JP2013527840A5 - - Google Patents
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- Publication number
- JP2013527840A5 JP2013527840A5 JP2013505408A JP2013505408A JP2013527840A5 JP 2013527840 A5 JP2013527840 A5 JP 2013527840A5 JP 2013505408 A JP2013505408 A JP 2013505408A JP 2013505408 A JP2013505408 A JP 2013505408A JP 2013527840 A5 JP2013527840 A5 JP 2013527840A5
- Authority
- JP
- Japan
- Prior art keywords
- formula
- compound
- bromo
- chloro
- alkyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000001875 compounds Chemical class 0.000 claims 22
- 125000001246 bromo group Chemical group Br* 0.000 claims 7
- 125000001309 chloro group Chemical group Cl* 0.000 claims 7
- 239000003446 ligand Substances 0.000 claims 5
- 238000000034 method Methods 0.000 claims 5
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims 4
- -1 alkyl lithium Chemical compound 0.000 claims 4
- 239000003054 catalyst Substances 0.000 claims 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 3
- 229910052739 hydrogen Inorganic materials 0.000 claims 3
- 239000001257 hydrogen Substances 0.000 claims 3
- 125000002524 organometallic group Chemical group 0.000 claims 2
- 229910052763 palladium Inorganic materials 0.000 claims 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 claims 2
- RIOQSEWOXXDEQQ-UHFFFAOYSA-N triphenylphosphine Chemical compound C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 RIOQSEWOXXDEQQ-UHFFFAOYSA-N 0.000 claims 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 1
- PGTKVMVZBBZCKQ-UHFFFAOYSA-N Fulvene Chemical compound C=C1C=CC=C1 PGTKVMVZBBZCKQ-UHFFFAOYSA-N 0.000 claims 1
- 239000005922 Phosphane Substances 0.000 claims 1
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 claims 1
- 229910052802 copper Inorganic materials 0.000 claims 1
- 239000010949 copper Substances 0.000 claims 1
- 229910052744 lithium Inorganic materials 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- 239000011777 magnesium Substances 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 238000006385 ozonation reaction Methods 0.000 claims 1
- 229910000064 phosphane Inorganic materials 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 0 *c1ccccc1 Chemical compound *c1ccccc1 0.000 description 2
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP10160439.5 | 2010-04-20 | ||
| EP10160439 | 2010-04-20 | ||
| PCT/EP2011/055870 WO2011131544A1 (en) | 2010-04-20 | 2011-04-14 | Process for the preparation of pyrazole carboxylic acid amides |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013527840A JP2013527840A (ja) | 2013-07-04 |
| JP2013527840A5 true JP2013527840A5 (OSRAM) | 2014-03-20 |
| JP6153864B2 JP6153864B2 (ja) | 2017-06-28 |
Family
ID=43984050
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013505408A Active JP6153864B2 (ja) | 2010-04-20 | 2011-04-14 | ピラゾールカルボン酸アミドの調製方法 |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US8524915B2 (OSRAM) |
| EP (1) | EP2560960B1 (OSRAM) |
| JP (1) | JP6153864B2 (OSRAM) |
| CN (1) | CN102858749B (OSRAM) |
| AR (1) | AR080923A1 (OSRAM) |
| BR (1) | BR112012026456B1 (OSRAM) |
| ES (1) | ES2458935T3 (OSRAM) |
| IL (1) | IL222400A (OSRAM) |
| MX (1) | MX2012012009A (OSRAM) |
| TW (1) | TWI480041B (OSRAM) |
| UY (1) | UY33341A (OSRAM) |
| WO (1) | WO2011131544A1 (OSRAM) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI534126B (zh) | 2011-01-25 | 2016-05-21 | 先正達合夥公司 | 用於製備吡唑羧酸醯胺之方法 |
| CN103483407B (zh) * | 2013-10-10 | 2015-11-18 | 宁夏启元药业有限公司 | 一种硫氰酸红霉素萃取结晶用复合溶媒及萃取结晶方法 |
| GB201403438D0 (en) * | 2014-02-27 | 2014-04-16 | Syngenta Participations Ag | Polymorphs |
| CN105985254B (zh) * | 2015-02-17 | 2018-03-16 | 上海中科绿碳化工科技有限公司 | 一种制备甲酰胺类化合物的方法 |
| CN106588745B (zh) * | 2016-12-02 | 2019-06-14 | 杭州百昂锐地科技有限公司 | 一种苯并烯氟菌唑的中间体及其制备方法和应用 |
| CA3261352A1 (en) | 2022-07-22 | 2024-01-25 | Syngenta Crop Protection Ag | SOLID FORM OF A HETEROCYCLIC AMIDE DERIVATIVE |
| WO2025157998A1 (en) | 2024-01-26 | 2025-07-31 | Syngenta Crop Protection Ag | Chemical process |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH075487B2 (ja) | 1985-11-14 | 1995-01-25 | 住友化学工業株式会社 | １―ブロモ―２―クロロ―４―フルオロベンゼンの製造法 |
| US5093347A (en) | 1991-01-28 | 1992-03-03 | Monsanto Company | 3-difluoromethylpyrazolecarboxamide fungicides, compositions and use |
| US7223879B2 (en) | 1998-07-10 | 2007-05-29 | Massachusetts Institute Of Technology | Ligands for metals and improved metal-catalyzed processes based thereon |
| NZ567219A (en) * | 2005-10-25 | 2010-03-26 | Syngenta Participations Ag | Heterocyclic amide derivatives useful as microbiocides |
| AR058302A1 (es) * | 2005-12-12 | 2008-01-30 | Syngenta Participations Ag | Proceso para la preparacion de aminas |
| BRPI0717985A2 (pt) | 2006-10-25 | 2013-11-12 | Syngenta Ltd | Processo para a produção de bromobenzenos substituídos |
| CN102026982A (zh) * | 2008-05-14 | 2011-04-20 | 先正达参股股份有限公司 | 制备酰胺的方法 |
| BRPI0923401B1 (pt) * | 2008-12-24 | 2021-11-23 | Syngenta Limited | Método para o preparo de aril amidas e composto |
| BR112012024705A2 (pt) * | 2010-03-31 | 2016-06-07 | Actelion Pharmaceuticals Ltd | derivados antibacterianos de isoquinolin-3-ilureia |
| CN102906072B (zh) * | 2010-04-20 | 2014-07-02 | 先正达参股股份有限公司 | 吡唑羧酸酰胺的制备方法 |
| MX2012012007A (es) * | 2010-04-20 | 2012-12-17 | Syngenta Participations Ag | Proceso para preparar amidas de acidos carboxilicos pirazolicos. |
| WO2011131546A1 (en) * | 2010-04-20 | 2011-10-27 | Syngenta Participations Ag | Process for the preparation of pyrazole carboxylic acid amides |
-
2011
- 2011-04-14 US US13/642,511 patent/US8524915B2/en active Active
- 2011-04-14 BR BR112012026456-7A patent/BR112012026456B1/pt active IP Right Grant
- 2011-04-14 EP EP11715687.7A patent/EP2560960B1/en active Active
- 2011-04-14 ES ES11715687.7T patent/ES2458935T3/es active Active
- 2011-04-14 JP JP2013505408A patent/JP6153864B2/ja active Active
- 2011-04-14 CN CN201180019764.XA patent/CN102858749B/zh active Active
- 2011-04-14 MX MX2012012009A patent/MX2012012009A/es active IP Right Grant
- 2011-04-14 WO PCT/EP2011/055870 patent/WO2011131544A1/en not_active Ceased
- 2011-04-15 UY UY0001033341A patent/UY33341A/es active IP Right Grant
- 2011-04-18 AR ARP110101327A patent/AR080923A1/es active IP Right Grant
- 2011-04-19 TW TW100113508A patent/TWI480041B/zh active
-
2012
- 2012-10-11 IL IL222400A patent/IL222400A/en active IP Right Grant
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