヒドロキシカルボン酸に由来する化合物は、式
nおよびmは、独立して、1から5の整数であってよく;
Xは、脂肪族もしくは脂環式の基、または炭素鎖に酸素原子を含有する脂肪族もしくは脂環式の基、または上記の型の置換基であってよく、前記基は最大6個の炭素原子を含有し、n+m個の利用可能な結合点を有し(すなわち、例えば1個または複数の水素原子に結合することによって満たされる追加の結合価がXにあってよいが、特定のヒドロキシカルボン酸のためにn+m個の基に結合するのに十分な利用できる結合価が少なくともある);
各Yは、独立して、−O−もしくは>NR1であるか、または2つのYは2個のカルボニル基の間で形成されるイミド構造R−N<の窒素を一緒に表してもよく;
各RおよびR1は、独立して、水素またはヒドロカルビル基であってよく、但し、少なくとも1個のRまたはR1基はヒドロカルビル基であり;各R2は、独立して、水素、ヒドロカルビル基またはアシル基であってよく、さらに、但し、少なくとも1個の−OR2基は、−C(O)−Y−R基の少なくとも1個にαまたはβであるX中の炭素原子に位置する。
リン化合物は、リン酸エステルのアミン塩(一般的にリン酸炭化水素エステルのアミン塩)、4個以上の炭素原子を有する少なくとも1個のヒドロカルビル基を有するホスファイト、4個以上の炭素原子を有する少なくとも1個のヒドロカルビル基を有する第2のホスファイト、およびそれらの混合物からなる群から選択することができる。
一実施形態では、潤滑組成物は、リン酸エステルのアミン塩(一般的にリン酸の炭化水素エステルのアミン塩)であってよいリン化合物を含有する。ホスフェートのアミン塩は、式
R3およびR4は、独立して、水素であるか、または一般的に4から40個、もしくは6から30個、もしくは6から18個、もしくは8から18個の炭素原子を含有するヒドロカルビル基(例えば炭化水素基)であってよく、但し、少なくとも1つはヒドロカルビル基であり;R5、R6、R7およびR8は、独立して、水素またはヒドロカルビル基であってよく、但し、少なくとも1つはヒドロカルビル基である。しばしば、リン酸エステルのアミン塩は、ジアルキルおよびモノアルキルの1:1の混合物であってよく、すなわち、リン酸エステルのモル数の半分については、R3またはR4の1つは水素であってよい。
一実施形態では、潤滑組成物はホスファイトを含有し、そこで、ホスファイトは4個以上の炭素原子を有する少なくとも1個のヒドロカルビル基を有する。ホスファイトのヒドロカルビル基は、8個以上または12個以上の炭素原子を有することができる。ヒドロカルビル基の炭素原子数の一般的な範囲には、4から30、または10から24、または12から22、または14から20、または16から18が含まれる。ホスファイトは、モノヒドロカルビル置換ホスファイト、ジヒドロカルビル置換ホスファイトまたはトリヒドロカルビル置換ホスファイトであってよい。
潤滑組成物は、潤滑粘度の油を含む。そのような油には、天然および合成の油、水素化分解、水素化および水素化仕上げに由来する油、未精製油、精製油、再精製油、またはそれらの混合物が含まれる。未精製油、精製油、再精製油のより詳細な記載は、国際公開第WO2008/147704号の段落[0054]から[0056]で提供される(類似した開示は、米国特許出願第2010/197536号で提供される、[0072]から[0073]を参照)。天然および合成の潤滑油のより詳細な記載は、WO2008/147704の段落[0058]から[0059]でそれぞれ記載される(類似した開示は、米国特許出願第2010/197536号で提供される、[0075]から[0076]を参照)。合成油はフィッシャー−トロプシュ反応によって生成することもでき、一般的に水素異性化されたフィッシャー−トロプシュ炭化水素またはワックスであってよい。一実施形態では、油は、フィッシャー−トロプシュのGTL(gas−to−liquid)ガスから液体式の合成手法ならびに他のGTL油によって調製することができる。
一実施形態では、潤滑組成物は、有機硫化物またはその混合物をさらに含む。一実施形態では、有機硫化物は、ポリスルフィド、チアジアゾール化合物またはそれらの混合物の少なくとも1つを含む。
チアジアゾールの例には、2,5−ジメルカプト−1,3,4−チアジアゾールまたはそのオリゴマー、ヒドロカルビル置換2,5−ジメルカプト−1,3,4−チアジアゾール、ヒドロカルビルチオ置換2,5−ジメルカプト−1,3,4−チアジアゾールまたはそのオリゴマーが含まれる。ヒドロカルビル置換2,5−ジメルカプト−1,3,4−チアジアゾールのオリゴマーは、2,5−ジメルカプト−1,3,4−チアジアゾール単位の間で硫黄間結合を形成して2つ以上の前記チアジアゾール単位のオリゴマーを形成することによって一般的に形成される。これらのチアジアゾール化合物は、ポリイソブチレンスクシンイミドのジメルカプトチアジアゾール誘導体の形成で、下記の分散剤の後処理で用いることもできる。
一実施形態では、ポリスルフィド分子の少なくとも50重量%は、三硫化物または四硫化物の混合物である。他の実施形態では、ポリスルフィド分子の少なくとも55重量%または少なくとも60重量%は、三硫化物または四硫化物の混合物である。
一実施形態では、潤滑組成物は、摩擦調整剤をさらに含む。異なる実施形態では、摩擦調整剤は、潤滑組成物の0重量%から5重量%、0.1重量%から4重量%、0.25重量%から3.5重量%、0.5重量%から2.5重量%、および1重量%から2.5重量%、または0.05重量%から0.5重量%からなる群から選択される範囲で存在する。
本発明の組成物は、少なくとも1つの他の性能添加剤を任意選択でさらに含む。他の性能添加剤には、金属不活性化剤、分散剤(本発明の非ホウ素化分散剤以外のもの)、粘度調整剤、分散粘度調整剤、抗酸化剤、腐食防止剤、消泡剤、抗乳化剤、流動点降下剤、シール膨潤剤、リン酸およびそれらの混合物が含まれる。
本発明の方法は、様々なドライブライン装置応用体を潤滑するために有益である。ドライブライン装置は、ギア、ギアボックス、車軸ギア、トラクションドライブ変速装置、自動変速装置または手動式変速装置の少なくとも1つを含む。一実施形態では、ドライブライン装置は、手動式変速装置、またはギア、ギアボックスもしくは車軸ギアである。
(d)で示された量は、14〜50重量%の希釈油を含む。
実施例1〜10は、マグネシウム清浄剤を含有するSAEグレード75W−90の液であり、示した量は39重量%の希釈油を含む。
実施例11〜18は、カルシウム清浄剤を含有するSAEグレード75W−90の液であり、示した量は42重量%の希釈油を含む。
Claims (34)
- 潤滑粘度の油、非ホウ素化分散剤、清浄剤、ならびに(a)ヒドロキシカルボン酸の誘導体、(b)リン酸エステルのアミン塩および(c)4個以上の炭素原子を有する少なくとも1個のヒドロカルビル基を有するホスファイトを含む耐摩耗パッケージを含む潤滑組成物。
- 前記清浄剤が最高200mg KOH/g(一般的に20から175、または30から100mg KOH/g)のTBNを有する中性清浄剤である、請求項1に記載の潤滑組成物。
- 前記清浄剤が、200mg KOH/gを超える(一般的に250から600、または300から500mg KOH/g)TBNで過塩基化される、請求項1に記載の潤滑組成物。
- 前記清浄剤が、サリキサレート、サリチレート、サリゲニン、スルホネート、フェネートまたはそれらの混合物である、先行するいずれかの請求項に記載の潤滑組成物。
- 前記清浄剤が、サリキサレート、サリチレートまたはそれらの混合物である、先行するいずれかの請求項に記載の潤滑組成物。
- 前記清浄剤が、サリゲニン、フェネートまたはそれらの混合物である、先行するいずれかの請求項に記載の潤滑組成物。
- 前記清浄剤が、スルホネート、フェネートまたはそれらの混合物である、先行するいずれかの請求項に記載の潤滑組成物。
- 前記フェネートが、アルキルフェネート、アルデヒド結合アルキルフェネート、硫化アルキルフェネートまたはそれらの混合物である、請求項7に記載の潤滑組成物。
- 前記清浄剤が、アルカリ土類金属またはアルカリ金属(一般的にナトリウム、バリウム、カルシウムまたはマグネシウム)、例えばカルシウムまたはマグネシウムを含有する、先行するいずれかの請求項に記載の潤滑組成物。
- 前記清浄剤がホウ素化されたかホウ素化されていない、先行するいずれかの請求項に記載の潤滑組成物。
- 前記清浄剤が、前記潤滑組成物の0.1重量%から1重量%、または0.2重量%から0.9重量%、または0.1重量%から0.4重量%、または0.4重量%から1.0重量%で存在する、先行するいずれかの請求項に記載の潤滑組成物。
- 前記非ホウ素化分散剤がスクシンイミド分散剤、マンニッヒ分散剤、スクシンアミド分散剤、ポリオレフィンコハク酸のエステル、アミドもしくはエステルアミド、またはそれらの混合物である、先行するいずれかの請求項に記載の潤滑組成物。
- 前記非ホウ素化分散剤がスクシンイミド分散剤またはその混合物である、先行するいずれかの請求項に記載の潤滑組成物。
- 前記非ホウ素化分散剤がポリイソブチレンスクシンイミドであり、前記ポリイソブチレンスクシンイミドが由来するポリイソブチレンは350から5000、または500から3000、または750から2200、または750から1150の範囲内の数平均分子量を有する、先行するいずれかの請求項に記載の潤滑組成物。
- 前記非ホウ素化分散剤が非ホウ素化スクシンイミドであり、前記非ホウ素化分散剤がホウ素化分散剤(一般的にホウ素化ポリイソブチレンスクシンイミド)との混合物状態である、先行するいずれかの請求項に記載の潤滑組成物。
- 前記非ホウ素化分散剤が、エチレンジアミン、ジエチレントリアミン、トリエチレンテトラミン、テトラエチレンペンタミン、ペンタエチレンヘキサミン、ポリアミンスチルボトムおよびそれらの混合物からなる群から選択される脂肪族ポリアミンに由来するポリイソブチレンスクシンイミドである、先行するいずれかの請求項に記載の潤滑組成物。
- 前記非ホウ素化分散剤が、テトラエチレンペンタミン、ペンタエチレンヘキサミン、ポリアミンスチルボトムおよびそれらの混合物からなる群から選択される脂肪族ポリアミンに由来するポリイソブチレンスクシンイミドである、先行するいずれかの請求項に記載の潤滑組成物。
- 前記分散剤が、分散剤分子の50モル%未満に存在する炭素環式環を有するポリイソブチレンスクシンイミドである、先行するいずれかの請求項に記載の潤滑組成物。
- 前記分散剤が、分散剤分子の50モル%以上に存在する炭素環式環を有するポリイソブチレンスクシンイミドである、先行するいずれかの請求項に記載の潤滑組成物。
- 前記非ホウ素化分散剤が、前記潤滑組成物の0.01重量%から2重量%、または0.025重量%から1.5重量%、または0.025重量%から0.4重量%、または0.4重量%から1.2重量%で存在する、先行するいずれかの請求項に記載の潤滑組成物。
- 前記ヒドロキシカルボン酸の誘導体が、式
nおよびmは、独立して、1から5の整数であり;
Xは、脂肪族もしくは脂環式の基、または炭素鎖に酸素原子を含有する脂肪族もしくは脂環式の基、または上記の型の置換基であり、前記基は最大6個の炭素原子を含有し、n+m個の利用可能な結合点を有し、
各Yは、独立して、−O−もしくは>NR1であるか、または2つのYは2個のカルボニル基の間で形成されるイミド構造R−N<の窒素を一緒に表し;
各RおよびR1は、独立して、水素またはヒドロカルビル基であり、但し、少なくとも1個のRまたはR1基はヒドロカルビル基であり;各R2は、独立して、水素、ヒドロカルビル基またはアシル基であり、さらに、但し、少なくとも1個の−OR2基は、−C(O)−Y−R基の少なくとも1個にαまたはβであるX中の炭素原子に位置する、
先行するいずれかの請求項に記載の潤滑組成物。 - 前記ヒドロキシカルボン酸の誘導体が酒石酸の誘導体またはクエン酸の誘導体である、先行するいずれかの請求項に記載の潤滑組成物。
- 前記ヒドロキシカルボン酸の誘導体が、前記潤滑組成物の0.05重量%から1.5重量%、または0.05重量%から1重量%、または0.05重量%から0.8重量%で存在する、先行するいずれかの請求項に記載の潤滑組成物。
- 前記リン酸エステルのアミン塩が、前記潤滑組成物の0.1重量%から2.5重量%、または0.1重量%から1.5重量%、または1重量%から2重量%、または0.1重量%から1重量%で存在する、先行するいずれかの請求項に記載の潤滑組成物。
- 前記ホスファイトが、4個以上、8個以上または12個以上の炭素原子を有する少なくとも1個のヒドロカルビル基を有する、先行するいずれかの請求項に記載の潤滑組成物。
- 前記ホスファイトが、モノヒドロカルビル置換ホスファイト、ジヒドロカルビル置換ホスファイトまたはトリヒドロカルビル置換ホスファイトである、先行するいずれかの請求項に記載の潤滑組成物。
- 前記ホスファイト化合物が、前記潤滑組成物の0.05重量%から2.0重量%、または0.05重量%から1.5重量%、または0.1重量%から1.0重量%で存在する、先行するいずれかの請求項に記載の潤滑組成物。
- リン総含有量が、前記潤滑組成物の0.02から0.2重量%、または0.04から0.18重量%、または0.04から0.1重量%、または0.08から0.18重量%である、先行するいずれかの請求項に記載の潤滑組成物。
- 請求項1〜30のいずれかに記載の潤滑組成物をドライブライン装置に供給することを含む、ドライブライン装置を潤滑する方法。
- 前記ドライブライン装置が同期装置を含む、請求項31に記載の方法。
- 前記ドライブライン装置が車軸を含む、請求項31に記載の方法。
- 前記同期装置の作動表面が、真鍮、炭素、モリブデン、フェノール樹脂もしくは焼結金属(一般的にブロンズ)またはそれらの混合物を含む、請求項33に記載の方法。
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KR101496484B1 (ko) | 2007-05-24 | 2015-03-09 | 더루우브리졸코오포레이션 | 하이드록시폴리카르복시산 유도체 및 몰리브덴 화합물을 기반으로 하는 무회분 내마모제를 함유하는 윤활 조성물 |
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JP4638530B2 (ja) | 2008-08-19 | 2011-02-23 | 日本電波工業株式会社 | 圧電部品及びその製造方法 |
WO2010132318A1 (en) * | 2009-05-13 | 2010-11-18 | The Lubrizol Corporation | Imides and bis-amides as friction modifiers in lubricants |
CA2772165C (en) | 2009-08-18 | 2019-06-25 | The Lubrizol Corporation | Antiwear composition and method of lubricating driveline device |
EP2467457B1 (en) | 2009-08-18 | 2015-07-22 | The Lubrizol Corporation | Lubricating composition containing an antiwear agent |
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2012
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- 2012-02-15 WO PCT/US2012/025159 patent/WO2012112635A1/en active Application Filing
- 2012-02-15 CN CN201710675023.6A patent/CN107502414A/zh active Pending
- 2012-02-15 JP JP2013554561A patent/JP6034807B2/ja active Active
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- 2012-02-15 CA CA2827472A patent/CA2827472C/en active Active
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Also Published As
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WO2012112635A1 (en) | 2012-08-23 |
CN107502414A (zh) | 2017-12-22 |
CA2827472A1 (en) | 2012-08-23 |
EP2675875A1 (en) | 2013-12-25 |
AU2012217751A1 (en) | 2013-08-29 |
US10954465B2 (en) | 2021-03-23 |
CN103459570A (zh) | 2013-12-18 |
EP2675875B1 (en) | 2017-09-13 |
AU2012217751B2 (en) | 2016-05-26 |
CA2827472C (en) | 2019-08-20 |
US20170369810A1 (en) | 2017-12-28 |
US20140038866A1 (en) | 2014-02-06 |
JP6034807B2 (ja) | 2016-11-30 |
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