JP2012213834A - Super-abrasive sintered body polishing patch, and method for manufacturing the same - Google Patents

Super-abrasive sintered body polishing patch, and method for manufacturing the same Download PDF

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JP2012213834A
JP2012213834A JP2011080946A JP2011080946A JP2012213834A JP 2012213834 A JP2012213834 A JP 2012213834A JP 2011080946 A JP2011080946 A JP 2011080946A JP 2011080946 A JP2011080946 A JP 2011080946A JP 2012213834 A JP2012213834 A JP 2012213834A
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polishing
patch
sintered body
straight line
patches
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Hiroshi Ishizuka
博 石塚
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SHINGIJUTSU KAIHATSU KK
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Abstract

PROBLEM TO BE SOLVED: To provide a polishing patch constituted of a super-abrasive sintered body such as a sintered body for pad conditioning and capable of being cut from a circular sintered body material without waste.SOLUTION: The polishing patch is one in which two sheets of polishing patches are cut from a regular hexagon located at a circular center and six sheets of polishing patches cut from six sheets of congruent material pieces located at the outside of the regular hexagon in a circular super-abrasive sintered body material. Eight sheets of polishing patch materials in total are congruent, and patch corners are rounded in contour not to damage a material to be polished during polishing. The congruent patches may be further made into eight sheets of congruent patches of a plurality of pairs which are divided along lines forming concentric circles with circular arc shaped sides. This invention further includes a method for manufacturing the polishing patches and a polishing tool using the polishing patches.

Description

本発明は、超砥粒焼結体研磨部を持つ工具のための超砥粒焼結体およびその製造方法に関する。とくに本発明は、各種半導体材料の表面、ハードディスクのディスク面等を研磨する、主に硬質ウレタンや不織布で構成された化学的機械的研磨(chemical-mechanical polishing:CMPと略す)パッド用の、パッドコンディショニングに用いる研磨用超砥粒焼結体等の製造困難な焼結体の研磨パッチおよびその製造方法に関する。   The present invention relates to a superabrasive sintered body for a tool having a superabrasive sintered body polishing section and a method for manufacturing the same. In particular, the present invention provides a pad for a chemical-mechanical polishing (abbreviated as CMP) pad composed mainly of hard urethane or non-woven fabric for polishing the surface of various semiconductor materials, the disk surface of a hard disk, etc. The present invention relates to a polishing patch for a sintered body that is difficult to manufacture such as a polishing superabrasive sintered body used for conditioning, and a method for manufacturing the same.

近年、超LSIデバイスにおける配線の多層化が進むにつれて、層間絶縁膜やシリコン等金属膜ウェハの平坦化にCMPが用いられてきている。そしてCMPで用いられる研磨パッド(一般に硬質発泡ポリウレタン製)の高い平坦化およびウェハ研磨速度を維持するためには、該研磨パッドの表面を常時または間欠的にコンディショニングする必要がある。   In recent years, CMP has been used to planarize metal film wafers such as interlayer insulating films and silicon as the number of wiring layers in VLSI devices has increased. In order to maintain a high level of a polishing pad (generally made of rigid foamed polyurethane) used in CMP and a wafer polishing rate, it is necessary to condition the surface of the polishing pad constantly or intermittently.

電子産業で使用されるメモリーチップ、その他のLSIデバイスの製造工程には、シリコンウエハ表面や、多層構造における層間絶縁膜の超精密平坦化が不可欠であり、これは一般に、研磨剤を含むスラリーと研磨パッドを用いたシステムにより行われている。研磨パッドは一般に硬質発泡ポリウレタン製であるが、平坦性およびウエハ研磨速度を維持するためには、常時または完結的にパッドの表面をコンディショニングする必要があり、この目的のために、主として、ダイヤモンド砥粒を電着により基板に固着した工具、或いは、一般に超硬合金で裏打ちされている焼結ダイヤモンド層にピラミッド状突起の列を設けた工具(コンディショナー、ドレッサー)が知られている。   In the manufacturing process of memory chips and other LSI devices used in the electronics industry, it is indispensable to ultra-precision planarize silicon wafer surfaces and interlayer insulation films in multilayer structures. This is done by a system using a polishing pad. The polishing pad is generally made of rigid polyurethane foam, but in order to maintain flatness and wafer polishing rate, it is necessary to condition the surface of the pad at all times or completely, and for this purpose, diamond polishing is mainly used. A tool in which grains are fixed to a substrate by electrodeposition or a tool (conditioner or dresser) in which a row of pyramidal protrusions is provided on a sintered diamond layer generally lined with a cemented carbide is known.

金属めっき層で固着された個々の超砥粒粒子に代えて、ピラミッド状の突起の列を焼結ダイヤモンドで形成した工具、特に、半導体ウェハ等の表面を高精度かつ高能率で加工可能なCMPパッドのコンディショニングに好適なCMPパッドコンディショナーとして使用する研磨工具およびその製造方法が提供された(特許文献1)。この技術において研磨単位と称される突起群は、超硬合金で裏打ちされている焼結ダイヤモンド層に、ワイヤカットで切り込むことにより形成される。研磨単位の形状は面間角度が90°のピラミッド型(四角錐)や四角錐台、他にも三角錐や三角錐台等が記載されている。   Instead of individual superabrasive particles fixed with metal plating layer, a tool with pyramid-shaped projections formed of sintered diamond, especially CMP that can process the surface of semiconductor wafers with high accuracy and high efficiency A polishing tool used as a CMP pad conditioner suitable for pad conditioning and a manufacturing method thereof have been provided (Patent Document 1). In this technique, a group of protrusions called a polishing unit is formed by cutting a sintered diamond layer lined with a cemented carbide with a wire cut. As the shape of the polishing unit, a pyramid type (quadrangular pyramid) or a quadrangular pyramid with an angle between planes of 90 °, a triangular pyramid, a triangular frustum, or the like is described.

また、焼結ダイヤモンド層に、表面に対して一定レベル内に位置する平坦な頂面を持つ研磨単位を複数個配置した研磨工具であって、研磨単位は焼結ダイヤモンド層へワイヤカット等での切込みにより、先端が平面の、整列された四角や三角の角柱乃至角錐台上の切れ刃を形成する研磨工具が、本発明者により提供された(特許文献2)。   Also, a polishing tool in which a plurality of polishing units having a flat top surface located within a certain level with respect to the surface are arranged on the sintered diamond layer, and the polishing unit is formed by wire cutting or the like on the sintered diamond layer. An inventor has provided a polishing tool that forms a cutting edge on an aligned square or triangular prism or pyramid with a flat tip by cutting (Patent Document 2).

国際公開WO2007−023949号公報International Publication WO2007-023949 特開2011−20182号公報JP2011-20182A

しかしながら、特許文献1および2の超砥粒焼結体は、特に近年必要とされてきつつある、ICチップの配線幅が例えば35μmルール以下であるような、超高精細配線を有するIC用等の半導体材料表面を研磨するCMPパッド用のコンディショナー等に加工する素材として、加工が困難であり、材料としても貴重である。従って、焼結体素材を無駄なく工具として使用できるための、特定の研磨パッチとしての素材からの切り出し態様を確立することが望ましい。   However, the superabrasive sintered bodies of Patent Documents 1 and 2 are particularly required in recent years, such as for ICs having ultrahigh-definition wiring in which the wiring width of the IC chip is, for example, 35 μm or less. As a material to be processed into a conditioner for a CMP pad for polishing the surface of a semiconductor material, it is difficult to process and is valuable as a material. Therefore, it is desirable to establish a cut-out aspect from a material as a specific polishing patch so that the sintered body material can be used as a tool without waste.

本発明者は、上記の課題を解決すべく、検討を重ね、一般に円板状に形成される、ダイヤモンド等の超砥粒焼結体からなる研磨部を有する研磨用焼結体を、研磨用パッチとして高性能である研磨工具を構成でき、焼結体素材を最も無駄なく利用する研磨用パッチの形状寸法を見出し、本発明を完成するに至ったものである。   In order to solve the above-mentioned problems, the present inventor has repeatedly studied and generally uses a polishing sintered body having a polishing portion made of a superabrasive sintered body such as diamond, which is generally formed in a disk shape, for polishing. A high-performance polishing tool can be configured as a patch, and the shape and dimensions of a polishing patch that uses a sintered body material most efficiently are found, and the present invention has been completed.

すなわち本発明は、ダイヤモンド等の超砥粒焼結体からなる研磨部をもつ回転式研磨工具に用いるに好適な、円板状材料を最も効率的に利用できる、以下の超砥粒焼結体研磨パッチおよびその製法に関する。
なお、本発明において、「円板状」と記載されている場合の円は、数学的な厳密な意味の真円のみを指すのではなく、焼結体等の実際の物質においてほぼ円形であって中心が近似的に一点に定めうる程度のものをも包含する。
That is, the present invention provides the following superabrasive sintered body that can be most efficiently used as a disk-shaped material suitable for use in a rotary polishing tool having a polishing portion made of a superabrasive sintered body such as diamond. The present invention relates to an abrasive patch and a method for producing the same.
In the present invention, the circle in the case of “disc shape” does not refer only to a true circle in a strict mathematical sense, but is substantially circular in an actual substance such as a sintered body. In other words, the center of which can be approximately determined at one point is also included.

[1]円板状の焼結体素材(1)から切り出した研磨パッチであって、
該円板の輪郭円を中心角60°で六分割した扇型の1つから、中心側から前記輪郭円の半径の半分だけ隔たった点を通る辺を有する正三角形を取り除いた、扇台型形状の、円弧側の両端角部がなめらかに丸められた輪郭形状を有する前記研磨パッチ。
[2]上記[1]に記載の研磨パッチ2枚を、円弧に向かい合う辺で接合した形の輪郭形状を有する、研磨パッチ。
[3]円板状の焼結体素材(1)の中心を通る直線(2)と、前記直線に直交する半径(3)、(3’)を2等分した点(4)、(4’)を通り、前記直線(2)に平行な線と円板の中心を通り前記直線と60°の角度をなす2本の直線(6)、(7)との交点(8)、(9)、(10)、(11)を結ぶ前記直線に平行な線分(12)、(12’)を1辺とする正六角形と該直径(2)とで円板を分割して得られる4枚の分割片の、該正六角形の外側に位置する2つの部分を、前記2本の直径(6)、(7)でさらにそれぞれ3分割して得られる、6枚の合同な分割片(13)、(14)、(15)、(16)、(17)、(18)、および正六角形の3辺と直径とを辺とする2枚の台形状の分割片から、前記6枚の分割片とほぼ合同な2枚の焼結体分割片(19)、(20)を切り出すことによって得られる、8枚のほぼ合同な焼結体分割片の、円弧状の辺の両端部角を丸めたものからなる、8枚のほぼ合同な形状の研磨パッチ。
[4][3]に記載の8枚の合同な焼結体分割片を、さらに円板外形をなしていた円弧と同心円をなす円弧(23)で2つまたはそれ以上のパッチ片に分割し、円弧状の辺の両端部角を丸めて得られる、8枚のほぼ合同な研磨パッチの複数の組からなる、研磨パッチ。
[5][3]に記載の研磨パッチの組において、正六角形の内側の2枚の焼結体分割片(19)、(20)とそれらとそれぞれ正六角形の1辺で接している外側の焼結体分割片(13)、(14)とに代えて、それぞれ接している1辺で結合した輪郭を有する、瓢箪型のくびれを有する2枚のほぼ合同な切片(28)、(29)の組とした、1辺が円弧である台形様の4枚のほぼ合同な切片(14)、(15)、(17)、(18)の組とからなる、6枚の研磨パッチ。
[6]前記[1]〜[5]のいずれかに記載の研磨パッチを、円形基板の外周部分に、1種または複数種の研磨パッチが円周方向に均等に配置されるように設けた、研磨工具。
[7]円板状の焼結体素材(1)の中心を通る直線(2)と、前記直線に直交する半径(3)、(3’)を2等分した点(4)、(4’)を通り、前記直線に平行な線と円板の中心を通り前記直線と60°の角度をなす2本の直線(6)、(7)との交点(8)、(9)、(10)、(11)を結ぶ前記直線(2)に平行な線分(12)、(12’)を1辺とする正六角形と前記直線(2)とで円板を4枚に分割し、該正六角形の外側に位置する2つの部分を、前記2本の直線(6)、(7)でさらにそれぞれ3分割して得られる、6枚の合同な分割片(13)、(14)、(15)、(16)、(17)、(18)、および正六角形の3辺と直径とを辺とする2枚の台形状の分割片(19)、(20)から切り出すことによって、円板状の焼結体素材から8枚の焼結体分割片を得る、研磨パッチ製造方法。
[8]前記[7]に記載の方法において、正六角形の内側の2枚の焼結体分割片(19)、(20)と、それぞれ正六角形の1辺で接している、外側の焼結体分割片(13)、(14)との間は切断せずに、瓢箪型のくびれを有する2枚の合同な切片(28)、(29)として残す、1辺が円弧である台形様の4枚の合同な切片(14)、(15)、(17)、(18)の組と、瓢箪型の括れを有する2枚の合同な切片(28)、(29)とから切り出すことにより、円板状の焼結体素材から6枚の研磨パッチを製造する方法。
[9]前記[7]または[8]に記載の方法において、切り出した研磨パッチの角部を丸めて、研磨パッチを互いにほぼ合同とする工程をさらに含む、方法。
[1] A polishing patch cut out from a disk-shaped sintered material (1),
A fan-shaped unit in which an equilateral triangle having a side passing through a point separated from the center side by half the radius of the contour circle is removed from one of the sector shapes obtained by dividing the contour circle of the disk into six at a central angle of 60 °. The polishing patch having a contour shape in which both corners on the arc side are smoothly rounded.
[2] A polishing patch having a contour shape in which two polishing patches according to the above [1] are joined at sides facing an arc.
[3] Points (4), (4) obtained by dividing a straight line (2) passing through the center of the disk-shaped sintered material (1) and radii (3) and (3 ′) perpendicular to the straight line into two equal parts. '), And the intersections (8) and (9) ), (10), and (11) obtained by dividing the disc into a regular hexagon having one side of the line segments (12) and (12 ′) parallel to the straight line and the diameter (2) 4 Six concatenated pieces (13) obtained by further dividing the two portions of the divided pieces outside the regular hexagon into three parts by the two diameters (6) and (7), respectively. ), (14), (15), (16), (17), (18), and two trapezoidal divided pieces having three sides and a diameter of a regular hexagon as sides. Two pieces that are almost congruent with one piece 8 substantially composed of 8 pieces of substantially congruent sintered body divided pieces obtained by cutting out the divided pieces (19) and (20) and rounded corners of both ends of the arc-shaped side. Polished patch of the same shape.
[4] Eight congruent sintered body divided pieces according to [3] are further divided into two or more patch pieces by an arc (23) that is concentric with the arc that has formed the outer shape of the disk. A polishing patch comprising a plurality of sets of eight substantially congruent polishing patches, obtained by rounding the corners of both ends of an arc-shaped side.
[5] In the set of polishing patches according to [3], the two sintered body divided pieces (19) and (20) on the inside of the regular hexagon, and the outer side in contact with each of them on one side of the regular hexagon In place of the sintered body divided pieces (13) and (14), two substantially congruent sections (28) and (29) having a saddle-shaped constriction having a contour joined at one side in contact with each other. Six polishing patches comprising four substantially trapezoidal sections (14), (15), (17), and (18) in a trapezoidal shape, each side being an arc.
[6] The polishing patch according to any one of [1] to [5] is provided on the outer peripheral portion of the circular substrate so that one or more types of polishing patches are evenly arranged in the circumferential direction. , Polishing tools.
[7] Points (4), (4) obtained by dividing a straight line (2) passing through the center of the disk-shaped sintered material (1) and radii (3) and (3 ′) perpendicular to the straight line into two equal parts Crossing points (8), (9), (2) passing through the straight line parallel to the straight line and the two straight lines (6), (7) passing through the center of the disk and forming an angle of 60 ° with the straight line. 10), dividing the disc into four with a regular hexagon having one side of the line segment (12), (12 ′) parallel to the straight line (2) connecting (11) and the straight line (2), Six concatenated pieces (13), (14), obtained by further dividing the two portions located outside the regular hexagon into three parts by the two straight lines (6) and (7), respectively. By cutting out from (15), (16), (17), (18) and two trapezoidal split pieces (19), (20) having three sides and a diameter of a regular hexagon as sides, Plate-like sintering Obtaining eight sintered body split pieces from the material, the polishing patch production method.
[8] In the method according to [7], the outer sintered body is in contact with the two inner hexagonal sintered pieces (19) and (20) at one side of the regular hexagon. A trapezoidal shape in which one side is a circular arc is left as two concatenated sections (28), (29) having a saddle-shaped constriction without cutting between the body segment pieces (13), (14) By cutting out from a set of four conjoint sections (14), (15), (17), (18) and two conjoint sections (28), (29) having a saddle-shaped constriction, A method for producing six polishing patches from a disk-shaped sintered material.
[9] The method according to [7] or [8], further including a step of rounding corner portions of the cut polishing patches so that the polishing patches are substantially congruent with each other.

ダイヤモンド等の超砥粒焼結体は、焼結体素材が円板状であり、その円板から、回転式研磨工具用の焼結体研磨パッチを、最も有効に無駄なく切り出すために、該円板の任意の直径を決定し、該直径に直交する半径を2等分した点を通り、該直径に平行な線と円板の中心を通り該直径と60°の角度をなす2本の直径との交点を結ぶ該直径に平行な線分を1辺とする正六角形と該直径とで円板を4枚に分割し、該正六角形の外側に位置する2つの部分を、前記2本の直径でさらにそれぞれ3分割して得られる、6枚の合同な分割片、および正六角形の3辺と直径とを辺とする2枚の台形状の分割片から切り出した、前記6枚の分割片と合同な2枚の焼結体分割片を切り出すことによって得られる、8枚の合同な焼結体分割片を、さらに円板外形をなしていた円弧と同心円をなす円弧で2つに分割して得られる合同な8枚が2組となった、焼結体研磨パッチを得ることによって、本願発明の焼結体研磨パッチが得られる。
また、本願発明の別の態様においては、前記正六角形と該直径とで円板を4枚に分割することに代えて、該直径と、正六角形の該直径に平行でない4個の辺と、および円板の中心を通り該直径と60°の角度をなす2本の直径の正六角形の外側に位置する部分とで円板を分割することによって得られる、2枚の合同な1辺が円弧である瓢箪型のくびれを有する切片の組と、1辺が円弧である台形様の4枚の合同な切片の組とからなる素材が得られ、瓢箪型の切片は、さらにくびれの2つの頂点を結ぶ線に対称な外形となるように直線状の部分を加工することにより、合同な4枚の台形様切片と、その合同な台形様切片を、円弧状辺に向かい合う直線辺で接合した形の2枚の瓢箪型切片とを得る。
これらの態様の16枚または6枚の研磨パッチは、研磨効果を向上させるために、円弧側の角部分は丸く加工されて、研磨時に被研磨材に食い込むことが無いようにされていることが好ましい。
In the superabrasive sintered body such as diamond, the sintered body material is disk-shaped, and in order to cut the sintered body polishing patch for a rotary polishing tool from the disk most effectively without waste, Determine the arbitrary diameter of the disk, pass through a point that bisects the radius orthogonal to the diameter, pass through a line parallel to the diameter and the center of the disk, and form an angle of 60 ° with the diameter. A regular hexagon having a line parallel to the diameter connecting the intersection with the diameter as one side and the diameter is used to divide the disk into four pieces, and the two portions located outside the regular hexagon are The six divisions cut out from six congruent division pieces obtained by further dividing each of the two pieces into two and a trapezoidal division piece having three sides and a diameter of a regular hexagon as sides. Eight congruent sintered body divided pieces obtained by cutting out two conjoined sintered body divided pieces, and By obtaining a sintered body polishing patch in which two sets of eight congruent pieces obtained by dividing into two arcs that are concentric with the arc that was formed, the sintered body polishing patch of the present invention was obtained. It is done.
Further, in another aspect of the present invention, instead of dividing the disc into four pieces by the regular hexagon and the diameter, the diameter and four sides not parallel to the diameter of the regular hexagon, And two congruent one sides obtained by dividing the disc into two regular hexagons of two diameters that pass through the center of the disc and form an angle of 60 ° with the diameter of the disc. A material consisting of a set of sections with a saddle-shaped constriction and a trapezoid-like set of four pieces with a circular arc on one side is obtained, and the saddle-shaped section has two vertices of the constriction. By processing a linear part so that it has a symmetric outer shape with a line connecting the two, a congruent four trapezoidal pieces and a jointed trapezoidal piece with a straight side facing the arcuate side Are obtained.
In order to improve the polishing effect, the 16 or 6 polishing patches of these aspects are processed so that the corners on the arc side are rounded so that they do not bite into the workpiece during polishing. preferable.

本発明は、例えばレーザーカットして研磨単位を研磨面に多数形成した研磨パッチを得るための超砥粒焼結体を、最も無駄なく円板状の焼結体素材から切り出すことのできる、超砥粒焼結体研磨パッチであるので、製造が困難で高価な超砥粒焼結体を最も無駄なく使用して製造することが可能となる。
また、合同な形状の研磨パッチを、複数の円板状焼結体から得られるため、研磨パッチを接着して製作する研磨工具作成時において、寸法あわせ等する必要がなく、また、本発明の研磨パッチは、必要以上に細分化した大きさでないため、研磨工具作成時の研磨パッチ接着作業が不合理に煩雑化することを防ぐことができる。
請求項1に係る発明の研磨パッチは、輪郭の一部をなす円弧の半径の半分の幅となるように扇型から正三角形を取り除いた寸法を有しており、この寸法のものだけが、円板状の焼結体素材から、最も無駄なく研磨パッチを切り出すことのできる形状・寸法のものである。また、請求項2に係る発明の研磨パッチは、上記の円板状素材から最も無駄なく切り出せる研磨パッチを2個結合した輪郭を有し、円板状素材から単独の研磨パッチ2個とともに切り出すことによって、やはり最も無駄なく切り出すことができる。
The present invention is, for example, a superabrasive sintered body for obtaining a polishing patch in which a large number of polishing units are formed on the polishing surface by laser cutting, and can be cut out from a disk-shaped sintered body material without waste. Since it is an abrasive-sintered body polishing patch, it is possible to manufacture by using the super-abrasive sintered body that is difficult and expensive to use without waste.
Further, since the congruent shape of the polishing patch can be obtained from a plurality of disc-shaped sintered bodies, it is not necessary to adjust the size when creating a polishing tool for bonding and manufacturing the polishing patch. Since the size of the polishing patch is not more finely divided than necessary, it is possible to prevent the polishing patch adhering work when creating the polishing tool from becoming unreasonably complicated.
The polishing patch of the invention according to claim 1 has a dimension obtained by removing an equilateral triangle from a fan shape so as to be a half width of a radius of an arc that forms a part of a contour, and only a thing of this dimension is It is of a shape and size that can cut a polishing patch from a disk-shaped sintered material with the least waste. The polishing patch of the invention according to claim 2 has a contour in which two polishing patches that can be cut out most efficiently from the disk-shaped material are combined, and is cut out from the disk-shaped material together with two single polishing patches. It is possible to cut out without any waste.

本発明の研磨用焼結体は、結合材の溶融温度以上で焼結されていることにより、超砥粒の固着強度が大きく、実質上脱落がないという利点がある。とくに超砥粒としてダイヤモンド粒子を用いた場合、ダイヤモンドは、製造工程において結合材金属が溶融しかつダイヤモンドが熱力学的に安定な温度圧力条件下に供されており、ダイヤモンド微粒子が結合材金属への部分溶解を介して強力に一体化されていることにより、固着強度がさらに大きいため、実質上脱落がなくなる。   The sintered body for polishing according to the present invention is advantageous in that it is sintered at a temperature equal to or higher than the melting temperature of the binder, so that the fixing strength of the superabrasive grains is large and there is substantially no dropout. Particularly when diamond particles are used as superabrasive grains, diamond is subjected to temperature and pressure conditions in which the binder metal is melted and the diamond is thermodynamically stable in the manufacturing process, and the diamond fine particles become the binder metal. Because of the strong integration through partial dissolution, the fixing strength is further increased, so that there is virtually no dropout.

さらに研磨単位が形成されている研磨部は、表面が充分な厚さを持つ超砥粒焼結体で構成されていることにより、研磨単位が使用により磨滅しても、研磨単位を容易に再生して、本発明の工具として再利用できる。   In addition, the polishing part in which the polishing unit is formed is composed of a superabrasive sintered body with a sufficient thickness on the surface, so that even if the polishing unit is worn out by use, the polishing unit can be easily regenerated. Thus, it can be reused as the tool of the present invention.

本発明による8枚研磨パッチ切り出しを説明する図である。It is a figure explaining 8 sheet | seat patch cutting out by this invention. 本発明による8枚研磨パッチ切り出しを示す図である。It is a figure which shows 8 sheet | seat patch cutout by this invention. 本発明の別の態様による16枚研磨パッチ切り出しを示す図である。It is a figure which shows 16-sheet polishing patch cut-out by another aspect of this invention. 本発明のさらに別の態様による6枚研磨パッチ切り出しを示す図である。It is a figure which shows 6 sheet | seat grinding | polishing patch cut-out by another aspect of this invention. 本発明による研磨パッチを用いた研磨用工具を示す図である。It is a figure which shows the polishing tool using the polishing patch by this invention. 本発明の別の態様による研磨パッチを用いた研磨工具を示す平面図および側面図である。It is the top view and side view which show the polishing tool using the polishing patch by another aspect of this invention. 本発明のさらに別の態様による2種の研磨パッチを用いた研磨工具を示す平面図および側面図である。It is the top view and side view which show the polishing tool using 2 types of polishing patches by another aspect of this invention. 本発明による研磨パッチの研磨面として代表的な、レーザーカットした研磨単位の平面図である。1 is a plan view of a laser-cut polishing unit that is representative of a polishing surface of a polishing patch according to the present invention. 本発明による研磨パッチの研磨面として代表的な、レーザーカットした研磨単位の実施例の写真である。It is a photograph of the Example of the laser-cut grinding | polishing unit typical as a grinding | polishing surface of the grinding | polishing patch by this invention. 本発明による研磨パッチの研磨面として代表的な、各種研磨単位の構造を示す図である。It is a figure which shows the structure of various grinding | polishing units typical as a grinding | polishing surface of the grinding | polishing patch by this invention. 本発明による研磨パッチの研磨面として代表的な、研磨単位の形成方法を示す図である。It is a figure which shows the formation method of a polishing unit typical as a polishing surface of the polishing patch by this invention.

本発明の研磨パッチの研磨用焼結体の材料となる超砥粒焼結体は、ダイヤモンドやc−BN(立方晶窒化硼素)等の超砥粒の粉末を常法により超高圧高温工程で処理して得られるものが好ましい。この状態の焼結体は超砥粒焼結体は歪みが大きいので型放電加工などにより予備的にあらかた平坦化しておく。次いで、溝及び突起側面を段階的に形成していくことにより、研磨単位、即ち、直接研磨対象と接触する突起部分を創生する。図8に研磨単位の列の平面図を示す。なお超砥粒焼結体として市販品を利用する場合は、仕様によるが、表面が平坦化されているので、上記平坦化予備処理は省略できる。
前記溝の形成には、レーザーカット、とくに青色レーザー、例えばYAGレーザーを用いて、短いピッチで研磨単位を形成し、研磨単位の研磨作用をおこなうエッジが比較的鋭利な状態を保って加工することができる。
The superabrasive sintered body used as a material for the polishing sintered body of the polishing patch of the present invention is obtained by subjecting superabrasive powder such as diamond or c-BN (cubic boron nitride) to a high pressure and high temperature process by a conventional method. What is obtained by processing is preferred. Since the sintered body in this state has a large strain in the superabrasive sintered body, it is preliminarily flattened by die discharge machining or the like. Next, the grooves and the side surfaces of the protrusions are formed stepwise to create a polishing unit, that is, a protrusion portion that directly contacts the object to be polished. FIG. 8 shows a plan view of a row of polishing units. When a commercially available product is used as the superabrasive sintered body, although depending on the specifications, since the surface is flattened, the flattening pretreatment can be omitted.
For the formation of the groove, a laser cut, in particular, a blue laser, for example, a YAG laser, is used to form a polishing unit at a short pitch and to process the polishing unit with a sharp edge. Can do.

本発明の研磨パッチの研磨用焼結体において、上記研磨単位は、円形焼結体層へ、レーザー加工機で切り込むことにより、創生することができる。レーザー加工機は、スキャン動作により所望の形状での焼結体層への切り込み加工を、焼結体層へのダメージを与えずにおこなうことが可能であるため、エッジの鈍りの少ない任意の形状の研磨単位が形成可能である。レーザー加工動作の能率等を考慮すると、直線状にスキャンすることが好ましい。   In the sintered body for polishing a polishing patch of the present invention, the polishing unit can be created by cutting the circular sintered body layer with a laser processing machine. The laser processing machine can perform cutting into the sintered body layer in the desired shape by scanning operation without damaging the sintered body layer, so any shape with less edge dullness can be obtained. Can be formed. Taking the efficiency of the laser processing operation into consideration, it is preferable to scan linearly.

研磨単位が頂部に直線状の稜線を呈する形状(図10;No.1 三角錐台、No.3 六角錐台、 No.4 四角錐台)や、稜線が湾曲しているもの(図10 ; No.2)などであってもよい。研磨単位は、レーザー加工機により形成されるので、ワイヤカット放電加工に比べて、格段に細かい密度で形成でき、研磨単位の形状も、ワイヤカット放電加工に比較して、エッジの鋭い状態がたもたれるものである。   A shape in which the polishing unit has a linear ridge line at the top (FIG. 10; No. 1 triangular frustum, No. 3 hexagonal frustum, No. 4 quadrangular frustum) or a curved ridge line (FIG. 10; No. 2) may be used. Since the polishing unit is formed by a laser processing machine, it can be formed with a much finer density compared to wire-cut electric discharge machining, and the shape of the polishing unit is also sharper than that of wire-cut electric discharge machining. It is leaning.

上記例において、各研磨単位が有効な研磨部分として機能するために、各研磨単位の頂部エッジは充分に鋭く、かつ隣接研磨単位同士は、200μm以下という従来なかった短い間隔で隔てられる。エッジの長さは、各研磨単位頂部が多角形であり、一辺の長さが30μm以上という長さを有している。また、研磨単位の側壁面は、研磨単位頂面に垂直な研磨工具回転軸方向に対して0°〜30°、好ましくは0°〜15°の角度を有している。   In the above example, since each polishing unit functions as an effective polishing portion, the top edge of each polishing unit is sufficiently sharp, and adjacent polishing units are separated from each other by an unprecedented short interval of 200 μm or less. As for the length of the edge, each polishing unit top has a polygonal shape, and the length of one side is 30 μm or more. The side wall surface of the polishing unit has an angle of 0 ° to 30 °, preferably 0 ° to 15 °, with respect to the direction of the rotation axis of the polishing tool perpendicular to the top surface of the polishing unit.

溝の深さ(研磨単位の溝底からの高さ)は、50μm以下で、切屑を排除できる程度の深さがあれば良い。溝が深すぎると、研磨単位の強度が不足する上、過剰な超砥粒層の厚さが必要となるが、レーザー加工においては、精密な加工が可能であり、ピッチを短くすることが出来るため、溝の深さも従来に比べて浅いものが実現できる。   The depth of the groove (height from the groove bottom of the polishing unit) should be 50 μm or less, and it should be deep enough to eliminate chips. If the groove is too deep, the strength of the polishing unit will be insufficient and an excessive superabrasive layer thickness will be required, but in laser processing, precise processing is possible and the pitch can be shortened. Therefore, it is possible to realize a groove having a shallower depth than the conventional one.

研磨単位の形状としては、研磨単位の各側面を傾斜させて錐台状、例えば、四角錐台状または三角錐台状とすることが好ましい。
また、整列した角柱状や角柱台状研磨単位において、長方形や三角形のひとつまたは複数方向の側面を専用の工具で研磨することにより、頂部の縁又は頂点を鋭利化する、いわゆる「刃付け」を行なうと、さらに良好な切れ味が達成できる。研磨単位が、多角形柱、多角形錐台であり、頂部が多角形(典型的には、三角形または四角形)の場合、頂部の面の少なくとも一辺に刃付けを行なうが、研磨単位が四角錐状または三角錐状の場合は、刃付けを行なわなくても十分な切れ味を達成することができる。
As the shape of the polishing unit, it is preferable that each side surface of the polishing unit is inclined to form a frustum shape, for example, a quadrangular frustum shape or a triangular frustum shape.
In addition, in the aligned prismatic or prismatic polishing units, so-called "blading" that sharpens the edge or vertex of the top by polishing one or more sides of a rectangle or triangle with a dedicated tool. If done, a better sharpness can be achieved. When the polishing unit is a polygonal column or a polygonal frustum, and the top is a polygon (typically a triangle or a quadrangle), cutting is performed on at least one side of the top surface, but the polishing unit is a quadrangular pyramid. In the case of a shape or a triangular pyramid shape, a sufficient sharpness can be achieved without cutting.

焼結超砥粒層としては、ダイヤモンド焼結体(PCD)やc-BN焼結体(PcBN)の一方の面を超硬合金即ち炭化タングステン系複合材、或は周期律表第6a族金属の炭化物を主成分とする複合材のブロックで裏打ちされた構造のものを用い、複合材側を接着剤等によって工具基板に固着し、反対側に区分溝を形成して研磨部として使用する。   As a sintered superabrasive layer, one surface of a diamond sintered body (PCD) or c-BN sintered body (PcBN) is cemented with a cemented carbide, that is, a tungsten carbide based composite material, or a group 6a metal of the periodic table. The composite material is composed of a composite material block consisting mainly of carbides, and the composite material side is fixed to the tool substrate with an adhesive or the like, and a division groove is formed on the opposite side to be used as a polishing portion.

このような焼結体は、典型的には一軸加圧型の高温超高圧静水圧プレスで調製された円板状のものが市販されている。   As such a sintered body, a disk-shaped one typically prepared by a uniaxial pressurization type high temperature ultrahigh pressure isostatic press is commercially available.

四角錐台状研磨単位の作製においては、例えば図11に示すように、研磨部の表面にレーザー加工機で一定溝間隔(ピッチ)で第一の方向の平行溝群および錐台状体両側面を形成した後、研磨部を固着した基板ごと円環中心軸の周囲に90°回転し、同じようにして第二の方向の平行溝群を一定溝間隔で、また各溝に隣接する錐台体傾斜側面を形成することにより、直交する2組の平行溝群、および溝に沿って整列した四角錐台状研磨単位を得るようにしてもよい。   In the production of the quadrangular frustum-shaped polishing unit, for example, as shown in FIG. 11, the parallel groove group and the frustum-shaped body on both sides of the first direction at a fixed groove interval (pitch) on the surface of the polishing portion with a laser processing machine. Then, the substrate to which the polishing part is fixed is rotated by 90 ° around the central axis of the ring, and in the same way, parallel groove groups in the second direction are formed at a constant groove interval, and the frustum adjacent to each groove. By forming the body inclined side surfaces, two sets of parallel groove groups orthogonal to each other and a truncated pyramid shaped polishing unit aligned along the grooves may be obtained.

三角錐体の場合においても、第一の方向の平行溝群および溝に隣接する角錐台の傾斜面を形成後、焼結体素材を中心軸の周囲に120°回転し、同様に一定溝間隔で第二の方向の平行溝群、および隣接する傾斜側面の形成をレーザーカットにより行う。操作完了後、研磨部をさらに120°回転し同じ操作を行うことによって、120°で交差する第三方向の平行溝群、および隣接する傾斜側面、溝に沿って整列した三角錐台状研磨単位を得るようにしてもよい。   Even in the case of a triangular pyramid, after forming the parallel groove group in the first direction and the inclined surface of the truncated pyramid adjacent to the groove, the sintered body material is rotated by 120 ° around the central axis, and the constant groove spacing is similarly applied. Then, the parallel groove groups in the second direction and the adjacent inclined side surfaces are formed by laser cutting. After the operation is completed, the polishing unit is further rotated by 120 °, and the same operation is performed, so that parallel groove groups in the third direction intersecting at 120 ° and the adjacent inclined side surfaces and the triangular frustum-shaped polishing units aligned along the grooves. May be obtained.

上記研磨単位において、錐台状体頂部の溝底面に対する突き出し高さは三角形、四角形共に50μm以下とすることができる。レーザーカットであるからこその微細加工により、研磨単位の整列ピッチが200μm以下であるため、従来よりも突き出しが浅くても、研磨部本体がパッド等のワークと直接接触することがなく、研磨単位の強度が不足したり、過剰な超砥粒層の厚さが必要となることがない。
さらにレーザーカットであるため、エッジの鈍りが少なく、本発明のような小さな突き出し高さでも、十分な研磨作用が得られる。
In the above polishing unit, the protruding height of the top of the frustum-like body with respect to the groove bottom can be 50 μm or less for both the triangle and the quadrangle. Due to the fine processing because of laser cutting, the alignment pitch of the polishing unit is 200 μm or less, so even if the protrusion is shallower than before, the polishing unit body does not come in direct contact with the work such as the pad, and the polishing unit In this case, there is no need for insufficient strength or excessive superabrasive layer thickness.
Furthermore, since it is a laser cut, there is little blunting of the edge, and a sufficient polishing action can be obtained even with a small protruding height as in the present invention.

上記研磨単位の研磨性能は、錐(台)状体の頂部に含有される超砥粒の粒度に依存する。超砥粒がダイヤモンド粒子である場合、即ち研磨部を構成する焼結体が焼結ダイヤモンド(PCD)層である場合、ダイヤモンド粒子の粒度(公称粒度)としては、40-60μm以下、8-16μmや0-2μmなどの各粒度のPCD層が利用できるが、8-16μm以下の公称粒度が好ましく、特に0-2μmが好ましい。   The polishing performance of the polishing unit depends on the particle size of the superabrasive grains contained at the top of the cone-shaped body. When the superabrasive grains are diamond particles, that is, when the sintered body constituting the polished portion is a sintered diamond (PCD) layer, the diamond particle size (nominal particle size) is 40-60 μm or less, 8-16 μm PCD layers of various particle sizes such as 0-2 μm can be used, but nominal particle sizes of 8-16 μm or less are preferred, with 0-2 μm being particularly preferred.

本発明の研磨パッチの研磨用焼結体に用い得るダイヤモンド焼結体は、ダイヤモンド粒子を、裏打ち材としての超硬合金および、必要に応じてコバルト等の結合材金属と共に、ダイヤモンドが熱力学的に安定な超高圧高温条件下に供して得られる。焼結体から本発明のパッドコンディショニング用超砥粒焼結体への加工はレーザーカット、典型的には青色レーザーカットによる表面の加工による研磨単位の形成によって実現できる。
焼結体素材から、研磨用焼結体を切り出すための輪郭カットにおいては、レーザーカットの他、ワイヤカット放電加工等の、一般的加工手段が利用可能である。
The diamond sintered body that can be used for the polishing sintered body of the polishing patch of the present invention is composed of diamond particles together with a cemented carbide as a backing material and, if necessary, a binder metal such as cobalt, and the diamond is thermodynamic. It is obtained by subjecting to ultra-high pressure and high temperature conditions that are stable to high temperatures. Processing from the sintered body to the super-abrasive sintered body for pad conditioning of the present invention can be realized by forming a polishing unit by processing the surface by laser cutting, typically blue laser cutting.
In contour cutting for cutting out a sintered sintered body from a sintered body material, general processing means such as wire cut electric discharge machining can be used in addition to laser cutting.

本発明の研磨パッチに用いうる研磨用焼結体においては、研磨単位の三角錐台または四角錐台等の多角形錐台体は、レーザーカットにより形成されるため、エッジが鋭くなり、また、エッジの綿密度も高いものであるため、特に0.35μm以下の超精細配線ルールのLSI用の半導体材料表面の研磨に用いるCMPパッドの効果的なコンディショニングが初めて可能となり、コンディショニングに際しての、CMPパッドの無用な摩滅も少なく抑えることが出来る。
また、ピッチの短い研磨単位列であるため、研磨作用をなすエッジの綿密度が高くなり、必要な超砥粒焼結体材料も、従来の長いピッチのものと比較して少なくて済む。
また、研磨単位の高さを従来のように高くする必要がなく、必要とされる超砥粒焼結体部分の厚みは従来よりも少なくて済む。
In the polishing sintered body that can be used for the polishing patch of the present invention, a polygonal frustum such as a triangular frustum or a quadrangular frustum of a polishing unit is formed by laser cutting, so that the edge becomes sharp, Since the cotton density of the edge is also high, it is possible for the first time to effectively condition a CMP pad used for polishing the surface of a semiconductor material for an LSI with an ultrafine wiring rule of 0.35 μm or less for the first time. Can reduce unnecessary wear.
In addition, since the polishing unit row has a short pitch, the cotton density of the edge that performs the polishing action is increased, and the necessary superabrasive sintered body material is less than that of the conventional long pitch.
Further, it is not necessary to increase the height of the polishing unit as in the prior art, and the required thickness of the superabrasive sintered body portion is smaller than in the prior art.

図1および2を参照して、本発明の1態様を説明する。
円板状の焼結体素材(1)の任意の円板の中心を通る直線(2)を決定し、該直線に直交する半径(3)を2等分した点(4)を通り、該直径に平行な線と円板の中心を通り該直径と60°の角度をなす2本の直線(6)、(7)との交点(8)、(9)、(10)、(11)を結ぶ前記直線(2)に平行な線分(12)を1辺とする正六角形と前記直線(2)とで円板を4枚に分割し、該正六角形の外側に位置する2つの部分(13)、(14)を、前記2本の直線(6)、(7)でさらにそれぞれ3分割して得られる、6枚の合同な分割片(15)、(16)、(17)、(18)、(19)、(20)および正六角形の3辺と前記直線(2)とを辺とする2枚の台形状の分割片から切り出した、前記6枚の分割片と合同な2枚の焼結体分割片(21)、(22)を切り出すことによって、8枚の合同な焼結体分割片(15)、(16)、(17)、(18)、(19)、(20)、(21)、(22)が得られる。
One embodiment of the present invention will be described with reference to FIGS.
A straight line (2) passing through the center of an arbitrary disk of the disk-shaped sintered body material (1) is determined, and the radius (3) perpendicular to the straight line is divided into two equal parts (4), Intersections (8), (9), (10), (11) with two straight lines (6), (7) passing through the center of the disk parallel to the diameter and forming an angle of 60 ° with the diameter The disc is divided into four parts by a regular hexagon with one side of a line segment (12) parallel to the straight line (2) connecting the two and the straight line (2), and two parts located outside the regular hexagon (13) and (14) are further divided into three by the two straight lines (6) and (7), respectively, and six concatenated pieces (15), (16), (17), (18), (19), (20) and 2 congruent with the six divided pieces cut out from two trapezoidal divided pieces having three sides of the regular hexagon and the straight line (2) as sides. Single sintered body By cutting out the split pieces (21) and (22), eight congruent sintered body split pieces (15), (16), (17), (18), (19), (20), (21 ) And (22) are obtained.

このようにして、合同なパッチを、ひとつの円板状素材から最も無駄なく切り出すことができるが、このようにして切り出した合同なパッチの輪郭は、円板状素材の輪郭円を中心角60°で六分割した扇型の1つから、中心側から前記輪郭円の半径の半分だけ隔たった点を通る辺を有する正三角形を取り除いた、扇台型形状である。取り除く正三角形の大きさは、正確に輪郭円の半径の半分だけ隔たった点を通る辺を有するものであり、これより大きくても小さくても、切り出しに際し無駄な部分が発生する。   In this way, the congruent patch can be cut out most efficiently from one disc-shaped material, but the contour of the congruent patch cut out in this way is centered on the contour circle of the disc-shaped material. A fan-shaped shape obtained by removing an equilateral triangle having a side passing through a point separated from the center side by a half of the radius of the contour circle from one of the fan-shaped sections divided into six. The size of the regular triangle to be removed has a side that passes through a point separated by exactly half the radius of the contour circle, and even if it is larger or smaller than this, a wasteful part is generated in the cutting.

また、図3には、図1のものを、さらに円板外形をなしていた円弧と同心円をなす円弧(23)で2つに分割して得られる、2組の合同な8枚からなる、16枚の焼結体研磨パッチを示し、もととなる図1のものが最も無駄なく切り出す輪郭形状・寸法であるのだから、やはり最も無駄のない輪郭・形状である。   Also, FIG. 3 includes two sets of eight congruent pieces obtained by dividing the one in FIG. 1 into two by an arc (23) that is concentric with the arc that had formed the outer shape of the disk. Since 16 sintered compact polishing patches are shown, and the original one in FIG. 1 has the most contour shape / dimension cut out without waste, it is still the least waste contour / shape.

さらに、図4に示す本願発明の別の態様においては、図1のものにおいて、正六角形の内側の2枚の焼結体分割片(21)、(22)を、それぞれ正六角形の1辺で接している、外側の焼結体分割片と結合した、瓢箪型のくびれを有する2枚の合同な切片(28)、(29)の組と、1辺が円弧である台形様の4枚の合同な切片(30)(31)(32)(33)の組とからなる、6枚の研磨パッチを示す。   Furthermore, in another aspect of the present invention shown in FIG. 4, in FIG. 1, the two sintered body divided pieces (21) and (22) inside the regular hexagon are each connected to one side of the regular hexagon. A set of two congruent sections (28) and (29) having a saddle-shaped constriction combined with an outer sintered body divided piece in contact with each other, and four trapezoid-like pieces each having an arc on one side 6 shows six polishing patches comprising a set of congruent sections (30) (31) (32) (33).

上記瓢箪型の括れを有する切片は、円板状素材から最も無駄なく切り出すことができる、上記の8枚の合同なパッチのうちの2枚を接合した形状であり、この瓢箪型の長軸方向長さは、正確に円板状素材の半径に一致するものである。
これらの態様の、8枚、16枚または6枚の研磨パッチは、研磨効果を向上させるために、円弧側の角部分は丸く加工されており、研磨時に被研磨材に食い込むことが無いようにされていることが好ましい。
The section having the saddle-shaped constriction is a shape obtained by joining two of the above-mentioned eight congruent patches that can be cut out most efficiently from a disk-shaped material. The length exactly matches the radius of the disk-shaped material.
In these aspects, the 8, 16, or 6 polishing patches are rounded at the corners on the arc side in order to improve the polishing effect, so that they do not bite into the workpiece during polishing. It is preferable that

図5は、本発明による研磨パッチを用いた研磨工具の一態様を示す。
この例においては、研磨パッチは図1のものを大小2個づつ使用している。
FIG. 5 shows an embodiment of a polishing tool using the polishing patch according to the present invention.
In this example, two polishing patches of the size shown in FIG. 1 are used.

図6は、本発明による研磨パッチを用いた研磨工具の別の態様を示す。この態様においては、図2に示す研磨パッチのうち、台形様切片のみを使用した、研磨工具を示す。   FIG. 6 shows another embodiment of an abrasive tool using an abrasive patch according to the present invention. In this embodiment, a polishing tool using only a trapezoidal section of the polishing patch shown in FIG. 2 is shown.

図7は、本発明による研磨パッチを用いた研磨工具のさらに別の態様を示す。この態様においては、図2に示す瓢箪型切片と台形様切片との両方を使用する。   FIG. 7 shows still another embodiment of an abrasive tool using an abrasive patch according to the present invention. In this embodiment, both the saddle-shaped section and the trapezoidal section shown in FIG. 2 are used.

図6のものおよび図7のものは、合同の研磨パッチを円形基板の周縁部に複数設けているが、一枚の研磨パッチは比較的大面積であり、上記した研磨単位が緻密に設けられた研磨パッチの場合、比較的少数の研磨パッチを円形基板に貼付するだけで、十分な研磨効果を奏する研磨工具が得られる。
また、研磨パッチが間隔をあけて周縁部に配置されるため、パッチの無い部分を均等に設けることができ、研磨屑の排出が有効に行われるという効果もある。
次に、本発明の実施例による工具の具体例を説明する。
6 and 7 are provided with a plurality of congruent polishing patches on the peripheral edge of the circular substrate, but one polishing patch has a relatively large area, and the above-mentioned polishing units are densely provided. In the case of a polishing patch, a polishing tool that exhibits a sufficient polishing effect can be obtained by simply attaching a relatively small number of polishing patches to a circular substrate.
In addition, since the polishing patches are arranged at the peripheral edge with a space therebetween, it is possible to uniformly provide the portions without the patches, and there is an effect that the polishing dust is effectively discharged.
Next, a specific example of the tool according to the embodiment of the present invention will be described.

[実施例1]
厚さ0.5mm、直径60mmの焼結ダイヤモンド層を超硬合金ブロックと一体化した、全体厚さ3.2mmの円板状ダイヤモンド焼結体をワイヤカットによって図3のように切断し、同一形状の円弧状パッチを大小2種類、各8個切り出した。より大なる円弧は8個について長さ約27mm、より小なる円弧は長さ約21mm、円弧中央における幅は、16個について同様の約7mmであった。
これらの円弧状焼結体片を大小それぞれについて5個づつ取り、平らな金属板上に向きを揃えて固定し、各ダイヤモンド層表面に青色レーザーで切込みにより、底部に対する高さ50μmの四角錐台状研磨単位群を130μmピッチの格子状に形成して研磨パッチとした。格研磨単位頂部は一辺30μmの正方形状、側壁面は軸方向に対して15°の契斜をつけた。
[Example 1]
A disc-shaped diamond sintered body having a total thickness of 3.2 mm, in which a sintered diamond layer having a thickness of 0.5 mm and a diameter of 60 mm is integrated with a cemented carbide block, is cut by wire cutting as shown in FIG. Eight arc-shaped patches of shape, each of two types, large and small, were cut out. The larger arcs had a length of about 27 mm for 8 pieces, the smaller arcs had a length of about 21 mm, and the width at the center of the arc was about 7 mm, the same for 16 pieces.
Take 5 pieces of each of these arc-shaped sintered compacts, large and small, and fix them on a flat metal plate with their orientations aligned, and cut each diamond layer surface with a blue laser to make a square pyramid with a height of 50 μm from the bottom. A group of polishing units was formed in a lattice pattern with a pitch of 130 μm to form a polishing patch. The top of the polishing unit was a square shape with a side of 30 μm, and the side wall surface was inclined by 15 ° with respect to the axial direction.

これらの研磨パッチを外径108mmの円形基板の外周に部分に、5個ずつ交互にそれぞれ72°ごとに各々の同心円上に配置した。各パッチは中心において長手方向をを円周方向に対して30°傾斜させてそれぞれ配置し、接着剤で固定した。
この工具を不織布および硬質ウレタン(共にCeiba Technologies製)の研磨試験に供して表1の結果を得た。
この値は、例えば特許文献5に開示される、ワイヤカットにより研磨単位を形成した従来技術のダイヤモンド焼結体研磨工具、これは研磨単位の頂面四角形の辺の長さが100μmでピッチが1500μmのものと頂面四角形の辺200μmでピッチが2000μmのもの、と比較すると、カットレートは従来技術の80〜120μm/hと比べて百倍以上も低く、すなわち、コンディショニングされる硬質ウレタンの減りが少なく、それでいて表面粗さは従来技術のダイヤモンド焼結体研磨工具と同等または優れている、ということを意味している。
Five of these polishing patches were alternately arranged on the outer periphery of a circular substrate having an outer diameter of 108 mm on each concentric circle every 72 °. Each patch was arranged with its longitudinal direction inclined at 30 ° with respect to the circumferential direction at the center, and fixed with an adhesive.
This tool was subjected to a polishing test of nonwoven fabric and hard urethane (both manufactured by Ciba Technologies), and the results shown in Table 1 were obtained.
This value is disclosed in, for example, Patent Document 5, a conventional diamond sintered body polishing tool in which a polishing unit is formed by wire cutting, which is 100 μm in length of the side of the top quadrangular surface of the polishing unit and 1500 μm in pitch. The cut rate is more than 100 times lower than that of the conventional technology of 80 to 120 μm / h, that is, the reduction of the hard urethane to be conditioned is small. However, it means that the surface roughness is equivalent or superior to that of the prior art diamond sintered body polishing tool.

本発明の研磨パッチは、上記実施例のような優れた工具を得ることの出来る、細かいピッチで研磨単位を形成した超砥粒研磨工具用の研磨パッチとして、特に有用である。なぜならば、細かいピッチの研磨単位を有した超砥粒焼結体は、レーザーカットという手間のかかる工程を経て作成されるものであるため、貴重であり、無駄のない使用がとりわけ重要だからである。   The polishing patch of the present invention is particularly useful as a polishing patch for a superabrasive polishing tool in which polishing units are formed at a fine pitch, which can provide an excellent tool as in the above embodiment. This is because a superabrasive sintered body having a fine-pitch polishing unit is produced through a time-consuming process called laser cutting, and is therefore valuable and particularly useless. .

本発明の超砥粒焼結体研磨は、超砥粒焼結体素材の無駄が無いように研磨パッチを切り出すことができるので、例えばCMPパッドコンディショナーとして、特に高精細回路ルールで製造されるLSI用の半導体材料表面の研磨に用いるためのCMPパッドのコンディショナーとして極めて優秀な研磨パッチに関して適用すれば、極めて有益である。   In the polishing of the superabrasive sintered body of the present invention, the polishing patch can be cut out so that there is no waste of the superabrasive sintered body material. Therefore, for example, as a CMP pad conditioner, an LSI manufactured with a high-definition circuit rule. It is extremely beneficial if applied with respect to an extremely excellent polishing patch as a conditioner for a CMP pad for use in polishing a semiconductor material surface.

1:円板状超砥粒焼結体
2:直径
3:直径に直角な半径
4:半径の中点
6:直径2に60°で交わる直径
7:直径2に60°で交わるもう1つの直径
8、9、10、11:半径の中点4を通り直径2に平行な線と直径2に60°で交わる直径との交点
13、14、15、16、17、18、19、20:8枚の合同な研磨パッチ
28、29:繭型研磨パッチ
図8の1:研磨パッチ表面
図8の2:四角錐台状の研磨単位の頂面
図8の3:研磨単位の間の溝
1: Disk-shaped superabrasive sintered body 2: Diameter 3: Radius perpendicular to diameter 4: Radius midpoint 6: Diameter 2 intersects at 60 ° Diameter 7: Another diameter intersects with diameter 2 at 60 ° 8, 9, 10, 11: Intersection points 13, 14, 15, 16, 17, 18, 19, 20: 8 of the line passing through the midpoint 4 of the radius and parallel to the diameter 2 and the diameter intersecting the diameter 2 at 60 ° Sheets of congruent polishing patches 28, 29: vertical polishing patch FIG. 8 1: polishing patch surface FIG. 8 2: top of a truncated pyramid shaped polishing unit FIG. 8 3: groove between polishing units

Claims (9)

円板状の焼結体素材(1)から切り出した研磨パッチであって、
該円板の輪郭円を中心角60°で六分割した扇型の1つから、中心側から前記輪郭円の半径の半分だけ隔たった点を通る辺を有する正三角形を取り除いた、扇台型形状の、円弧側の両端角部がなめらかに丸められた輪郭形状を有する前記研磨パッチ。
A polishing patch cut out from a disk-shaped sintered material (1),
A fan-shaped unit in which an equilateral triangle having a side passing through a point separated from the center side by half the radius of the contour circle is removed from one of the sector shapes obtained by dividing the contour circle of the disk into six at a central angle of 60 °. The polishing patch having a contour shape in which both corners on the arc side are smoothly rounded.
円板状の焼結体素材(1)から切り出した研磨パッチであって、請求項1に記載の研磨パッチ2枚を、円弧に向かい合う辺で接合した形の輪郭形状を有する、研磨パッチ。   A polishing patch cut out from a disk-shaped sintered material (1), wherein the polishing patch has a contour shape in which two polishing patches according to claim 1 are joined at sides facing an arc. 円板状の焼結体素材(1)の中心を通る直線(2)と、前記直線に直交する半径(3)を2等分した点(4)を通り、前記直線(2)に平行な線と円板の中心を通り前記直線と60°の角度をなす2本の直線(6)、(7)との交点(8)、(9)、(10)、(11)を結ぶ、前記直線に平行な線分(12)を1辺とする正六角形と前記直線(2)とで円板を分割して得られる4枚の分割片の、該正六角形の外側に位置する2つの部分を、前記2本の直線(6)、(7)でさらにそれぞれ3分割して得られる、6枚の合同な分割片(13)、(14)、(15)、(16)、(17)、(18)、および正六角形の3辺と直径とを辺とする2枚の台形状の分割片から、前記6枚の分割片とほぼ合同な2枚の焼結体分割片(19)、(20)を切り出すことによって得られる、8枚のほぼ合同な焼結体分割片の、円弧状の辺の両端部角を丸めたものからなる、8枚のほぼ合同な形状の研磨パッチ。   A straight line (2) passing through the center of the disk-shaped sintered material (1) and a point (4) obtained by dividing a radius (3) perpendicular to the straight line into two equal parts are parallel to the straight line (2). Connecting the intersections (8), (9), (10), (11) with two straight lines (6), (7) passing through the center of the line and the disk and forming an angle of 60 ° with the straight line, Two parts located outside the regular hexagon of four divided pieces obtained by dividing a disc into a regular hexagon having one side of a line segment (12) parallel to the straight line and the straight line (2) Are obtained by further dividing each of the two straight lines (6) and (7) into three, respectively, and six concatenated pieces (13), (14), (15), (16), (17) , (18) and two trapezoidal divided pieces having three sides and a diameter of a regular hexagon as sides, and two sintered body divided pieces (19) substantially congruent with the six divided pieces, (20) Obtained by cutting, the eight substantially congruent sintered body split pieces, consist of rounded both ends angle of the arc-shaped sides, polishing patch eight substantially congruent shapes. 請求項3に記載の8枚の合同な焼結体分割片を、さらに円板外形をなしていた円弧と同心円をなす円弧(23)で2つまたはそれ以上のパッチ片に分割し、円弧状の辺の両端部角を丸めて得られる、8枚のほぼ合同な研磨パッチの複数の組からなる、研磨パッチ。   The eight congruent sintered body divided pieces according to claim 3 are further divided into two or more patch pieces by an arc (23) that is concentric with the arc that has formed the outer shape of the disk, A polishing patch comprising a plurality of sets of eight substantially congruent polishing patches, obtained by rounding the corners on both ends of the side. 請求項3に記載の研磨パッチにおいて、正六角形の内側の2枚の焼結体分割片(19)、(20)とそれらとそれぞれ正六角形の1辺で接している外側の焼結体分割片(13)、(14)とに代えて、それぞれ接している1辺で結合した輪郭を有する、瓢箪型のくびれを有する2枚のほぼ合同な切片(28)、(29)の組と、1辺が円弧である台形様の4枚のほぼ合同な切片(14)、(15)、(17)、(18)の組とからなる、
6枚の研磨パッチ。
4. The polishing patch according to claim 3, wherein the two sintered body divided pieces (19) and (20) on the inner side of the regular hexagon and the outer sintered body divided pieces respectively in contact with one side of the regular hexagon. Instead of (13) and (14), a set of two substantially congruent sections (28) and (29) having a saddle-shaped constriction, each having a contour joined by one side in contact with each other, and 1 It consists of a set of four substantially congruent sections (14), (15), (17), (18) in a trapezoidal shape whose sides are arcs.
6 polishing patches.
請求項1〜5のいずれかに記載の研磨パッチを、円形基板の外周部分に、1種または複数種の研磨パッチが、円周方向に均等に配置されるように設けた、研磨工具。   A polishing tool in which the polishing patch according to any one of claims 1 to 5 is provided on an outer peripheral portion of a circular substrate so that one or more types of polishing patches are evenly arranged in a circumferential direction. 円板状の焼結体素材(1)の中心を通る直線(2)と、前記直線に直交する半径(3)、(3’)を2等分した点(4)、(4’)を通り、前記直線に平行な線と円板の中心を通り前記直線と60°の角度をなす2本の直線(6)、(7)との交点(8)、(9)、(10)(11)を結ぶ前記直線(2)に平行な線分(12)、(12’)を1辺とする正六角形と前記直線(2)とで円板を4枚に分割し、該正六角形の外側に位置する2つの部分を、前記2本の直線(6)(7)でさらにそれぞれ3分割して得られる、6枚の合同な分割片(13)、(14)、(15)(16)、(17)、(18)、および正六角形の3辺と前記直線(2)とを辺とする2枚の台形状の分割片(19)、(20)から切り出すことにより、円板状の焼結体素材から8枚の焼結体分割片を得る、研磨パッチ製造方法。   Points (4) and (4 ') obtained by dividing a straight line (2) passing through the center of the disk-shaped sintered material (1) and radii (3) and (3') perpendicular to the straight line into two equal parts. And intersections (8), (9), (10) (2) of two straight lines (6), (7) passing through the center of the disk and a line parallel to the straight line and forming an angle of 60 ° with the straight line. 11) A regular hexagon with one side of the line segments (12) and (12 ′) parallel to the straight line (2) connecting the straight line (2) and the straight line (2) are divided into four disks, Six concatenated pieces (13), (14), (15), (16) obtained by further dividing the two portions located outside by the two straight lines (6) (7), respectively. ), (17), (18) and two trapezoidal split pieces (19), (20) each having three sides of the regular hexagon and the straight line (2) as a disk, Sintering Obtaining eight sintered body split pieces from the material, the polishing patch production method. 請求項7に記載の方法において、正六角形の内側の2枚の焼結体分割片(19)、(20)と、それぞれ正六角形の1辺で接している、外側の焼結体分割片(13)、(14)との間は切断せずに、瓢箪型のくびれを有する2枚の合同な切片(28)、(29)として残す、1辺が円弧である台形様の4枚の合同な切片(14)、(15)、(17)、(18)の組と、瓢箪型の括れを有する2枚の合同な切片(28)、(29)とから切り出すことにより、円板状の焼結体素材から6枚の研磨パッチを製造する方法。   The method according to claim 7, wherein the two sintered body divided pieces (19) and (20) inside the regular hexagon are in contact with one side of the regular hexagon, respectively. 13) and (14) are not cut and left as two congruent sections (28) and (29) having a saddle-shaped constriction. By cutting out from a set of sections (14), (15), (17), (18) and two joint sections (28), (29) having a saddle-shaped constriction, A method of manufacturing six polishing patches from a sintered material. 切り出した研磨パッチの角部を丸めて、研磨パッチを互いにほぼ合同とする工程をさらに含む、請求項7または8に記載の方法。   The method according to claim 7 or 8, further comprising the step of rounding corners of the cut abrasive patch so that the abrasive patches are substantially congruent with each other.
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