JP2012213833A - Sintered body for pad conditioning and its manufacturing method - Google Patents

Sintered body for pad conditioning and its manufacturing method Download PDF

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JP2012213833A
JP2012213833A JP2011080945A JP2011080945A JP2012213833A JP 2012213833 A JP2012213833 A JP 2012213833A JP 2011080945 A JP2011080945 A JP 2011080945A JP 2011080945 A JP2011080945 A JP 2011080945A JP 2012213833 A JP2012213833 A JP 2012213833A
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polishing
sintered body
pieces
regular hexagon
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Hiroshi Ishizuka
博 石塚
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SHINGIJUTSU KAIHATSU KK
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Abstract

PROBLEM TO BE SOLVED: To provide a sintered body for pad conditioning which can obtain a polishing tool for conditioning a CMP polishing pad which polishes the surface of a semiconductor material for LSI etc. of an ultra high-density wiring rule of 0.35 μm rule or lower, and its manufacturing method.SOLUTION: The sintered body for polishing with polishing units aligned on a polishing surface of a super-abrasive sintered body processes the surface of the super-abrasive sintered body by laser cutting, thereby the polishing units can be formed precisely while maintaining sharp edges, and with its high density polishing unit lines, the polishing tool for conditioning the CMP polishing pad which polishes the surface of the semiconductor material for LSI etc. can be provided. From a material of the round super-abrasive sintered body, two polishing patches are cut out from a regular hexagon positioned at the center of a circular form and six polishing patches are cut out from six similar material pieces positioned outside the regular hexagon. Corners of the patches are rounded so as not to damage the polished material during the polishing.

Description

本発明は、焼結体研磨部を持つ工具のための研磨用焼結体およびその製造方法に関する。とくに本発明は、各種半導体材料の表面、ハードディスクのディスク面等を研磨する、主に硬質ウレタンや不織布で構成された化学的機械的研磨(chemical-mechanical polishing:CMPと略す)パッド用の、パッドコンディショニングに用いるに好適な研磨用焼結体およびその製造方法に関する。   The present invention relates to a polishing sintered body for a tool having a sintered body polishing portion and a method for manufacturing the same. In particular, the present invention provides a pad for a chemical-mechanical polishing (abbreviated as CMP) pad composed mainly of hard urethane or non-woven fabric for polishing the surface of various semiconductor materials, the disk surface of a hard disk, etc. The present invention relates to a polishing sintered body suitable for use in conditioning and a method for producing the same.

近年、超LSIデバイスにおける配線の多層化が進むにつれて、層間絶縁膜やシリコン等金属膜ウェハの平坦化に、また、ハードディスクの高密度化が進むにつれて、ハードディスクのディスク面の平坦化に、CMPが用いられてきている。そしてCMPで用いられる研磨パッド(一般に硬質発泡ポリウレタン製や不織布製)の高い平坦化およびウェハ研磨速度を維持するためには、該研磨パッドの表面を常時または間欠的にコンディショニングする必要がある。   In recent years, CMP has been used to flatten interlayer insulating films and metal film wafers such as silicon as wiring of multilayered VLSI devices progresses, and to flatten the disk surface of hard disks as the density of hard disks increases. It has been used. In order to maintain a high level of a polishing pad (generally made of rigid foamed polyurethane or non-woven fabric) used in CMP and to maintain a wafer polishing rate, it is necessary to condition the surface of the polishing pad constantly or intermittently.

電子産業で使用されるメモリーチップ、その他のLSIデバイスの製造工程には、シリコンウエハ表面や、多層構造における層間絶縁膜の超精密平坦化が不可欠であり、これは一般に、研磨剤を含むスラリーと研磨パッドを用いたシステムにより行われている。研磨パッドは一般に硬質発泡ポリウレタン製や不織布製であるが、平坦性およびウエハ研磨速度を維持するためには、常時または間欠的にパッドの表面をコンディショニングする必要があり、この目的のために、主として、ダイヤモンド砥粒を電着により基板に固着した工具、或いは、一般に超硬合金で裏打ちされている焼結ダイヤモンド層にピラミッド状突起の列を設けた工具(コンディショナー、ドレッサー)が知られている。   In the manufacturing process of memory chips and other LSI devices used in the electronics industry, it is indispensable to ultra-precision planarize silicon wafer surfaces and interlayer insulation films in multilayer structures. This is done by a system using a polishing pad. The polishing pad is generally made of rigid polyurethane foam or non-woven fabric, but in order to maintain flatness and wafer polishing rate, it is necessary to condition the surface of the pad constantly or intermittently. A tool in which diamond abrasive grains are fixed to a substrate by electrodeposition, or a tool (conditioner or dresser) provided with a row of pyramidal protrusions on a sintered diamond layer generally lined with a cemented carbide is known.

電着タイプのコンディショニング用の工具の例として、円板形基台の円形表面の中央に、砥粒を配置しない中空領域を、その外側に第一の、さらにその外側に第二の砥粒層領域をそれぞれ設け、第一の砥粒層領域には、間隔をおいて小砥粒層部が複数列設けられ、各小砥粒層部は、略部分球面状を呈する隆起部の表面に、超砥粒を金属めっき層で固着したものであって、第二の砥粒層領域は、リング状の円周隆起部に超砥粒を金属めっき層で固着して構成されている回転研磨工具が公知である(特許文献1)。
このような電着タイプの工具は、砥粒の基板への固着が電着されたニッケルにより物理的に固着されているだけであることから保持力が必ずしも満足いくものではなく、使用中にダイヤモンド砥粒が脱落し、工具寿命は十分に長いものではなかった。
As an example of an electrodeposition-type conditioning tool, a hollow area in which no abrasive grains are arranged is arranged at the center of the circular surface of a disk-shaped base, and a first abrasive grain layer is formed on the outer side, and a second abrasive grain layer on the outer side. Each region is provided, and the first abrasive layer region is provided with a plurality of rows of small abrasive layer portions at intervals, and each small abrasive layer portion is formed on the surface of the raised portion having a substantially spherical shape, A rotating abrasive tool in which superabrasive grains are fixed with a metal plating layer, and the second abrasive layer area is formed by fixing superabrasive grains with a metal plating layer on a ring-shaped circumferential ridge. Is known (Patent Document 1).
Such electrodeposition type tools are not always satisfactory in holding power because the abrasive grains are only physically fixed to the substrate by the electrodeposited nickel. The abrasive grains fell off and the tool life was not sufficiently long.

また、ダイヤモンド等からなる砥粒をレジンボンド材で円形回転平面上に固着した砥材層を有し、該砥材層表面に放射状および同心円状にスリットを設けた研磨工具が公知である(特許文献2)。
しかし、レジンボンド材による砥粒の保持強度は必ずしも満足できるレベルにないため、用途によっては充分な工具寿命が得られず、また電着工具においても満足できるレベルにはなかった。
Also known is a polishing tool having an abrasive layer in which abrasive grains made of diamond or the like are fixed on a circular rotation plane with a resin bond material, and slits are provided radially and concentrically on the surface of the abrasive layer (patent) Reference 2).
However, since the retention strength of the abrasive grains by the resin bond material is not always at a satisfactory level, a sufficient tool life cannot be obtained depending on the application, and the electrodeposition tool is not at a satisfactory level.

また、凸部を有する台金の作用面に、気相合成法により多結晶ダイヤモンド薄膜を形成してなるドレッサが公知である(特許文献3)。
しかし、気相合成法による形成では、台金の小さな凹凸に忠実にダイヤモンド薄膜を形成することは困難で、必ずしも十分な精度が得られず、また、薄膜と台金との接合力も十分とはいえない。
Also, a dresser is known in which a polycrystalline diamond thin film is formed on the working surface of a base metal having a convex portion by a vapor phase synthesis method (Patent Document 3).
However, it is difficult to form a diamond thin film faithfully to the small unevenness of the base metal by the vapor phase synthesis method, and sufficient accuracy cannot be obtained, and the bonding force between the thin film and the base metal is not sufficient. I can't say that.

上記のような従来の研磨工具(パッドコンディショナー)は、基板(台金)に、粒子径がそれぞれ異なる複数個の砥粒粒子を固着した構造の故に、一様な砥粒(頂点)レベルが得にくいので、コンディショニング工程では基板(台金)面に対して最も突き出た粒子のみが使用される結果、過度の負荷に供されるこれらの粒子の消耗が激しく、結局本来の工具寿命に達する前に使用不可となることが多い。   The conventional polishing tool (pad conditioner) as described above has a structure in which a plurality of abrasive grains having different particle diameters are fixed to a substrate (base metal), so that a uniform abrasive grain (vertex) level can be obtained. The conditioning process uses only the most protruding particles on the substrate (base metal) surface, resulting in excessive consumption of these particles that are subjected to excessive loads, before eventually reaching the original tool life. Often unavailable.

上記のような、金属めっき層で固着された個々の超砥粒粒子に代えて、ピラミッド状の突起の列を焼結ダイヤモンドで形成した工具、特に、半導体ウェハ等の表面を高精度かつ高能率で加工可能なCMPパッドのコンディショニングに好適なCMPパッドコンディショナーとして使用する研磨工具およびその製造方法が提供された(特許文献4)。この従来技術において研磨単位と称される突起群は、超硬合金で裏打ちされている焼結ダイヤモンド層に、ワイヤカットで切り込むことにより形成される。研磨単位の形状は面間角度が90°のピラミッド型(四角錐)や四角錐台、他にも三角錐や三角錐台等が記載されている。   Instead of individual superabrasive particles fixed with a metal plating layer as described above, the surface of a pyramid-shaped projection formed of sintered diamond, in particular, the surface of a semiconductor wafer or the like has high accuracy and high efficiency. A polishing tool used as a CMP pad conditioner suitable for conditioning a CMP pad that can be processed by the above-mentioned method and a manufacturing method thereof have been provided (Patent Document 4). In this prior art, a group of protrusions called a polishing unit is formed by cutting a sintered diamond layer lined with a cemented carbide with a wire cut. As the shape of the polishing unit, a pyramid type (quadrangular pyramid) or a quadrangular pyramid with an angle between planes of 90 °, a triangular pyramid, a triangular frustum, or the like is described.

また、焼結ダイヤモンド層に、表面に対して一定レベル内に位置する平坦な頂面を持つ研磨単位を複数個配置した研磨工具であって、研磨単位は焼結ダイヤモンド層へワイヤカット等での切込みにより、先端が平面の、整列された四角や三角の角柱乃至角錐台上の切れ刃を形成する研磨工具が、本発明者により提供された(特許文献5)。   Also, a polishing tool in which a plurality of polishing units having a flat top surface located within a certain level with respect to the surface are arranged on the sintered diamond layer, and the polishing unit is formed by wire cutting or the like on the sintered diamond layer. The inventor has provided a polishing tool that forms a cutting edge on an aligned square or triangular prism or pyramid with a flat tip by cutting (Patent Document 5).

特開2002−337050号公報JP 2002-337050 A 特開2004−291184号公報JP 2004-291184 A 特開平10−071559号公報Japanese Patent Laid-Open No. 10-071559 国際公開WO2007−023949号公報International Publication WO2007-023949 特開2011−20182号公報JP2011-20182A

しかしながら、本発明者が当該分野で研究を進めるなかで、特許文献4および5のものであっても、特に近年必要となりつつある、例えば配線幅が35μmルール以下の超高精細配線を有するLSI用等の半導体材料表面を研磨するためのCMPパッド用のコンディショナーとしては、必ずしも満足できるものとはいえない。
本発明の課題は、かかる超高精細配線を有するLSI用等として好適な半導体材料表面を得るためのパッドを、より高機能に、合理的にコンディショニングするコンディショナーを得ることにある。
However, as the inventor researches in this field, even those disclosed in Patent Documents 4 and 5 are becoming particularly necessary in recent years, for example, for LSIs having ultra-high-definition wiring whose wiring width is 35 μm or less. As a conditioner for a CMP pad for polishing the surface of a semiconductor material such as the above, it is not always satisfactory.
An object of the present invention is to obtain a conditioner for rationally conditioning a pad for obtaining a semiconductor material surface suitable for an LSI having such an ultra-high-definition wiring with higher functionality.

本発明者は、上記の課題を解決すべく、なお鋭意検討する中で、ダイヤモンド等の超砥粒焼結体からなる研磨部を有するパッドコンディショナーとして、研磨用焼結体の、研磨部における研磨単位となる突起の形状を、従来に無い微小寸法、微小ピッチかつ鋭利なエッジとすることにより、特に微小線幅のLSI等に用いられる半導体材料表面研磨用CMPパッドを好適にコンディショニングすることができることを見出し、さらに研究を進めた結果、本発明を完成するに至った。   In order to solve the above problems, the present inventor is still eagerly studying, and as a pad conditioner having a polishing portion made of a superabrasive sintered body of diamond or the like, polishing the polishing sintered body in the polishing portion. By making the shape of the projection as a unit a minute dimension, a minute pitch, and a sharp edge that are not conventional, it is possible to suitably condition a CMP pad for polishing a semiconductor material surface particularly used for LSIs having a minute line width. As a result of further research, the present invention has been completed.

すなわち本発明は、以下のパッドコンディショニング用焼結体、該焼結体の製造方法、該焼結体からなる研磨パッチ、該研磨パッチの製造方法および該研磨パッチを有する工具に関する。
[1]相互に略同一平面上にある頂部を有する複数の研磨単位が、焼結体の超砥粒表層部を加工することにより200μm以下のピッチで複数個整列して形成された、超砥粒焼結体からなる、パッドコンディショニング用燒結体。
[2]加工が、レーザー加工によりおこなわれたものである、前記[1]に記載の研磨用焼結体。
[3]レーザーが青色レーザーである、前記[2]に記載の研磨用焼結体。
[4]パッドが、CMPパッドである、前記[1]〜[3]のいずれか1項に記載の研磨用焼結体。
[5]研磨単位の頂面と側壁面最上部との成す角が、90°〜60°である、前記[1]〜[4]のいずれか1項に記載の研磨用焼結体。
[6]研磨単位の頂面が多角形、または多角形の一部または全部の辺を隣接頂点を結ぶ内側または外側に湾曲した湾曲線で置き換えた形状であり、多角形の1辺の長さが、30μm以上である、前記[1]〜[5]のいずれか1項に記載の研磨用焼結体。
[7]研磨単位の底部からの高さが、50μm以下である、前記[1]〜[6]のいずれか1項に記載の研磨用焼結体。
[8]超砥粒がダイヤモンドである、前記[1]〜[7]のいずれか1項に記載の研磨用焼結体。
[9]青色レーザーを含むレーザー加工により、ダイヤモンド焼結体からなる研磨部の、表層部に溝加工することにより、相互に略同一平面上にある頂部を有する研磨単位が、200μm以下のピッチで複数個形成する、研磨用燒結体製造方法。
That is, the present invention relates to the following pad-conditioning sintered body, a method for producing the sintered body, a polishing patch comprising the sintered body, a method for producing the polishing patch, and a tool having the polishing patch.
[1] A superabrasive formed by aligning a plurality of polishing units having apexes substantially on the same plane with each other at a pitch of 200 μm or less by processing a superabrasive surface layer portion of a sintered body A sintered body for pad conditioning consisting of a grain sintered body.
[2] The polishing sintered body according to [1], wherein the processing is performed by laser processing.
[3] The polishing sintered body according to [2], wherein the laser is a blue laser.
[4] The sintered body for polishing according to any one of [1] to [3], wherein the pad is a CMP pad.
[5] The polishing sintered body according to any one of [1] to [4], wherein an angle formed between the top surface of the polishing unit and the uppermost portion of the side wall surface is 90 ° to 60 °.
[6] The top surface of the polishing unit is a polygon, or a shape in which a part or all of the sides of the polygon are replaced with a curved line curved inward or outward connecting adjacent vertices, and the length of one side of the polygon The polishing sintered body according to any one of [1] to [5], wherein is at least 30 μm.
[7] The polishing sintered body according to any one of [1] to [6], wherein the height from the bottom of the polishing unit is 50 μm or less.
[8] The sintered body for polishing according to any one of [1] to [7], wherein the superabrasive grains are diamond.
[9] By polishing a surface portion of a polished portion made of a diamond sintered body by laser processing including a blue laser, polishing units having top portions that are substantially on the same plane with each other have a pitch of 200 μm or less. A method for manufacturing a sintered body for polishing, wherein a plurality of the sintered bodies are formed.

[10]前記[1]〜[8]の超砥粒焼結体からなるパッドコンディショニング用焼結体からなる、研磨パッチであり、円板状の焼結体素材(1)の中心を通る直線(2)と、該直線に直交する半径(3)、(3’)、を2等分した点(4)、(4’)を通り、該直線(2)に平行な線と円板の中心を通り該直径と60°の角度をなす2本の直線(6)、(7)との交点(8)、(9)、(10)、(11)を結ぶ前記直線(2)に平行な線分(12)、(12’)、を1辺とする正六角形と前記直線(2)とで円板を分割して得られる4枚の分割片の、該正六角形の外側に位置する2つの部分を、前記2本の直線(6)、(7)でさらにそれぞれ3分割して得られる、6枚の合同な分割片(13)、(14)、(15)、(16)、(17)、(18)、および正六角形の3辺と直径とを辺とする2枚の台形状の分割片から、前記6枚の分割辺とほぼ合同な2枚の焼結体分割片(19)、(20)を切り出すことによって得られる、8枚のほぼ合同な焼結体分割片の、円弧状の辺の両端部角を丸めたものからなる、8枚のほぼ合同な形状の研磨パッチ。
[11]前記[10]に記載の8枚の合同な焼結体分割片を、さらに円板外形をなしていた円弧と同心円をなす円弧(23)で2つまたはそれ以上のパッチ片に分割し、円弧状の辺の両端部角を丸めて得られる、8枚のほぼ合同な研磨パッチの複数の組からなる、研磨パッチ。
[12]前記[10]に記載の研磨パッチにおいて、正六角形の内側の2枚の焼結体分割片(19)、(20)を、それぞれ正六角形の1辺で接している、外側の焼結体分割片(13)、(14)と結合した、瓢箪型のくびれを有する2枚のほぼ合同な切片(28)、(29)の組と、1辺が円弧である台形様の4枚のほぼ合同な切片(14)、(15)、(17)、(18)の組とからなる、6枚の研磨パッチ。
[13]前記[10]〜[12]のいずれかに記載の研磨パッチを、円形基板の外周部分に、1種または複数種の研磨パッチが、円周方向に均等に配置されるように設けた、研磨工具。
[14]前記[1]〜[8]に記載の研磨用焼結体からなり、円板状の焼結体素材(1)の中心を通る直線(2)と、該直線に直交する半径(3)、(3’)を2等分した点(4)、(4’)を通り該直線に平行な線と円板の中心を通り該直径と60°の角度をなす2本の直線(6)、(7)との交点(8)、(9)、(10)、(11)を結ぶ前記直線に平行な線分(12)、(12’)を1辺とする正六角形とで円板を4枚に分割し、該正六角形の外側に位置する2つの部分を、前記2本の直線(6)(7)でさらにそれぞれ3分割して得られる、6枚の合同な分割片(13)、(14)、(15)、(16)、(17)、(18)、および正六角形の3辺と直径とを辺とする2枚の台形状の分割片(19)、(20)から切り出すことにより、円板状の焼結体素材から8枚の焼結体分割片を得る、研磨パッチ製造方法。
[15]前記[14]に記載の方法において、正六角形の内側の2枚の焼結体分割片(19)、(20)と、それぞれ正六角形の1辺で接している、外側の焼結体分割片(13)、(14)との間は切断せずに、瓢箪型のくびれを有する2枚の合同な切片(28)、(29)として残す、1辺が円弧である台形様の4枚の合同な切片(14)、(15)、(17)、(18)の組と、瓢箪型の括れを有する2枚の合同な切片(28)、(29)とから切り出すことにより、円板状焼結体素材から6枚の研磨パッチを製造する方法である。
[10] A polishing patch comprising a pad-conditioning sintered body comprising the superabrasive sintered bodies of [1] to [8] above, and a straight line passing through the center of the disc-shaped sintered body material (1). The line (2) and the radii (3), (3 ′) perpendicular to the straight line are divided into two equal points (4), (4 ′), and the line parallel to the straight line (2) and the disc Parallel to the straight line (2) connecting the intersections (8), (9), (10) and (11) with two straight lines (6) and (7) passing through the center and forming an angle of 60 ° with the diameter. Of the four divided pieces obtained by dividing the disk into regular hexagons each having a straight line segment (12), (12 ′) as one side and the straight line (2), are located outside the regular hexagon. Two concatenated pieces (13), (14), (15), (16), obtained by further dividing the two portions into three parts by the two straight lines (6) and (7), respectively. (17), 18), and two trapezoidal divided pieces having three sides and a diameter of a regular hexagon as sides, and two sintered body divided pieces (19) and (20) substantially congruent with the six divided sides. 8) The substantially congruent shaped polishing patches, which are obtained by cutting out both end corners of the arc-shaped side of the eight substantially congruent sintered body divided pieces obtained by cutting out the same).
[11] Eight congruent sintered body divided pieces according to [10] are further divided into two or more patch pieces by an arc (23) concentric with the circular arc forming the outer shape of the disk. A polishing patch comprising a plurality of sets of eight substantially congruent polishing patches obtained by rounding the corners of both ends of an arc-shaped side.
[12] In the polishing patch described in [10], the two outer side sintered pieces (19) and (20) inside the regular hexagon are in contact with one side of the regular hexagon. A set of two substantially concatenated sections (28) and (29) having a saddle-shaped constriction combined with the divided pieces (13) and (14) and four trapezoid-like pieces each having a circular arc. 6 polishing patches consisting of a set of substantially congruent sections (14), (15), (17) and (18).
[13] The polishing patch according to any one of [10] to [12] is provided so that one or more types of polishing patches are evenly arranged in a circumferential direction on an outer peripheral portion of a circular substrate. A polishing tool.
[14] A straight line (2) made of the polishing sintered body according to the above [1] to [8], passing through the center of the disk-shaped sintered body material (1), and a radius ( 3) Two straight lines (3 ′) and (3 ′) are divided into two equal lines (4), (4 ′) and parallel to the straight line through the center of the disk and at an angle of 60 ° with the diameter. 6) and a regular hexagon with one side of line segments (12) and (12 ′) parallel to the straight line connecting the intersection points (8), (9), (10) and (11) with (7) Six concatenated divided pieces obtained by dividing the disc into four pieces and further dividing the two portions located outside the regular hexagon into three pieces by the two straight lines (6) and (7), respectively. (13), (14), (15), (16), (17), (18), and two trapezoidal split pieces (19) having three sides and a diameter of a regular hexagon as sides. 20) To obtain a disk-shaped of eight from the sintered body material sintered body split pieces, grinding the patch production method.
[15] In the method according to the above [14], the outer sintered body that is in contact with the two sintered body divided pieces (19) and (20) on the inner side of the regular hexagon, each on one side of the regular hexagon. A trapezoidal shape in which one side is a circular arc is left as two concatenated sections (28), (29) having a saddle-shaped constriction without cutting between the body segment pieces (13), (14) By cutting out from a set of four conjoint sections (14), (15), (17), (18) and two conjoint sections (28), (29) having a saddle-shaped constriction, This is a method for producing six polishing patches from a disk-shaped sintered material.

研磨単位の列のピッチの短いコンディショナーは、青色レーザー加工によりダイヤモンド等の超砥粒焼結体に研磨単位の列を形成することにより得られるものである。
この焼結体は、研磨部が、超硬合金の裏打ち材に焼結一体化したダイヤモンド焼結体からなるものが好ましく、研磨単位が、該研磨部を彫りこむように加工することにより形成される。
また、レーザー加工が微細加工を可能とするものであることにより、研磨単位の頂面は、多角形であるか、または湾曲した輪郭線を有する多面体形状の頂面を有する研磨単位となるように加工される。
A conditioner having a short pitch of the polishing unit rows is obtained by forming a row of polishing units on a superabrasive sintered body such as diamond by blue laser processing.
This sintered body is preferably formed of a diamond sintered body in which the polishing portion is sintered and integrated with the backing material of the cemented carbide, and the polishing unit is formed by processing so as to engrave the polishing portion. .
Further, since the laser processing enables fine processing, the top surface of the polishing unit is a polygonal or a polishing unit having a polyhedral top surface having a curved outline. Processed.

本発明は、パッドコンディショニング用超砥粒焼結体を、レーザー加工により加工して研磨単位を形成しているため、従来のワイヤカットと比較して、研磨単位の列のピッチが格段に短く、また、焼結体のエッジを鈍らせる作用が格段に少ないので、従来の研磨工具に比して、より高精度の研磨単位形状をもつパッドコンディショニング用工具が得られる。
そのために、本願発明のパッドコンディショニング用超砥粒焼結体は、従来のワイヤカットによる超砥粒焼結体の研磨工具では成し得なかった、超精細配線ルールのLSI等に用いることの出来る半導体材料表面を得るためのCMPパッドを、実現することができたものである。
さらに本願発明のパッドコンディショニング用超砥粒焼結体は、超精細配線ルール用半導体材料の表面研磨用CMPパッドのコンディショニングが可能である上に、CMPパッドのコンディショニングによる磨り減りを防止する効果が大きく、それでいてコンディショニングによるCMPパッドの研磨効果は高いという、従来に全く無かった格別の効果を奏するものである。
このコンディショナーは、ダイヤモンド等の超砥粒焼結体からなる研磨部をもつコンディショナーであり、超砥粒焼結体からなる研磨部に複数の研磨単位を形成するに際し、短波長で強力な青色レーザー加工により、短いピッチの研磨単位が形成可能である。
Since the present invention forms a polishing unit by processing a super-abrasive sintered body for pad conditioning by laser processing, the pitch of a row of polishing units is significantly shorter than conventional wire cutting, In addition, since the action of blunting the edge of the sintered body is remarkably less, a pad conditioning tool having a more accurate polishing unit shape than that of a conventional polishing tool can be obtained.
Therefore, the super-abrasive sintered body for pad conditioning according to the present invention can be used for an LSI or the like of an ultra-fine wiring rule that could not be achieved with a conventional polishing tool for a super-abrasive sintered body by wire cutting. A CMP pad for obtaining a semiconductor material surface could be realized.
Furthermore, the superabrasive sintered body for pad conditioning according to the present invention can condition a CMP pad for polishing a surface of a semiconductor material for an ultra-fine wiring rule, and has a great effect of preventing wear due to the conditioning of the CMP pad. However, the polishing effect of the CMP pad by the conditioning is high, and there is an exceptional effect that has never existed before.
This conditioner is a conditioner having a polishing portion made of a superabrasive sintered body such as diamond, and a blue laser that is powerful at a short wavelength when forming a plurality of polishing units in the polishing portion made of a superabrasive sintered body. By processing, a polishing unit with a short pitch can be formed.

本発明の研磨用焼結体は、結合材の溶融温度以上で焼結されていることにより、超砥粒の固着強度が大きく、実質上脱落がないという利点がある。とくに超砥粒としてダイヤモンド粒子を用いた場合、ダイヤモンドは、製造工程において結合材金属が溶融しかつダイヤモンドが熱力学的に安定な温度圧力条件下に供されており、ダイヤモンド微粒子が結合材金属への部分溶解を介して強力に一体化されていることにより、固着強度がさらに大きいため、実質上脱落がなくなる。   The sintered body for polishing according to the present invention is advantageous in that it is sintered at a temperature equal to or higher than the melting temperature of the binder, so that the fixing strength of the superabrasive grains is large and there is substantially no dropout. Particularly when diamond particles are used as superabrasive grains, diamond is subjected to temperature and pressure conditions in which the binder metal is melted and the diamond is thermodynamically stable in the manufacturing process, and the diamond fine particles become the binder metal. Because of the strong integration through partial dissolution, the fixing strength is further increased, so that there is virtually no dropout.

さらに研磨単位が形成されている研磨部は、表面が充分な厚さを持つ超砥粒焼結体で構成されていることにより、研磨単位が使用により磨滅しても、研磨単位を容易に再生して、本発明の工具として再利用できる。   In addition, the polishing part in which the polishing unit is formed is composed of a superabrasive sintered body with a sufficient thickness on the surface, so that even if the polishing unit is worn out by use, the polishing unit can be easily regenerated. Thus, it can be reused as the tool of the present invention.

本発明によるコンディショニング用焼結体の一例(研磨単位が四角錐台のもの)の表面を示す平面図である。It is a top view which shows the surface of an example (a grinding | polishing unit is a thing of a square pyramid) of the sintered compact for conditioning by this invention. 本発明によるコンディショニング用焼結体の一例の写真である。It is a photograph of an example of the sintered compact for conditioning by this invention. 本発明によるコンディショニング用焼結体の研磨単位の各種の例を示す説明図(平面図および側面図)である。It is explanatory drawing (plan view and side view) which shows the various examples of the grinding | polishing unit of the sintered compact for conditioning by this invention. 本発明によるコンディショニング用焼結体の製造方法を示す説明図である。It is explanatory drawing which shows the manufacturing method of the sintered compact for conditioning by this invention. 本発明によるコンディショニング用焼結体の実施例の切り出し例を示す図である。It is a figure which shows the example of a cut-out of the Example of the sintered compact for conditioning by this invention. 本発明によるコンディショニング用焼結体を用いた実施例の加工具の平面図である。It is a top view of the processing tool of the Example using the sintered compact for conditioning by this invention. 本発明による8枚研磨パッチ切り出しを説明する図である。It is a figure explaining 8 sheet | seat patch cutting out by this invention. 本発明による8枚研磨パッチ切り出しを示す図である。It is a figure which shows 8 sheet | seat patch cutout by this invention. 本発明の別の態様による16枚研磨パッチ切り出しを示す図である。It is a figure which shows 16-sheet polishing patch cut-out by another aspect of this invention. 本発明のさらに別の態様による6枚研磨パッチ切り出しを示す図である。It is a figure which shows 6 sheet | seat grinding | polishing patch cut-out by another aspect of this invention. 本発明による研磨パッチを用いた研磨用工具を示す図である。It is a figure which shows the polishing tool using the polishing patch by this invention. 本発明の別の態様による研磨パッチを用いた研磨工具を示す平面図および側面図である。It is the top view and side view which show the polishing tool using the polishing patch by another aspect of this invention. 本発明のさらに別の態様による2種の研磨パッチを用いた研磨工具を示す平面図および側面図である。It is the top view and side view which show the polishing tool using 2 types of polishing patches by another aspect of this invention.

本発明の研磨用焼結体の材料となる超砥粒焼結体は、ダイヤモンドやc−BN(立方晶窒化硼素)等の超砥粒の粉末を常法により超高圧高温工程で処理して得られる。この状態の焼結体は超砥粒焼結体は歪みが大きいので型放電加工などにより予備的にあらかた平坦化しておく。次いで、本発明で特定する態様にて溝及び突起側面を段階的に形成していくことにより、研磨単位、即ち、直接研磨対象と接触する突起部分を創生する。なお超砥粒焼結体として市販品を利用する場合は、仕様によるが、表面が平坦化されているので、上記平坦化予備処理は省略できる。
前記溝の形成には、レーザーカット、とくに青色レーザー、例えばYAGレーザーを用いて、短いピッチで研磨単位を形成し、研磨単位の研磨作用をおこなうエッジが比較的鋭利な状態を保って加工することができる。
The superabrasive sintered body as a material of the polishing sintered body of the present invention is obtained by treating superabrasive powders such as diamond and c-BN (cubic boron nitride) in an ultrahigh pressure and high temperature process by a conventional method. can get. Since the sintered body in this state has a large strain in the superabrasive sintered body, it is preliminarily flattened by die discharge machining or the like. Next, by forming the grooves and the side surfaces of the protrusions in a stepwise manner in a manner specified by the present invention, a polishing unit, that is, a protrusion portion that directly contacts the object to be polished is created. When a commercially available product is used as the superabrasive sintered body, although depending on the specifications, since the surface is flattened, the flattening pretreatment can be omitted.
For the formation of the groove, a laser cut, in particular, a blue laser, for example, a YAG laser, is used to form a polishing unit at a short pitch and to process the polishing unit with a sharp edge. Can do.

本発明の研磨用焼結体において、上記研磨単位は、例えば、円形、または同心の中心円形孔を有する円環状焼結体層へ、レーザー加工機で切り込むことにより、創生することができる。レーザー加工機は、スキャン動作により所望の形状での焼結体層への切り込み加工を、焼結体層へのダメージを与えずにおこなうことが可能であるため、エッジの鈍りの少ない任意の形状の研磨単位が形成可能である。レーザー加工動作の能率等を考慮すると、直線状にスキャンすることが好ましい。   In the polishing sintered body of the present invention, the above-mentioned polishing unit can be created, for example, by cutting with a laser processing machine into an annular sintered body layer having a circular or concentric central circular hole. The laser processing machine can perform cutting into the sintered body layer in the desired shape by scanning operation without damaging the sintered body layer, so any shape with less edge dullness can be obtained. Can be formed. Taking the efficiency of the laser processing operation into consideration, it is preferable to scan linearly.

研磨単位が頂部に直線状の稜線を呈する形状(図3;No.1 三角錐台、No.3 六角錐台、 No.4 四角錐台)や、稜線が湾曲しているもの(図3 ; No.2)などであってもよい。研磨単位は、レーザー加工機により形成されるので、ワイヤカット放電加工に比べて、格段に細かい密度で形成でき、研磨単位の形状も、ワイヤカット放電加工に比較して、エッジの鋭い状態がたもたれるものである。   A shape in which the polishing unit has a linear ridge line at the top (FIG. 3; No. 1 triangular frustum, No. 3 hexagonal frustum, No. 4 quadrangular frustum) or a curved ridge line (FIG. 3; No. 2) may be used. Since the polishing unit is formed by a laser processing machine, it can be formed with a much finer density compared to wire-cut electric discharge machining, and the shape of the polishing unit is also sharper than that of wire-cut electric discharge machining. It is leaning.

上記例において、各研磨単位が有効な研磨部分として機能するために、各研磨単位の頂部エッジは充分に鋭く、かつ隣接研磨単位同士は、200μm以下という従来なかった短い間隔で隔てられる。エッジの長さは、各研磨単位頂部が多角形であり、一辺の長さが30μm以上という長さを有している。また、研磨単位の頂面と研磨単位側壁上端部とのなす角は、90〜60°、好ましくは90〜75°程度である。   In the above example, since each polishing unit functions as an effective polishing portion, the top edge of each polishing unit is sufficiently sharp, and adjacent polishing units are separated from each other by an unprecedented short interval of 200 μm or less. As for the length of the edge, each polishing unit top has a polygonal shape, and the length of one side is 30 μm or more. The angle formed between the top surface of the polishing unit and the upper end of the polishing unit side wall is about 90 to 60 °, preferably about 90 to 75 °.

溝の深さ(研磨単位の溝底からの高さ)は、50μm以下で、切屑を排除できる程度の深さがあれば良い。溝が深すぎると、研磨単位の強度が不足する上、過剰な超砥粒層の厚さが必要となるが、レーザー加工においては、精密な加工が可能であり、ピッチを短くすることが出来るため、溝の深さも従来に比べて浅いものが実現できる。   The depth of the groove (height from the groove bottom of the polishing unit) should be 50 μm or less, and it should be deep enough to eliminate chips. If the groove is too deep, the strength of the polishing unit will be insufficient and an excessive superabrasive layer thickness will be required, but in laser processing, precise processing is possible and the pitch can be shortened. Therefore, it is possible to realize a groove having a shallower depth than the conventional one.

研磨単位の形状としては、研磨単位の各側面を傾斜させて錐台状、例えば、四角錐台状または三角錐台状とした、図3に例示するようなものとすることが好ましい。
また、整列した角柱状や角柱台状研磨単位において、長方形や三角形のひとつまたは複数方向の側面を専用の工具で研磨することにより、頂部の縁又は頂点を鋭利化する、いわゆる「刃付け」を行なうと、さらに良好な切れ味が達成できる。研磨単位が、多角形柱、多角形錐台であり、頂部が多角形(典型的には、三角形または四角形)の場合、頂部の面の少なくとも一辺に刃付けを行なうが、研磨単位が四角錐状または三角錐状の場合は、刃付けを行なわなくても十分な切れ味を達成することができる。
The shape of the polishing unit is preferably as shown in FIG. 3 in which each side surface of the polishing unit is inclined to have a frustum shape, for example, a quadrangular frustum shape or a triangular frustum shape.
In addition, in the aligned prismatic or prismatic polishing units, so-called "blading" that sharpens the edge or vertex of the top by polishing one or more sides of a rectangle or triangle with a dedicated tool. If done, a better sharpness can be achieved. When the polishing unit is a polygonal column or a polygonal frustum, and the top is a polygon (typically a triangle or a quadrangle), cutting is performed on at least one side of the top surface, but the polishing unit is a quadrangular pyramid. In the case of a shape or a triangular pyramid shape, a sufficient sharpness can be achieved without cutting.

焼結超砥粒層としては、ダイヤモンド焼結体(PCD)やc−BN焼結体(PcBN)の一方の面を超硬合金即ち炭化タングステン系複合材、或は周期律表第6a族金属の炭化物を主成分とする複合材のブロックで裏打ちされた構造のものを用い、複合材側を接着剤等によって工具基板に固着し、反対側に区分溝を形成して研磨部として使用する。   As a sintered superabrasive layer, one surface of a diamond sintered body (PCD) or c-BN sintered body (PcBN) is cemented with a hard metal, that is, a tungsten carbide based composite material, or a group 6a metal of the periodic table. The composite material is composed of a composite material block consisting mainly of carbides, and the composite material side is fixed to the tool substrate with an adhesive or the like, and a division groove is formed on the opposite side to be used as a polishing portion.

このような焼結体は、典型的には一軸加圧型の高温超高圧静水圧プレスで調製された円板状のものが市販されている。   As such a sintered body, a disk-shaped one typically prepared by a uniaxial pressurization type high temperature ultrahigh pressure isostatic press is commercially available.

四角錐台状研磨単位の作製においては、例えば図4に示すように、研磨部の表面にYAGレーザー等のレーザー加工機で一定溝間隔(ピッチ)で第一の方向の平行溝群および錐台状体両側面を形成した後、研磨部を固着した基板ごと円環中心軸の周囲に90°回転し、同じようにして第二の方向の平行溝群を一定溝間隔で、また各溝に隣接する錐台体傾斜側面を形成することにより、直交する2組の平行溝群、および溝に沿って整列した四角錐台状研磨単位を得るようにしてもよい。   In the production of the square frustum-shaped polishing unit, for example, as shown in FIG. 4, parallel groove groups and frustums in the first direction at a constant groove interval (pitch) on the surface of the polishing portion with a laser processing machine such as a YAG laser After forming both side surfaces of the body, rotate the substrate 90 ° around the center axis of the ring together with the substrate to which the polishing part is fixed, and in the same way, parallel groove groups in the second direction are formed at a constant groove interval and in each groove. By forming adjacent frustum body inclined side surfaces, two sets of parallel groove groups orthogonal to each other and a quadrangular frustum-shaped polishing unit aligned along the grooves may be obtained.

三角錐体の場合においても、第一の方向の平行溝群および溝に隣接する角錐台の傾斜面を形成後、焼結体素材を中心軸の周囲に120°回転し、同様に一定溝間隔で第二の方向の平行溝群、および隣接する傾斜側面の形成をレーザーカットにより行う。操作完了後、研磨部をさらに120°回転し同じ操作を行うことによって、120°で交差する第三方向の平行溝群、および隣接する傾斜側面、溝に沿って整列した三角錐台状研磨単位を得るようにしてもよい。   Even in the case of a triangular pyramid, after forming the parallel groove group in the first direction and the inclined surface of the truncated pyramid adjacent to the groove, the sintered body material is rotated by 120 ° around the central axis, and the constant groove spacing is similarly applied. Then, the parallel groove groups in the second direction and the adjacent inclined side surfaces are formed by laser cutting. After the operation is completed, the polishing unit is further rotated by 120 °, and the same operation is performed, so that parallel groove groups in the third direction intersecting at 120 ° and the adjacent inclined side surfaces and the triangular frustum-shaped polishing units aligned along the grooves. May be obtained.

上記研磨単位において、錐台状体頂部の溝底面に対する突き出し高さは三角形、四角形共に50μm以下とすることができる。レーザーカットであるからこその微細加工により、研磨単位の整列ピッチが200μm以下であるため、従来よりも突き出しが浅くても、研磨部本体がパッド等のワークと直接接触することがなく、研磨単位の強度が不足したり、過剰な超砥粒層の厚さが必要となることがない。
さらにレーザーカットであるため、エッジの鈍りが少なく、本発明のような小さな突き出し高さでも、十分な研磨作用が得られる。
In the above polishing unit, the protruding height of the top of the frustum-like body with respect to the groove bottom can be 50 μm or less for both the triangle and the quadrangle. Due to the fine processing because of laser cutting, the alignment pitch of the polishing unit is 200 μm or less, so even if the protrusion is shallower than before, the polishing unit body does not come in direct contact with the work such as the pad, and the polishing unit In this case, there is no need for insufficient strength or excessive superabrasive layer thickness.
Furthermore, since it is a laser cut, there is little blunting of the edge, and a sufficient polishing action can be obtained even with a small protruding height as in the present invention.

上記研磨単位の研磨性能は、錐(台)状体の頂部に含有される超砥粒の粒度に依存する。超砥粒がダイヤモンド粒子である場合、即ち研磨部を構成する焼結体が焼結ダイヤモンド(PCD)層である場合、ダイヤモンド粒子は、40-60μm以下の公称粒度のもの、たとえば、8-16μmや0-2μmなどの各公称粒度のPCD層が利用できるが、公称粒度8-16μm以下が好ましく、特に公称粒度0-2μmが好ましい。   The polishing performance of the polishing unit depends on the particle size of the superabrasive grains contained at the top of the cone-shaped body. When the superabrasive grains are diamond particles, that is, when the sintered body constituting the polished portion is a sintered diamond (PCD) layer, the diamond particles have a nominal particle size of 40-60 μm or less, for example, 8-16 μm. PCD layers of various nominal particle sizes such as 0-2 μm can be used, but a nominal particle size of 8-16 μm or less is preferred, and a nominal particle size of 0-2 μm is particularly preferred.

本発明の研磨用焼結体に用い得るダイヤモンド焼結体は、ダイヤモンド粒子を、裏打ち材としての超硬合金および、必要に応じてコバルト等の結合材金属と共に、ダイヤモンドが熱力学的に安定な超高圧高温条件下に供して得られる。焼結体から本発明のパッドコンディショニング用超砥粒焼結体への加工はレーザーカット、典型的には青色レーザーカットによる表面の加工による研磨単位の形成によって実現できる。
焼結体素材から、研磨用焼結体を切り出すための輪郭カットにおいては、レーザーカットの他、ワイヤカット放電加工等の、一般的加工手段が利用可能である。
The diamond sintered body that can be used for the polishing sintered body according to the present invention is diamond-thermodynamically stable together with a cemented carbide as a backing material and, if necessary, a binder metal such as cobalt. It is obtained by subjecting to ultrahigh pressure and high temperature conditions. Processing from the sintered body to the super-abrasive sintered body for pad conditioning of the present invention can be realized by forming a polishing unit by processing the surface by laser cutting, typically blue laser cutting.
In contour cutting for cutting out a sintered sintered body from a sintered body material, general processing means such as wire cut electric discharge machining can be used in addition to laser cutting.

本発明においては、研磨単位の三角錐台または四角錐台等の多角形錐台体は、レーザーカットにより形成されるため、エッジが鋭くなり、また、エッジの綿密度も高いものであるため、特に0.35μm以下の超精細配線ルールのLSI用の半導体材料表面の研磨に用いるCMPパッドの効果的なコンディショニングが初めて可能となり、コンディショニングに際しての、CMPパッドの無用な摩滅も少なく抑えることが出来る。
また、ピッチの短い研磨単位列であるため、研磨作用をなすエッジの綿密度が高くなり、必要な超砥粒焼結体材料も、従来の長いピッチのものと比較して少なくて済む。
また、研磨単位の高さを従来のように高くする必要がなく、必要とされる超砥粒焼結体部分の厚みは従来よりも少なくて済む。
次に、本発明を実施例により具体的に説明する。
In the present invention, a polygonal frustum such as a triangular frustum or a quadrangular frustum of a polishing unit is formed by laser cutting, so that the edge is sharp and the cotton density of the edge is also high. In particular, effective conditioning of a CMP pad used for polishing the surface of a semiconductor material for an LSI having an ultra-fine wiring rule of 0.35 μm or less is possible for the first time, and unnecessary wear of the CMP pad during conditioning can be reduced.
In addition, since the polishing unit row has a short pitch, the cotton density of the edge that performs the polishing action is increased, and the necessary superabrasive sintered body material is less than that of the conventional long pitch.
Further, it is not necessary to increase the height of the polishing unit as in the prior art, and the required thickness of the superabrasive sintered body portion is smaller than in the prior art.
Next, the present invention will be specifically described with reference to examples.

[実施例1]
厚さ0.5mm、直径60mmの焼結ダイヤモンド層を超硬合金ブロックと一体化した、全体厚さ3.2mmの円板状ダイヤモンド焼結体をワイヤカットによって図5のように切断し、同一形状の円弧状パッチを大小2種類、各8個切り出した。より大なる円弧は8個について長さ約27mm、より小なる円弧は長さ約21mm、円弧中央における幅は、16個について同様の約7mmであった。
これらの円弧状焼結体片を大小それぞれについて5個づつ取り、平らな金属板上に向きを揃えて固定し、各ダイヤモンド層表面に青色レーザーで切込みにより、底部に対する高さ50μmの四角錐台状研磨単位群を130μmピッチの格子状に形成して研磨パッチとした。格研磨単位頂部は一辺30μmの正方形状、側壁面は軸方向に対して15°の傾斜をつけた。
[Example 1]
A sintered diamond layer having a thickness of 0.5 mm and a diameter of 60 mm and a cemented carbide block integrated with a cemented carbide block is cut into a disc-shaped diamond sintered body having a total thickness of 3.2 mm as shown in FIG. Eight arc-shaped patches of shape, each of two types, large and small, were cut out. The larger arcs had a length of about 27 mm for 8 pieces, the smaller arcs had a length of about 21 mm, and the width at the center of the arc was about 7 mm, the same for 16 pieces.
Take 5 pieces of each of these arc-shaped sintered compacts, large and small, and fix them on a flat metal plate with their orientations aligned, and cut each diamond layer surface with a blue laser to make a square pyramid with a height of 50 μm from the bottom. A group of polishing units was formed in a lattice pattern with a pitch of 130 μm to form a polishing patch. The top of the polishing unit was a square shape with a side of 30 μm, and the side wall surface was inclined 15 ° with respect to the axial direction.

これらの研磨パッチを外形108mmの円形基板の外周部分に、5個づつ交互にそれぞれ72°ごとに、各々の同心円上に配置した。各パッチは中心において長手方向を円周方向に対して30°傾斜させてそれぞれ配置し、接着剤で固定し図6に示す工具を得た。
この工具を不織布および硬質ウレタン(共にCeiba Technologies製)の研磨試験に供して表1の結果を得た。
この値は、例えば特許文献5に開示される、ワイヤカットにより研磨単位を形成した従来技術のダイヤモンド焼結体研磨工具、これは研磨単位の頂面四角形の辺の長さが100μmでピッチが1500μmのものと頂面四角形の辺200μmでピッチが2000μmのもの、と比較すると、カットレートは従来技術の80〜120μm/hと比べて百倍以上も低く、すなわち、コンディショニングされる硬質ウレタンの減りが少なく、それでいて表面粗さは従来技術のダイヤモンド焼結体研磨工具と同等または優れている、ということを意味している。
Five of these polishing patches were alternately arranged on the outer circumference of a circular substrate having an outer diameter of 108 mm on each concentric circle every 72 °. Each patch was arranged with its longitudinal direction inclined at 30 ° with respect to the circumferential direction at the center, and fixed with an adhesive to obtain the tool shown in FIG.
This tool was subjected to a polishing test of nonwoven fabric and hard urethane (both manufactured by Ciba Technologies), and the results shown in Table 1 were obtained.
This value is disclosed in, for example, Patent Document 5, a conventional diamond sintered body polishing tool in which a polishing unit is formed by wire cutting, which is 100 μm in length of the side of the top quadrangular surface of the polishing unit and 1500 μm in pitch. The cut rate is more than 100 times lower than that of the conventional technology of 80 to 120 μm / h, that is, the reduction of the hard urethane to be conditioned is small. However, it means that the surface roughness is equivalent or superior to that of the prior art diamond sintered body polishing tool.

本発明のパッドコンディショニング用焼結体は、CMPパッドコンディショナーとして、特に高精細回路ルールで製造されるLSI用の半導体材料表面の研磨に用いるためのC<Pパッドのコンディショナーとして極めて優秀である。   The sintered body for pad conditioning according to the present invention is extremely excellent as a CMP pad conditioner, particularly as a C <P pad conditioner for use in polishing the surface of a semiconductor material for LSI manufactured with a high-definition circuit rule.

本発明は、また、以上記載した、ダイヤモンド等の超砥粒焼結体からなる研磨部をもつ回転式研磨工具に用いるに好適な、円板状材料を最も効率的に利用できる、超砥粒焼結体研磨パッチおよびその製法に関する。
かかる研磨パッチおよびその製法により、上述したレーザーカットした微小ピッチ、小突起かつ鋭利なエッジを有する焼結体にかかる技術と相俟って、パッドに対する高機能なコンディショニングを可能にするばかりでなく、極めて合理的、経済的なコンディショナーを提供することが可能となる。
なお、本発明において、「円板状」と記載されている場合の円は、数学的な厳密な意味の真円のみを指すのではなく、焼結体等の実際の物質においてほぼ円形であって中心が近似的に一点に定めうる程度のものをも包含する。
The present invention also provides a superabrasive that can most efficiently utilize a disk-shaped material suitable for use in a rotary polishing tool having a polishing portion made of a superabrasive sintered body such as diamond as described above. The present invention relates to a sintered body polishing patch and a method for producing the same.
Such a polishing patch and its manufacturing method, in combination with the above-described technology related to a sintered body having a laser-cut fine pitch, small protrusions, and sharp edges, not only enables high-performance conditioning to the pad, It is possible to provide a very reasonable and economical conditioner.
In the present invention, the circle in the case of “disc shape” does not refer only to a true circle in a strict mathematical sense, but is substantially circular in an actual substance such as a sintered body. In other words, the center of which can be approximately determined at one point is also included.

ダイヤモンド等の超砥粒焼結体は、焼結体素材が円板状であり、その円板から、回転式研磨工具用の焼結体研磨パッチを、最も有効に無駄なく切り出すために、該円板の任意の位置の直径を決定し、該直径に直交する半径を2等分した点を通り、該直径に平行な線と円板の中心を通り該直径と60°の角度をなす2本の直径との交点を結ぶ該直径に平行な線分を1辺とする正六角形と該直径とで円板を4枚に分割し、該正六角形の外側に位置する2つの部分を、前記2本の直径でさらにそれぞれ3分割して得られる、6枚の合同な分割片、および正六角形の3辺と直径とを辺とする2枚の台形状の分割片から切り出した、前記6枚の分割辺と合同な2枚の焼結体分割片を切り出すことによって得られる、8枚の合同な焼結体分割片からなる本願発明の焼結体研磨パッチが得られる。
さらに円板外形をなしていた円弧と同心円をなす円弧で2つに分割して得られる合同な8枚が2組となった焼結体研磨パッチによって、本願発明の焼結体研磨パッチが得られる。
また、本願発明の別の態様においては、前記正六角形と該直径とで円板を4枚に分割することに代えて、該直径と、正六角形の該直径に平行でない4個の辺と、および円板の中心を通り該直径と60°の角度をなす2本の直径の正六角形の外側に位置する部分とで円板を分割することによって得られる、2枚の合同な1辺が円弧である瓢箪型のくびれを有する切片の組と、1辺が円弧である台形様の4枚の合同な切片の組とからなる素材が得られ、瓢箪型の切片は、さらにくびれの2つの頂点を結ぶ線に対称な外形となるように直線状の部分を加工することにより、合同な4枚の台形様切片と、その合同な台形様切片を、円弧状辺に向かい合う直線辺で接合した形の2枚の瓢箪型切片とを得る。
これらの態様の8枚、16枚または6枚の研磨パッチは、研磨効果を向上させるために、円弧側の角部分は丸く加工されて、研磨時に被研磨材に食い込むことが無いようにされていることが好ましい。
In the superabrasive sintered body such as diamond, the sintered body material is disk-shaped, and in order to cut the sintered body polishing patch for a rotary polishing tool from the disk most effectively without waste, A diameter of an arbitrary position of the disk is determined, and a radius perpendicular to the diameter is divided into two, passing through a point parallel to the diameter and the center of the disk, and forming an angle of 60 ° with the diameter 2 A regular hexagon having a line parallel to the diameter connecting the intersection with the diameter of the book as one side and the diameter divides the disk into four pieces, and two portions located outside the regular hexagon are The above six sheets cut out from six congruent divided pieces obtained by further dividing each of the two pieces into two diameters and two trapezoidal divided pieces having three sides and a diameter of a regular hexagon as sides. A book consisting of eight congruent sintered body divided pieces obtained by cutting out two sintered body divided pieces congruent with Sintered body polishing patches invention can be obtained.
Furthermore, the sintered body polishing patch according to the present invention is obtained by the sintered body polishing patch comprising two sets of congruent 8 sheets obtained by dividing into two arcs that are concentric with the arc that has formed the outer shape of the disk. It is done.
Further, in another aspect of the present invention, instead of dividing the disc into four pieces by the regular hexagon and the diameter, the diameter and four sides not parallel to the diameter of the regular hexagon, And two congruent one sides obtained by dividing the disc into two regular hexagons of two diameters that pass through the center of the disc and form an angle of 60 ° with the diameter of the disc. A material consisting of a set of sections with a saddle-shaped constriction and a trapezoid-like set of four pieces with a circular arc on one side is obtained, and the saddle-shaped section has two vertices of the constriction. By processing a linear part so that it has a symmetric outer shape with a line connecting the two, a congruent four trapezoidal pieces and a jointed trapezoidal piece with a straight side facing the arcuate side Are obtained.
In order to improve the polishing effect, the corners on the arc side of the 8, 16, or 6 polishing patches of these modes are rounded so that they do not bite into the workpiece during polishing. Preferably it is.

本発明の研磨パッチは、レーザーカットして研磨単位を研磨面に多数形成した研磨パッチを得るための超砥粒焼結体を、最も無駄なく円板状の焼結体素材から切り出すことのできる、超砥粒焼結体研磨パッチであるので、製造が困難で高価な超砥粒焼結体を最も無駄なく使用して製造することが可能となる。
また、合同な形状の研磨パッチを、複数の円板状焼結体から得られるため、研磨パッチを接着して製作する研磨工具作成時において、寸法あわせ等する必要がなく、また、本発明の研磨パッチは、必要以上に細分化した大きさでないため、研磨工具作成時の研磨パッチ接着作業が不合理に煩雑化することを防ぐことができる。
The polishing patch of the present invention is capable of cutting out a superabrasive sintered body for obtaining a polishing patch in which a number of polishing units are formed on a polishing surface by laser cutting from a disk-shaped sintered body material without waste. Since it is a superabrasive sintered body polishing patch, it is possible to manufacture by using the superabrasive sintered body, which is difficult and expensive, without waste.
Further, since the congruent shape of the polishing patch can be obtained from a plurality of disc-shaped sintered bodies, it is not necessary to adjust the size when creating a polishing tool for bonding and manufacturing the polishing patch. Since the size of the polishing patch is not more finely divided than necessary, it is possible to prevent the polishing patch adhering work when creating the polishing tool from becoming unreasonably complicated.

図1 Y:研磨単位頂面
1:パッドコンディショニング用焼結体表面
2:研磨単位頂面エッジ
3:研磨単位間の溝底面
図3 No.1:三角錐台である研磨単位の正面図および側面図
No.2:湾曲辺を有する四角錐台である研磨単位の正面図および側面図
No.3:六角錐台である研磨単位の正面図および側面図
No.4:四角錐台である研磨単位の正面図および側面図
図4 5:ダイヤモンド焼結体
6:レーザースキャンユニット
7:YAGレーザー
図5 8:円弧状焼結体片(大)
9:円弧状焼結体片(小)
図6 10:工具円形基板
11:焼結体研磨パッチ
1 Y: Polishing unit top surface 1: Surface of sintered body for pad conditioning 2: Polishing unit top surface edge 3: Groove bottom surface between polishing units 1: Front view and side view of a polishing unit that is a triangular frustum 2: Front view and side view of a polishing unit which is a quadrangular frustum having a curved side. 3: Front view and side view of polishing unit that is a hexagonal frustum 4: Front view and side view of a polishing unit which is a quadrangular pyramid FIG. 4 5: Diamond sintered body 6: Laser scanning unit 7: YAG laser FIG. 5 8: Arc-shaped sintered body piece (large)
9: Arc-shaped sintered compact (small)
Fig. 6 10: Tool circular substrate 11: Sintered body polishing patch

Claims (15)

相互に略同一平面上にある頂部を有する複数の研磨単位が、焼結体の超砥粒表層部を加工することにより200μm以下のピッチで複数個整列して形成された、超砥粒焼結体からなる、パッドコンディショニング用燒結体。   Superabrasive sintering in which a plurality of polishing units having apexes on substantially the same plane as each other are formed by aligning a plurality of polishing units on the surface of the superabrasive grain of the sintered body at a pitch of 200 μm or less. A sintered body for pad conditioning. 加工が、レーザー加工によりおこなわれたものである、請求項1に記載の研磨用焼結体。   The polishing sintered body according to claim 1, wherein the processing is performed by laser processing. レーザーが青色レーザーである、請求項2に記載の研磨用焼結体。   The polishing sintered body according to claim 2, wherein the laser is a blue laser. パッドが、CMPパッドである、請求項1〜3のいずれか1項に記載の研磨用焼結体。   The polishing sintered body according to any one of claims 1 to 3, wherein the pad is a CMP pad. 研磨単位の頂面と側壁面最上部との成す角が、90°〜60°である、請求項1〜4のいずれか1項に記載の研磨用焼結体。   The polishing sintered body according to any one of claims 1 to 4, wherein an angle formed between the top surface of the polishing unit and the uppermost portion of the side wall surface is 90 ° to 60 °. 研磨単位の頂面が多角形、または多角形の一部または全部の辺を隣接頂点を結ぶ内側または外側に湾曲した湾曲線で置き換えた形状であり、多角形の1辺の長さが、30μm以上である、請求項1〜5のいずれか1項に記載の研磨用焼結体。   The top surface of the polishing unit is a polygon, or a part or all of the sides of the polygon are replaced with a curved line curved inward or outward connecting adjacent vertices, and the length of one side of the polygon is 30 μm. It is the above, The sintered compact for grinding | polishing of any one of Claims 1-5. 研磨単位の底部からの高さが、50μm以下である、請求項1〜6のいずれか1項に記載の研磨用焼結体。   The sintered compact for polishing according to any one of claims 1 to 6, wherein the height from the bottom of the polishing unit is 50 µm or less. 超砥粒がダイヤモンドである、請求項1〜7のいずれか1項に記載の研磨用焼結体。   The polishing sintered body according to any one of claims 1 to 7, wherein the superabrasive grains are diamond. 青色レーザーを含むレーザー加工により、ダイヤモンド焼結体からなる研磨部の、表層部に溝加工することにより、相互に略同一平面上にある頂部を有する研磨単位が、200μm以下のピッチで複数個形成する、研磨用燒結体製造方法。   By polishing the surface of the polished portion made of a diamond sintered body by laser processing including blue laser, a plurality of polishing units having apexes on substantially the same plane are formed at a pitch of 200 μm or less. A method for manufacturing a sintered body for polishing. 請求項1〜8に記載の研磨用焼結体からなり、円板状の焼結体素材(1)の中心を通る直線(2)と、該直線に直交する半径(3)、(3’)を2等分した点(4)、(4’)を通り、該直線(2)に平行な線と円板の中心を通り該直線と60°の角度をなす2本の直線(6)、(7)との交点(8)、(9)、(10)、(11)を結ぶ前記直線に平行な線分(12)、(12’)を1辺とする正六角形と前記直線(2)とで円板を分割して得られる4枚の分割片の、該正六角形の外側に位置する2つの部分を、前記2本の直線(6)、(7)でさらにそれぞれ3分割して得られる、6枚の合同な分割片(13)、(14)、(15)、(16)、(17)、(18)、および正六角形の3辺と直径とを辺とする2枚の台形状の分割片から、前記6枚の分割辺とほぼ合同な2枚の焼結体分割片(19)、(20)を切り出すことによって得られる、8枚のほぼ合同な焼結体分割片の、円弧状の辺の両端部角を丸めたものからなる、8枚のほぼ合同な形状の研磨パッチ。   A straight line (2) passing through the center of the disk-shaped sintered body material (1), and a radius (3) orthogonal to the straight line (3 ' ) Are divided into two equal parts (4), (4 '), two straight lines (6) passing through the center of the disk and a line parallel to the straight line (2) and forming an angle of 60 ° with the straight line , (7) A regular hexagon with one side of line segments (12), (12 ′) parallel to the straight line connecting the lines (8), (9), (10), (11) and the straight line ( 2) Divide the two parts of the four divided pieces obtained by dividing the disc into the outer sides of the regular hexagon into three parts by the two straight lines (6) and (7). 6 concatenated divided pieces (13), (14), (15), (16), (17), (18), and two pieces having three sides of a regular hexagon and a diameter as sides From the trapezoidal split piece Of the eight substantially congruent sintered body divided pieces obtained by cutting out two sintered body divided pieces (19) and (20) substantially congruent to the six divided sides, Eight substantially congruent polishing patches made of rounded corners at both ends. 請求項10に記載の8枚の合同な焼結体分割片を、さらに円板外形をなしていた円弧と同心円をなす円弧(23)で2つまたはそれ以上のパッチ片に分割し、円弧状の辺の両端部角を丸めて得られる、8枚のほぼ合同な研磨パッチの複数の組からなる、研磨パッチ。   The eight congruent sintered body divided pieces according to claim 10 are further divided into two or more patch pieces by a circular arc (23) concentric with the circular arc that has formed the outer shape of the disk. A polishing patch comprising a plurality of sets of eight substantially congruent polishing patches, obtained by rounding the corners on both ends of the side. 請求項10に記載の研磨パッチにおいて、正六角形の内側の2枚の焼結体分割片(19)、(20)を、それぞれ正六角形の1辺で接している、外側の焼結体分割片(13)、(14)と結合した、瓢箪型のくびれを有する2枚のほぼ合同な切片(28)、(29)の組と、1辺が円弧である台形様の4枚のほぼ合同な切片(14)、(15)、(17)、(18)の組とからなる、
6枚の研磨パッチ。
11. The outer sintered body divided piece according to claim 10, wherein the two sintered body divided pieces (19) and (20) inside the regular hexagon are in contact with each other at one side of the regular hexagon. (13) A set of two substantially congruent sections (28) and (29) having a saddle-shaped constriction combined with (14) and four substantially congruent trapezoidal pieces each having a circular arc. Consisting of a set of sections (14), (15), (17), (18),
6 polishing patches.
請求項10〜12のいずれかに記載の研磨パッチを、円形基板の外周部分に、1種または複数種の研磨パッチが、円周方向に均等に配置されるように設けた、研磨工具。   A polishing tool, wherein the polishing patch according to any one of claims 10 to 12 is provided on an outer peripheral portion of a circular substrate so that one or more types of polishing patches are evenly arranged in a circumferential direction. 請求項1〜8に記載の研磨用焼結体からなり、円板状の焼結体素材(1)の中心を通る直線(2)と、該直線に直交する半径(3)、(3’)を2等分した点(4)、(4’)を通り該直線に平行な線と円板の中心を通り該直径と60°の角度をなす2本の直線(6)、(7)との交点(8)、(9)、(10)、(11)を結ぶ前記直線(2)に平行な線分(12)、(12’)を1辺とする正六角形とで円板を4枚に分割し、該正六角形の外側に位置する2つの部分を、前記2本の直線(6)、(7)でさらにそれぞれ3分割して得られる、6枚の合同な分割片(13)、(14)、(15)、(16)、(17)、(18)、および正六角形の3辺と直径とを辺とする2枚の台形状の分割片(19)、(20)から切り出すことにより、円板状の焼結体素材から8枚の焼結体分割片を得る、研磨パッチ製造方法。   A straight line (2) passing through the center of the disk-shaped sintered body material (1), and a radius (3) orthogonal to the straight line (3 ' ) Is divided into two equal parts (4), (4 ') and a line parallel to the straight line and the center of the disc, and two straight lines (6), (7) A disc with a regular hexagon with one side of line segments (12), (12 ′) parallel to the straight line (2) connecting the intersections (8), (9), (10), (11) with Six concatenated pieces (13) obtained by dividing the two parts divided into four and further dividing the two portions located outside the regular hexagon into three by the two straight lines (6) and (7), respectively. ), (14), (15), (16), (17), (18), and two trapezoidal split pieces (19), (20) having three sides and a diameter of a regular hexagon as sides. By cutting out from Obtaining a disk-shaped sintered body eight sintered body split pieces from the material, the polishing patch production method. 請求項14に記載の方法において、正六角形の内側の2枚の焼結体分割片(19)、(20)と、それぞれ正六角形の1辺で接している、外側の焼結体分割片(13)、(14)との間は切断せずに、瓢箪型のくびれを有する2枚の合同な切片(28)、(29)として残す、1辺が円弧である台形様の4枚の合同な切片(14)、(15)、(17)、(18)の組と、瓢箪型の括れを有する2枚の合同な切片(28)、(29)とから切り出すことにより円板状の焼結体素材から6枚の研磨パッチを製造する方法。   15. The method according to claim 14, wherein the outer hexagonal sintered pieces (19) and (20) are in contact with one side of the regular hexagon, respectively. 13) and (14) are not cut and left as two congruent sections (28) and (29) having a saddle-shaped constriction. Disc-shaped firing by cutting out from a set of various sections (14), (15), (17), (18) and two joint sections (28), (29) having a saddle-shaped constriction A method of manufacturing six polishing patches from a combined material.
JP2011080945A 2011-03-31 2011-03-31 Sintered body for pad conditioning and its manufacturing method Withdrawn JP2012213833A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104097146A (en) * 2013-04-08 2014-10-15 鑫晶鑽科技股份有限公司 Polishing pad dresser structure and manufacturing method thereof
JP2018192616A (en) * 2017-05-16 2018-12-06 中國砂輪企業股▲ふん▼有限公司 Grinding tool and manufacturing method of grinding tool
WO2023126761A1 (en) * 2021-12-31 2023-07-06 3M Innovative Properties Company Conditioning disk with microfeatures

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104097146A (en) * 2013-04-08 2014-10-15 鑫晶鑽科技股份有限公司 Polishing pad dresser structure and manufacturing method thereof
JP2018192616A (en) * 2017-05-16 2018-12-06 中國砂輪企業股▲ふん▼有限公司 Grinding tool and manufacturing method of grinding tool
WO2023126761A1 (en) * 2021-12-31 2023-07-06 3M Innovative Properties Company Conditioning disk with microfeatures

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