JP2012528710A5 - - Google Patents
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- JP2012528710A5 JP2012528710A5 JP2012513612A JP2012513612A JP2012528710A5 JP 2012528710 A5 JP2012528710 A5 JP 2012528710A5 JP 2012513612 A JP2012513612 A JP 2012513612A JP 2012513612 A JP2012513612 A JP 2012513612A JP 2012528710 A5 JP2012528710 A5 JP 2012528710A5
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- 239000000203 mixture Substances 0.000 claims description 106
- 239000007789 gas Substances 0.000 claims description 84
- 239000007788 liquid Substances 0.000 claims description 76
- 239000002245 particle Substances 0.000 claims description 59
- 239000002609 medium Substances 0.000 claims description 54
- 238000000034 method Methods 0.000 claims description 53
- 239000007787 solid Substances 0.000 claims description 37
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 36
- 239000012071 phase Substances 0.000 claims description 27
- 238000001914 filtration Methods 0.000 claims description 26
- 239000007791 liquid phase Substances 0.000 claims description 25
- 239000012141 concentrate Substances 0.000 claims description 23
- 238000005984 hydrogenation reaction Methods 0.000 claims description 19
- 239000000725 suspension Substances 0.000 claims description 17
- 230000000694 effects Effects 0.000 claims description 15
- 239000012224 working solution Substances 0.000 claims description 15
- 230000008569 process Effects 0.000 claims description 14
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 claims description 12
- 238000009295 crossflow filtration Methods 0.000 claims description 11
- -1 alkyl anthraquinone Chemical class 0.000 claims description 9
- 239000003054 catalyst Substances 0.000 claims description 9
- 238000004519 manufacturing process Methods 0.000 claims description 7
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 6
- 239000001257 hydrogen Substances 0.000 claims description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims description 5
- 238000011144 upstream manufacturing Methods 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 4
- 239000011949 solid catalyst Substances 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 3
- 239000012736 aqueous medium Substances 0.000 claims description 2
- 150000002431 hydrogen Chemical class 0.000 claims description 2
- 239000003960 organic solvent Substances 0.000 claims description 2
- 230000001590 oxidative effect Effects 0.000 claims description 2
- 238000004064 recycling Methods 0.000 claims description 2
- 239000003381 stabilizer Substances 0.000 claims description 2
- 238000007872 degassing Methods 0.000 description 26
- 230000002441 reversible effect Effects 0.000 description 24
- 239000002002 slurry Substances 0.000 description 17
- 239000012530 fluid Substances 0.000 description 10
- 230000014759 maintenance of location Effects 0.000 description 10
- 238000000926 separation method Methods 0.000 description 9
- 230000008901 benefit Effects 0.000 description 6
- 230000001141 propulsive effect Effects 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 230000004907 flux Effects 0.000 description 5
- 238000003786 synthesis reaction Methods 0.000 description 5
- 150000004056 anthraquinones Chemical class 0.000 description 4
- 238000011001 backwashing Methods 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 4
- 230000007423 decrease Effects 0.000 description 4
- 239000011295 pitch Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 125000000217 alkyl group Chemical group 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 239000000706 filtrate Substances 0.000 description 3
- 230000007246 mechanism Effects 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 239000000376 reactant Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 229910002091 carbon monoxide Inorganic materials 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 239000012263 liquid product Substances 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 101150025733 pub2 gene Proteins 0.000 description 2
- 239000011343 solid material Substances 0.000 description 2
- WUKWGUZTPMOXOW-UHFFFAOYSA-N 2-(2-methylbutan-2-yl)anthracene-9,10-dione Chemical compound C1=CC=C2C(=O)C3=CC(C(C)(C)CC)=CC=C3C(=O)C2=C1 WUKWGUZTPMOXOW-UHFFFAOYSA-N 0.000 description 1
- SJEBAWHUJDUKQK-UHFFFAOYSA-N 2-ethylanthraquinone Chemical compound C1=CC=C2C(=O)C3=CC(CC)=CC=C3C(=O)C2=C1 SJEBAWHUJDUKQK-UHFFFAOYSA-N 0.000 description 1
- BQUNPXRABCSKJZ-UHFFFAOYSA-N 2-propan-2-ylanthracene-9,10-dione Chemical compound C1=CC=C2C(=O)C3=CC(C(C)C)=CC=C3C(=O)C2=C1 BQUNPXRABCSKJZ-UHFFFAOYSA-N 0.000 description 1
- YTPSFXZMJKMUJE-UHFFFAOYSA-N 2-tert-butylanthracene-9,10-dione Chemical compound C1=CC=C2C(=O)C3=CC(C(C)(C)C)=CC=C3C(=O)C2=C1 YTPSFXZMJKMUJE-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 229910052768 actinide Inorganic materials 0.000 description 1
- 150000001255 actinides Chemical class 0.000 description 1
- 239000003570 air Substances 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000007037 hydroformylation reaction Methods 0.000 description 1
- 229910052809 inorganic oxide Inorganic materials 0.000 description 1
- 229910052747 lanthanoid Inorganic materials 0.000 description 1
- 150000002602 lanthanoids Chemical class 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000035485 pulse pressure Effects 0.000 description 1
- 239000012063 pure reaction product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 150000004053 quinones Chemical class 0.000 description 1
- 239000012465 retentate Substances 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 230000002459 sustained effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09162095.5 | 2009-06-05 | ||
| EP09162095 | 2009-06-05 | ||
| PCT/EP2010/057716 WO2010139728A1 (en) | 2009-06-05 | 2010-06-02 | Process and device for separating liquid from a multiphase mixture |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015119908A Division JP2016000394A (ja) | 2009-06-05 | 2015-06-15 | 多相混合物から液体を分離するための方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012528710A JP2012528710A (ja) | 2012-11-15 |
| JP2012528710A5 true JP2012528710A5 (enExample) | 2013-06-27 |
| JP5823384B2 JP5823384B2 (ja) | 2015-11-25 |
Family
ID=41199281
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012513612A Expired - Fee Related JP5823384B2 (ja) | 2009-06-05 | 2010-06-02 | 多相混合物から液体を分離するための方法 |
| JP2015119908A Pending JP2016000394A (ja) | 2009-06-05 | 2015-06-15 | 多相混合物から液体を分離するための方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015119908A Pending JP2016000394A (ja) | 2009-06-05 | 2015-06-15 | 多相混合物から液体を分離するための方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US8758612B2 (enExample) |
| EP (1) | EP2437877B1 (enExample) |
| JP (2) | JP5823384B2 (enExample) |
| CN (1) | CN102458636B (enExample) |
| AU (1) | AU2010255724B2 (enExample) |
| BR (1) | BRPI1011148C8 (enExample) |
| WO (1) | WO2010139728A1 (enExample) |
| ZA (1) | ZA201108893B (enExample) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010139728A1 (en) * | 2009-06-05 | 2010-12-09 | Solvay Sa | Process and device for separating liquid from a multiphase mixture |
| BR112013032627A2 (pt) | 2011-06-24 | 2017-01-24 | Angus Chemical | aparelho e processo |
| KR101323181B1 (ko) * | 2013-01-28 | 2013-10-30 | 주식회사 엔바이오니아 | 섬유층을 다단식으로 적층시키는 필터섬유 적층장치와, 이를 이용한 다단식 필터여과재 제조공정 |
| WO2015006361A1 (en) | 2013-07-11 | 2015-01-15 | Invista Technologies S.À R.L. | Improved butynediol process |
| CN104418309B (zh) * | 2013-09-05 | 2016-08-17 | 中国石油化工股份有限公司 | 一种过氧化氢的制备方法 |
| CA2974405A1 (en) * | 2015-01-20 | 2016-07-28 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude (Air Liquide Sa) | Ltft catalyst fines removal |
| CN104888668B (zh) * | 2015-05-15 | 2017-07-11 | 神华集团有限责任公司 | 一种费托合成与分离的装置及方法 |
| JP6372945B2 (ja) * | 2017-10-25 | 2018-08-15 | 国立研究開発法人産業技術総合研究所 | 測定試料調製装置およびこれを用いた測定試料の調製方法 |
| EP3543208A1 (en) | 2018-03-19 | 2019-09-25 | Solvay Sa | Process for manufacturing an aqueous hydrogen peroxide solution |
| CN110339803A (zh) * | 2019-08-13 | 2019-10-18 | 江苏和纯化学工业有限公司 | 次磷酸钠反应釜缓冲罐防堵塞结构 |
| WO2021048365A1 (en) | 2019-09-11 | 2021-03-18 | Solvay Sa | Process for manufacturing an alkyl substituted cyclohexanecarbonitrile |
| CA3147483A1 (en) | 2019-09-11 | 2021-03-18 | Karol Lorent | Process for manufacturing an aqueous hydrogen peroxide solution |
| JP2022548558A (ja) | 2019-09-11 | 2022-11-21 | ソルヴェイ（ソシエテ アノニム） | 置換シクロヘキサンカルボニトリルの製造方法 |
| CL2021001192A1 (es) | 2020-05-28 | 2021-11-19 | Evonik Operations Gmbh | Dispositivo y proceso para producir peróxido de hidrógeno mediante un proceso de antraquinona |
| EP4056553A1 (en) | 2021-03-08 | 2022-09-14 | Solvay SA | Alkyl substituted cyclohexanecarbonitriles |
| EP4063355A1 (en) | 2021-03-22 | 2022-09-28 | Evonik Operations GmbH | Integrated process and plant for making styrene and propene oxide |
| ES3029833T3 (en) | 2021-05-10 | 2025-06-25 | Evonik Operations Gmbh | An integrated plant and an integrated process for making propene oxide |
| EP4337603B1 (en) | 2021-05-10 | 2025-04-09 | Evonik Operations GmbH | Optimized steam network for the ao process |
| WO2024100221A1 (en) | 2022-11-10 | 2024-05-16 | Solvay Sa | Novel synthesis for nitrile solvents |
| WO2024110260A1 (en) | 2022-11-25 | 2024-05-30 | Solvay Sa | Novel synthesis for a nitrile solvent |
| WO2024120808A1 (en) | 2022-12-06 | 2024-06-13 | Solvay Sa | Novel mixture of cyclohexane carbonitrile isomers |
| WO2024125974A1 (en) | 2022-12-12 | 2024-06-20 | Solvay Sa | Process for manufacturing an aqueous hydrogen peroxide solution by using alkyl-cyclohexane carbonitrile solvents |
Family Cites Families (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3245318C3 (de) | 1982-12-08 | 1996-06-20 | Bayer Ag | Verfahren zur Durchführung von Druckreaktionen mit suspendierten Katalysatoren |
| US4605678A (en) | 1984-03-12 | 1986-08-12 | Mobil Oil Corporation | Separation of catalyst from slurry bubble column wax and catalyst recycle |
| JPS62132514A (ja) * | 1985-12-03 | 1987-06-15 | Ngk Insulators Ltd | クロスフロ−濾過器 |
| US5324335A (en) | 1986-05-08 | 1994-06-28 | Rentech, Inc. | Process for the production of hydrocarbons |
| JPH03229637A (ja) * | 1990-02-02 | 1991-10-11 | Asahi Chem Ind Co Ltd | スラリー触媒の製造法 |
| CA2038772C (en) | 1990-04-04 | 2001-12-25 | Eric Herbolzheimer | Catalyst fluidization improvements |
| JP3268022B2 (ja) * | 1992-09-03 | 2002-03-25 | 旭化成株式会社 | カルボン酸エステルの製造方法 |
| CA2105940C (en) | 1992-10-05 | 2001-12-25 | Robert M. Koros | Bubble column, tube side slurry process and apparatus |
| US5599849A (en) | 1993-01-27 | 1997-02-04 | Sasol Chemical Industries (Proprietary) Limited | Process for producing liquid and, optionally, gaseous products from gaseous reactants |
| GB9301723D0 (en) | 1993-01-28 | 1993-03-17 | Norske Stats Oljeselskap | Solid/liquid treatment apparatus and catalytic multi-phase reactor |
| US5527473A (en) | 1993-07-15 | 1996-06-18 | Ackerman; Carl D. | Process for performing reactions in a liquid-solid catalyst slurry |
| GB2281224B (en) | 1993-08-24 | 1998-02-11 | Norske Stats Oljeselskap | Solid/liquid slurry treatment apparatus and catalytic multi-phase reactor |
| US5900159A (en) | 1996-02-29 | 1999-05-04 | Shell Oil Company | Method for separating liquid from a slurry |
| DE19611976A1 (de) * | 1996-03-26 | 1997-10-02 | Basf Ag | Verfahren und Reaktor zur Durchführung von Stoffumwandlungen mit in Flüssigkeiten suspendierten Katalysatoren |
| FR2777798B1 (fr) | 1998-04-27 | 2000-06-02 | Inst Francais Du Petrole | Procede et dispositif d'amelioration de la purete d'un produit en lit mobile simule comprenant une recirculation forcee de fluide |
| AU767574B2 (en) * | 1998-09-12 | 2003-11-20 | Evonik Degussa Gmbh | Method for carrying out gas-liquid reactions and corresponding flow reactor |
| FR2796311B1 (fr) * | 1999-07-16 | 2001-09-14 | Atofina | Reacteur multietage, ses applications et procede de fabrication du peroxyde d'hydrogene |
| FR2832937B1 (fr) * | 2001-12-04 | 2004-01-16 | Technip France | Procede et dispositif de reaction chimique entre un gaz et au moins un compose en solution, mis en oeuvre en presence d'un catalyseur solide |
| ZA200407368B (en) | 2002-04-16 | 2006-02-22 | Conocophillips Co | Optimized solid/liquid separation system for multiphase converters. |
| US7375431B1 (en) | 2005-03-18 | 2008-05-20 | National Semiconductor Corporation | Solder bump formation in electronics packaging |
| US7378452B2 (en) | 2005-12-28 | 2008-05-27 | Exxonmobil Research And Engineering Company | Filtration system for slurry hydrocarbon synthesis process using both small and large pore filter elements |
| CN100371309C (zh) * | 2006-02-17 | 2008-02-27 | 黎明化工研究院 | 一种蒽醌法生产过氧化氢流化床氢化工艺 |
| US7655135B2 (en) | 2006-03-14 | 2010-02-02 | Syntroleum Corporation | Process for removing solid particles from a hydroprocessing feed |
| CN100443155C (zh) * | 2006-05-31 | 2008-12-17 | 中国石油化工股份有限公司 | 一种浆态床环流反应器及其应用 |
| CN101314120B (zh) * | 2007-05-31 | 2010-05-26 | 中国石油化工股份有限公司 | 一种浆态床反应器及其应用 |
| US10086365B2 (en) | 2007-08-30 | 2018-10-02 | Res Usa, Llc | Strengthened iron catalyst for slurry reactors |
| WO2010139728A1 (en) * | 2009-06-05 | 2010-12-09 | Solvay Sa | Process and device for separating liquid from a multiphase mixture |
-
2010
- 2010-06-02 WO PCT/EP2010/057716 patent/WO2010139728A1/en not_active Ceased
- 2010-06-02 US US13/375,691 patent/US8758612B2/en not_active Expired - Fee Related
- 2010-06-02 AU AU2010255724A patent/AU2010255724B2/en not_active Ceased
- 2010-06-02 JP JP2012513612A patent/JP5823384B2/ja not_active Expired - Fee Related
- 2010-06-02 CN CN201080024802.6A patent/CN102458636B/zh not_active Expired - Fee Related
- 2010-06-02 BR BRPI1011148A patent/BRPI1011148C8/pt not_active IP Right Cessation
- 2010-06-02 EP EP10724469.1A patent/EP2437877B1/en not_active Not-in-force
-
2011
- 2011-12-02 ZA ZA2011/08893A patent/ZA201108893B/en unknown
-
2015
- 2015-06-15 JP JP2015119908A patent/JP2016000394A/ja active Pending
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