JP2013516959A - 水の回収 - Google Patents
水の回収 Download PDFInfo
- Publication number
- JP2013516959A JP2013516959A JP2012548310A JP2012548310A JP2013516959A JP 2013516959 A JP2013516959 A JP 2013516959A JP 2012548310 A JP2012548310 A JP 2012548310A JP 2012548310 A JP2012548310 A JP 2012548310A JP 2013516959 A JP2013516959 A JP 2013516959A
- Authority
- JP
- Japan
- Prior art keywords
- concentrator
- storable
- drinking water
- palatable
- effluent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Images
Classifications
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- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
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- A—HUMAN NECESSITIES
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- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
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- A23L2/72—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
- A23L2/74—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration using membranes, e.g. osmosis, ultrafiltration
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/80—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by adsorption
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
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- C02F1/283—Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
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Abstract
Description
1.果実又は野菜又はサトウキビを粉砕して、内部構成成分を放出又は露出させる。又は供給された汁を使用する。
2.上記(工程1)のスラリー/汁を市販の蒸発器により処理して、濃縮及びLSJ画分を生成する。全ての蒸発器がLSJの外部水汚染を防止するように設計されているわけではないので、このようにLSJを汚染しない蒸発器、すなわちセントリサーム(Centritherm)を使用することが好ましい。
3.粗LSJを、好ましくはカチオン性樹脂、続いてアニオン性樹脂のイオン交換樹脂に通す。これにより、LSJの全有機構成成分の画分を除去し、LSJのpHを必要とされるレベルに調整する。
4.次に工程3のLSJを、海水精製又はナノ濾過に使用されるもののような低分子量カットオフ膜を有する逆浸透ユニットに通して、LSJの大部分の芳香成分の除去を達成する。
5.工程4のLSJを活性炭に通して濾過して、果実又は野菜又はサトウキビの芳香又は臭気を更に除去する。
6.この過程の後、LSJを好ましくはステンレス鋼タンクに貯蔵し、UV放射線ランプ、オゾン及び/又は濾過により滅菌を維持することができる。
7.塩基性植物由来水をパッケージする直前に、活性炭で再び濾過する。
1.更なる添加剤を用いることなく純粋、非発泡性でありうる。
2.鉱物強化されうる、炭酸化されうる又は非発泡性でありうる。
3.ビタミン/薬草抽出物及び他の植物由来添加剤を有し、非発泡性でありうる。
4.市場で受け入れられるように芳香化、風味付けされうる。
−抽出汁を濃縮する濃縮機から濃縮機排出流をもたらす工程(濃縮機排出流は、口当たりが悪い、非飲用である及び/又は貯蔵に不適切である);並びに
−濃縮機排出流を活性炭に通す工程を含む、濃縮機排出流を精製して、口当たりの良い貯蔵可能な飲用水を供給する工程
を含む方法が提供される。
●臭気#3Aを越える及び/又は飲料水に許容される閾値臭気を越える芳香/臭気構成成分;
●1cm又は約15単位のパス長を有する石英キュベットを介して測定したとき、実験室等級逆浸透水の420nm及び520nmでの分光光度吸光度の合計を越える知覚色又は吸光度;
●約0.05〜0.15°Bxの糖又は約0.005〜0.15°Bxの糖;
●水として許容できない味;
●約300〜800ppmの総溶解固形分(TDS)又は約30〜800ppmのTDS;
●約400〜2350ppm又は約30〜約2350ppmの総有機炭素(TOC);並びに
●約1.1NTU又は約0.8NTUを越える混濁度
を有する。
ヒ素0.05mg/L、バリウム1.0mg/L、ホウ酸塩30(H3BO3として計算)mg/L、カドミウム0.01mg/L、クロムVI0.05mg/L、銅1.0mg/L、シアン化物0.01(CN−として計算)mg/L、フッ化物(天然に生じる)2.0(F−として計算)mg/L、鉛0.05mg/L、マンガン2.0mg/L、水銀0.001mg/L、硝酸塩45(NO3−として計算)mg/L、亜硝酸塩0.005(NO2−として計算)mg/L、有機物質3.0(O2として消化されたKMnθ3)mg/L、セレン0.01mg/L、硫化物0.05(H2Sとして計算)mg/L又は亜鉛5.0mg/L。
●臭気#3A未満である及び/又は飲料水に許容される閾値臭気を越える芳香/臭気構成成分;
●1cm又は約15単位のパス長を有する石英キュベットを介して測定したとき、実験室等級逆浸透水の420nm及び520nmでの分光光度吸光度の合計を越える知覚色又は吸光度;
●約0.1°Bx未満の糖又は約0.005°Bx未満の糖;
●地域の飲用の飲料水として許容可能でありそれに匹敵する味;
●約50ppm未満の総溶解固形分(TDS);
●約600ppm未満の総有機炭素(TOC);並びに
●約0.5未満、好ましくは約0.5未満のNTUの混濁度
を有する
●濾過を使用して混濁度を低減する。混濁度の低減は、混濁度が比濁混濁計により決定して初めに0.5NTUを越える場合に好ましい。
●逆浸透を使用して、味に寄与する非揮発性有機化合物、例えば糖、タンニン、フェノール類及び有機酸の濃度を低減する。
●選択された活性炭を使用して、芳香に寄与する揮発性低分子量構成成分を低減する。
1.0.1〜0.22ミクロンのサイズの前濾過が、コロイド粒子及び微生物それぞれのような粒状物を除去するために必要である。このことは、逆浸透(RO)膜が閉塞及び腐敗する危険性を低減する。
2.密な膜(90ダルトン)を介した逆浸透(RO)は、味に寄与する成分をLSJにおいて低減する。これらの成分には、糖、非揮発性有機酸、タンニン、フェノール類などが含まれる。
3.芳香に寄与するLSJの残りの構成成分、すなわち低分子量揮発性有機成分は、粉末又は顆粒活性炭(GAC)のいずれかである活性炭で容易に除去される。LSJの炭素処理の好ましい方法は、生物学的に活性化された炭素(BAC)の使用である。このBACは、活性炭に結合する有機構成成分を消費し、そこに生存する細菌個体群を有し、使用する度に濾過媒体を効果的に再生する。有機構成成分をより容易に生分解性にするためには、LSJをBAC濾過の前にオゾンで処理する。
4.BACを完全に通過した液体は、供給源汁の味及び芳香を欠いており、大部分の瓶詰め飲料水と区別することができない。BACから最終水画分への微生物活性の漏出は、UV光線により破壊することができる又は0.22ミクロンの濾過により除去することができる。
5.その水は、瓶詰め及び人の消費に適している。
実施例1−ブドウ由来LSJからの口当たりの良い貯蔵可能な飲用水の回収
表1:逆浸透及び活性炭による処理後の未精製ブドウLSJの組成の変化。最終組成物は、鉱物処方及び炭酸化により強化された処理済LSJである。
LSJの品質及びその組成を許容されるレベルの貯蔵、飲用性及び/又は口当たりの良さに最適化するのに必要な処理の種類についての客観的分析は、分光光度計分析を使用して達成することができる。ここで実施例は、ブドウ汁の蒸発による方法で生成された未精製ブドウ由来LSJをどのように評価できるかを示し、決定された適切な処理を示す。
1.実験室用精製水。
2.更なる処理のない未精製ブドウLSJ。
3.顆粒活性炭(GAC)で処理された未精製ブドウLSJ。
4.逆浸透により、次にGACにより処理された未精製ブドウLSJ。
5.オーストラリア飲用水道水。
1.組成と芳香及び味の両方において完全に中立であることが知られている実験室用精製水を、適用された方法のどれがLSJの中立性を改善するかを視覚的に決定するために、スペクトル基準点として使用する。この水はY軸においてゼロAbsに最も近い。
2.対照的に未精製LSJは、Y軸において1.0Abs超(図1)及びY軸において0.1Abs超(図2)を示す線である。
3.RO及びGACの組み合わせで処理されたLSJは、Y軸においてゼロAbsから2番目の線である。
4.飲用水道水(オーストラリア)は、Y軸の上記の3と同じ点で交差する。
Claims (26)
- 抽出汁を濃縮する過程から口当たりの良い貯蔵可能な飲用水を回収する方法であって、
−抽出汁を濃縮する濃縮機から濃縮機排出流をもたらす工程(濃縮機排出流は、口当たりが悪く、非飲用であり、貯蔵に不適切である);及び
−濃縮機排出流を活性炭に通す工程を含む、濃縮機排出流を精製して、口当たりの良い貯蔵可能な飲用水を供給する工程
を含む方法。 - 抽出汁が果実又は野菜又はサトウキビ供給源のうちの少なくとも1つから得られる、請求項1記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が抽出汁の成分を含む、請求項1又は請求項2記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 成分が濃縮機排出流の味、芳香及び/又は色に影響を与える、請求項1〜3のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が、濃縮機排出流が臭気#3Aを越える及び/又は飲料水に許容される閾値臭気を越えるような芳香成分を含む、請求項1〜4のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が、1cm又は約15単位のパス長を有する石英キュベットを介して測定したとき、実験室等級逆浸透水の420nm及び520nmでの分光光度吸光度の合計を越える知覚色又は吸光度を有するような色成分を含む、請求項1〜5のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が、約0.05°Bxを越える糖又は約0.005°Bxを越える糖を有する、請求項1〜6のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が、約300〜約800ppmの総溶解固形分を有する、請求項1〜7のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が、約400〜約2350ppmの総有機炭素又は約30〜約2350ppmの総有機炭素を有する、請求項1〜8のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が、約1.1NTUを越える又は約0.8NTUを越える混濁度を有する、請求項1〜9のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流を精製する工程が、濃縮機排出流を活性炭処理の前に逆浸透及び/又は糖結合吸着剤への吸着に付す工程を含む、請求項8〜10のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流を精製する工程が、濃縮機排出流を活性炭工程の前に濾過する工程を含む、請求項8〜10のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濾過工程が、逆浸透工程の前又は糖結合吸着剤工程の前に実施される、請求項10〜12のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流を精製する工程が、濃縮機排出流をイオン交換樹脂に通す工程を更に含む、請求項1〜13のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流を精製する工程が、濃縮機排出流をオゾン処理に付す工程を更に含む、請求項1〜14のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流を精製する工程が、
−0.1μを越える粒状材料が存在する場合、排出流を濾過する工程及び
−特に排出流が0.05ブリックスを越える糖又は0.005ブリックスを越える糖を有する場合、排出流を逆浸透及び/又は糖結合吸着剤への吸着に付す工程
を更に含む、請求項1〜15のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。 - 活性炭が生物学的又は有機活性炭である、請求項16に記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- (i)濾過、(ii)逆浸透又は糖結合吸着剤への吸着及び(iii)活性炭への接触の工程が順次実施される、請求項16又は17に記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が、濃縮機排出流が臭気#3A未満である及び/又は飲料水に許容される閾値臭気を越えるような芳香成分を含む、請求項1〜18のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が、濃縮機排出流が約15単位未満の知覚色を有するような色成分を含む、請求項1〜19のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が、約0.1°Bx未満の糖又は約0.005°Bx未満の糖を有する、請求項1〜20のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が、約50ppm未満の総溶解固形分を有する、請求項1〜21のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が、約600ppm未満の総有機炭素を有する、請求項1〜22のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 濃縮機排出流が、約0.5NTU未満の混濁度を有する、請求項1〜23のいずれか1項記載の口当たりの良い貯蔵可能な飲用水を回収する方法。
- 請求項1〜24のいずれか1項記載の方法を使用して生成される口当たりの良い貯蔵可能な飲用水。
- 請求項1〜25のいずれか1項記載の方法により生成される口当たりの良い貯蔵可能な飲用水を含む瓶詰め水。
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JP2019528742A (ja) * | 2016-09-19 | 2019-10-17 | ザ コカ・コーラ カンパニーThe Coca‐Cola Company | 天然ウォーターエッセンス及びそれを製造する方法 |
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US20180072972A1 (en) * | 2016-09-09 | 2018-03-15 | Alpha Revolution, Inc. | Systems, devices and methods for fermenting beverages |
CN107937628A (zh) * | 2017-05-23 | 2018-04-20 | 中国科学院过程工程研究所 | 一种全组分利用的甘蔗制糖系统及其处理方法 |
PL422640A1 (pl) * | 2017-08-25 | 2019-03-11 | Piotr Łyczko | Sposób wytwarzania wody oraz produkt wytworzony tym sposobem |
BE1025224B9 (nl) * | 2017-12-20 | 2018-12-11 | Top Bronnen Nv | Werkwijze en inrichting voor het bottelklaar maken van mineraalwater geschikt voor limonadedranken en het verkregen mineraalwater geschikt voor limonadedranken |
EP3793947B1 (en) * | 2018-05-17 | 2022-06-29 | SABIC Global Technologies B.V. | A process to recycle water condensate from co2 off gas stream |
CH715829A1 (fr) * | 2019-02-12 | 2020-08-14 | Fabrice Thueler | Eau végétale. |
FI130897B1 (en) * | 2020-07-03 | 2024-05-15 | Lumene Oy | Use of berry fractions in cosmetic compositions |
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- 2010-12-21 CN CN2010800616831A patent/CN102724888A/zh active Pending
- 2010-12-21 ES ES10842778T patent/ES2798276T3/es active Active
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Also Published As
Publication number | Publication date |
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CN102724888A (zh) | 2012-10-10 |
CN106165810A (zh) | 2016-11-30 |
CA2786754C (en) | 2018-11-20 |
PL2523567T3 (pl) | 2020-08-24 |
WO2011085429A1 (en) | 2011-07-21 |
NZ601756A (en) | 2014-09-26 |
ZA201206121B (en) | 2013-04-24 |
AU2010342762A1 (en) | 2012-08-30 |
PT2523567T (pt) | 2020-06-22 |
EP2523567A4 (en) | 2014-09-10 |
BR112012017381B1 (pt) | 2019-08-27 |
EP2523567B1 (en) | 2020-03-18 |
ES2798276T3 (es) | 2020-12-10 |
EP2523567A1 (en) | 2012-11-21 |
AU2010342762B2 (en) | 2015-11-26 |
US9573826B2 (en) | 2017-02-21 |
US20110287144A1 (en) | 2011-11-24 |
BR112012017381A2 (pt) | 2015-09-01 |
CA2786754A1 (en) | 2011-07-21 |
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