JP2010527288A5 - - Google Patents
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- JP2010527288A5 JP2010527288A5 JP2010508393A JP2010508393A JP2010527288A5 JP 2010527288 A5 JP2010527288 A5 JP 2010527288A5 JP 2010508393 A JP2010508393 A JP 2010508393A JP 2010508393 A JP2010508393 A JP 2010508393A JP 2010527288 A5 JP2010527288 A5 JP 2010527288A5
- Authority
- JP
- Japan
- Prior art keywords
- con
- sulfur
- adsorbent
- mercury
- certain
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 239
- 229910052751 metal Inorganic materials 0.000 claims description 191
- 239000002184 metal Substances 0.000 claims description 188
- 239000003463 adsorbent Substances 0.000 claims description 176
- NINIDFKCEFEMDL-UHFFFAOYSA-N sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 170
- 239000003054 catalyst Substances 0.000 claims description 165
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims description 161
- 229910052717 sulfur Inorganic materials 0.000 claims description 148
- 239000011593 sulfur Substances 0.000 claims description 148
- 229910052753 mercury Inorganic materials 0.000 claims description 135
- 239000011159 matrix material Substances 0.000 claims description 60
- 239000003440 toxic substance Substances 0.000 claims description 54
- 231100000614 Poison Toxicity 0.000 claims description 48
- 229910052799 carbon Inorganic materials 0.000 claims description 44
- 239000012530 fluid Substances 0.000 claims description 31
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 28
- 150000001875 compounds Chemical class 0.000 claims description 27
- PWHULOQIROXLJO-UHFFFAOYSA-N manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 20
- 239000011572 manganese Substances 0.000 claims description 18
- 229910052748 manganese Inorganic materials 0.000 claims description 18
- 230000003647 oxidation Effects 0.000 claims description 18
- 238000007254 oxidation reaction Methods 0.000 claims description 18
- BUGBHKTXTAQXES-UHFFFAOYSA-N selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 claims description 17
- 229910052711 selenium Inorganic materials 0.000 claims description 17
- 239000011669 selenium Substances 0.000 claims description 17
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 claims description 16
- 229910052785 arsenic Inorganic materials 0.000 claims description 16
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 claims description 16
- 229910052793 cadmium Inorganic materials 0.000 claims description 16
- 229910052709 silver Inorganic materials 0.000 claims description 15
- HCHKCACWOHOZIP-UHFFFAOYSA-N zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 15
- 229910052725 zinc Inorganic materials 0.000 claims description 15
- 239000011701 zinc Substances 0.000 claims description 15
- 229910052804 chromium Inorganic materials 0.000 claims description 14
- VYZAMTAEIAYCRO-UHFFFAOYSA-N chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 14
- 239000011651 chromium Substances 0.000 claims description 14
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 14
- 229910052803 cobalt Inorganic materials 0.000 claims description 14
- 239000010941 cobalt Substances 0.000 claims description 14
- 229910052802 copper Inorganic materials 0.000 claims description 14
- 239000010949 copper Substances 0.000 claims description 14
- RYGMFSIKBFXOCR-UHFFFAOYSA-N copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 14
- 229910052759 nickel Inorganic materials 0.000 claims description 14
- 239000004332 silver Substances 0.000 claims description 14
- BQCADISMDOOEFD-UHFFFAOYSA-N silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 14
- 229910052720 vanadium Inorganic materials 0.000 claims description 14
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium(0) Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims description 14
- 210000003660 Reticulum Anatomy 0.000 claims description 12
- 229910052788 barium Inorganic materials 0.000 claims description 10
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium(0) Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims description 10
- 229910052716 thallium Inorganic materials 0.000 claims description 10
- BKVIYDNLLOSFOA-UHFFFAOYSA-N thallium Chemical compound [Tl] BKVIYDNLLOSFOA-UHFFFAOYSA-N 0.000 claims description 10
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims description 9
- 229910052787 antimony Inorganic materials 0.000 claims description 9
- 229910052790 beryllium Inorganic materials 0.000 claims description 9
- ATBAMAFKBVZNFJ-UHFFFAOYSA-N beryllium(0) Chemical compound [Be] ATBAMAFKBVZNFJ-UHFFFAOYSA-N 0.000 claims description 9
- 231100000167 toxic agent Toxicity 0.000 claims description 8
- ZOKXTWBITQBERF-UHFFFAOYSA-N molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 5
- 229910052750 molybdenum Inorganic materials 0.000 claims description 5
- 239000011733 molybdenum Substances 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxyl anion Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 1
- 150000003568 thioethers Chemical class 0.000 claims 1
- 201000002674 obstructive nephropathy Diseases 0.000 description 216
- 239000000463 material Substances 0.000 description 123
- 239000000203 mixture Substances 0.000 description 115
- 239000011148 porous material Substances 0.000 description 60
- 239000002594 sorbent Substances 0.000 description 49
- 239000007789 gas Substances 0.000 description 35
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical class [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 32
- UGFAIRIUMAVXCW-UHFFFAOYSA-N carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 31
- 239000003546 flue gas Substances 0.000 description 30
- 239000011256 inorganic filler Substances 0.000 description 30
- 229910003475 inorganic filler Inorganic materials 0.000 description 30
- 238000000034 method Methods 0.000 description 28
- 239000000843 powder Substances 0.000 description 25
- 238000001125 extrusion Methods 0.000 description 22
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 21
- -1 lanthanoids) Chemical class 0.000 description 21
- 238000003763 carbonization Methods 0.000 description 20
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 19
- 150000004763 sulfides Chemical class 0.000 description 19
- 239000006185 dispersion Substances 0.000 description 18
- 229920005989 resin Polymers 0.000 description 17
- 239000011347 resin Substances 0.000 description 17
- 239000012298 atmosphere Substances 0.000 description 16
- 239000011230 binding agent Substances 0.000 description 16
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 16
- 239000003921 oil Substances 0.000 description 16
- 235000019198 oils Nutrition 0.000 description 16
- 230000004913 activation Effects 0.000 description 15
- 239000000835 fiber Substances 0.000 description 15
- 230000015572 biosynthetic process Effects 0.000 description 14
- 238000006243 chemical reaction Methods 0.000 description 14
- 229910052742 iron Inorganic materials 0.000 description 13
- NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Substances [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 13
- 239000002245 particle Substances 0.000 description 12
- 239000011780 sodium chloride Substances 0.000 description 12
- 239000000126 substance Substances 0.000 description 12
- 241000264877 Hippospongia communis Species 0.000 description 11
- 229910052878 cordierite Inorganic materials 0.000 description 11
- 150000003839 salts Chemical class 0.000 description 11
- 101700049479 RFG1 Proteins 0.000 description 10
- 239000003245 coal Substances 0.000 description 10
- 239000000945 filler Substances 0.000 description 10
- 238000011065 in-situ storage Methods 0.000 description 10
- 229920001568 phenolic resin Polymers 0.000 description 10
- 239000005011 phenolic resin Substances 0.000 description 10
- NBIIXXVUZAFLBC-UHFFFAOYSA-N phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 10
- 210000002421 Cell Wall Anatomy 0.000 description 9
- 238000005755 formation reaction Methods 0.000 description 9
- 229910010272 inorganic material Inorganic materials 0.000 description 9
- 239000011147 inorganic material Substances 0.000 description 9
- 229920003043 Cellulose fiber Polymers 0.000 description 8
- 241000196324 Embryophyta Species 0.000 description 8
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 8
- 238000001994 activation Methods 0.000 description 8
- 238000009826 distribution Methods 0.000 description 8
- 229910052757 nitrogen Inorganic materials 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 7
- 238000005470 impregnation Methods 0.000 description 7
- 229910000468 manganese oxide Inorganic materials 0.000 description 7
- 229920003091 Methocel™ Polymers 0.000 description 6
- UIIMBOGNXHQVGW-UHFFFAOYSA-M NaHCO3 Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 6
- MCMNRKCIXSYSNV-UHFFFAOYSA-N ZrO2 Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 6
- 229910000323 aluminium silicate Inorganic materials 0.000 description 6
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 6
- VASIZKWUTCETSD-UHFFFAOYSA-N manganese(II) oxide Inorganic materials [Mn]=O VASIZKWUTCETSD-UHFFFAOYSA-N 0.000 description 6
- 229920003987 resole Polymers 0.000 description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 229910001868 water Inorganic materials 0.000 description 6
- LNAZSHAWQACDHT-XIYTZBAFSA-N (2R,3R,4S,5R,6S)-4,5-dimethoxy-2-(methoxymethyl)-3-[(2S,3R,4S,5R,6R)-3,4,5-trimethoxy-6-(methoxymethyl)oxan-2-yl]oxy-6-[(2R,3R,4S,5R,6R)-4,5,6-trimethoxy-2-(methoxymethyl)oxan-3-yl]oxyoxane Chemical compound CO[C@@H]1[C@@H](OC)[C@H](OC)[C@@H](COC)O[C@H]1O[C@H]1[C@H](OC)[C@@H](OC)[C@H](O[C@H]2[C@@H]([C@@H](OC)[C@H](OC)O[C@@H]2COC)OC)O[C@@H]1COC LNAZSHAWQACDHT-XIYTZBAFSA-N 0.000 description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N AI2O3 Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 5
- XPFVYQJUAUNWIW-UHFFFAOYSA-N Furfuryl alcohol Chemical compound OCC1=CC=CO1 XPFVYQJUAUNWIW-UHFFFAOYSA-N 0.000 description 5
- RYYKJJJTJZKILX-UHFFFAOYSA-M Sodium stearate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 5
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 5
- 239000011575 calcium Substances 0.000 description 5
- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 description 5
- 238000011049 filling Methods 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 238000001746 injection moulding Methods 0.000 description 5
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 5
- 229910000460 iron oxide Inorganic materials 0.000 description 5
- 235000013980 iron oxide Nutrition 0.000 description 5
- 229910052747 lanthanoid Inorganic materials 0.000 description 5
- 241000894007 species Species 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-L sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 5
- 238000003786 synthesis reaction Methods 0.000 description 5
- 230000002194 synthesizing Effects 0.000 description 5
- 229910052723 transition metal Inorganic materials 0.000 description 5
- POILWHVDKZOXJZ-ARJAWSKDSA-M (Z)-4-oxopent-2-en-2-olate Chemical compound C\C([O-])=C\C(C)=O POILWHVDKZOXJZ-ARJAWSKDSA-M 0.000 description 4
- VUKAUDKDFVSVFT-UHFFFAOYSA-N 2-[6-[4,5-bis(2-hydroxypropoxy)-2-(2-hydroxypropoxymethyl)-6-methoxyoxan-3-yl]oxy-4,5-dimethoxy-2-(methoxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)-5-methoxyoxane-3,4-diol Chemical compound COC1C(OC)C(OC2C(C(O)C(OC)C(CO)O2)O)C(COC)OC1OC1C(COCC(C)O)OC(OC)C(OCC(C)O)C1OCC(C)O VUKAUDKDFVSVFT-UHFFFAOYSA-N 0.000 description 4
- UKWHYYKOEPRTIC-UHFFFAOYSA-N Mercury(II) oxide Chemical compound [Hg]=O UKWHYYKOEPRTIC-UHFFFAOYSA-N 0.000 description 4
- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 description 4
- 239000000654 additive Substances 0.000 description 4
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- 238000002347 injection Methods 0.000 description 4
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- VBMVTYDPPZVILR-UHFFFAOYSA-N iron(2+);oxygen(2-) Chemical class [O-2].[Fe+2] VBMVTYDPPZVILR-UHFFFAOYSA-N 0.000 description 4
- 150000002602 lanthanoids Chemical class 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- FYYHWMGAXLPEAU-UHFFFAOYSA-N magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 4
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- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium Chemical class [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 4
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- 239000010955 niobium Chemical class 0.000 description 4
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- 239000000075 oxide glass Substances 0.000 description 4
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- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 238000001878 scanning electron micrograph Methods 0.000 description 4
- KEAYESYHFKHZAL-UHFFFAOYSA-N sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 4
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- 239000011734 sodium Substances 0.000 description 4
- 150000003624 transition metals Chemical class 0.000 description 4
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- NUJOXMJBOLGQSY-UHFFFAOYSA-N Manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 3
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- LSNNMFCWUKXFEE-UHFFFAOYSA-L Sulphite Chemical class [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 3
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
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- 229910052783 alkali metal Inorganic materials 0.000 description 3
- 150000001340 alkali metals Chemical class 0.000 description 3
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- 239000011324 bead Substances 0.000 description 3
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- MBMLMWLHJBBADN-UHFFFAOYSA-N iron-sulfur Chemical compound [Fe]=S MBMLMWLHJBBADN-UHFFFAOYSA-N 0.000 description 3
- AMWRITDGCCNYAT-UHFFFAOYSA-L manganese(II,III) oxide Inorganic materials [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 description 3
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- 125000004432 carbon atoms Chemical group C* 0.000 description 2
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- PPNAOCWZXJOHFK-UHFFFAOYSA-N manganese(2+);oxygen(2-) Chemical class [O-2].[Mn+2] PPNAOCWZXJOHFK-UHFFFAOYSA-N 0.000 description 2
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| US7998898B2 (en) | 2007-10-26 | 2011-08-16 | Corning Incorporated | Sorbent comprising activated carbon, process for making same and use thereof |
| US20090297885A1 (en) * | 2008-05-30 | 2009-12-03 | Kishor Purushottam Gadkaree | Composite Comprising An Inorganic Substrate With A Coating Comprising Activated Carbon And Metal Sulfide |
| US8691722B2 (en) | 2008-07-03 | 2014-04-08 | Corning Incorporated | Sorbent comprising activated carbon particles, sulfur and metal catalyst |
| US20100050869A1 (en) * | 2008-08-28 | 2010-03-04 | Kishor Purushottam Gadkaree | Plate System For Contaminant Removal |
| CN101480605B (zh) * | 2009-01-05 | 2011-05-25 | 浙江工业大学 | 一种活性炭纤维吸附剂及其制备方法和应用 |
| GB0900965D0 (en) * | 2009-01-21 | 2009-03-04 | Johnson Matthey Plc | Sorbents |
| US8598073B2 (en) * | 2009-04-20 | 2013-12-03 | Corning Incorporated | Methods of making and using activated carbon-containing coated substrates and the products made therefrom |
| US10471384B2 (en) | 2009-04-22 | 2019-11-12 | The Babcock & Wilcox Company | System and method for reducing halogen levels necessary for mercury control, increasing the service life and/or catalytic activity of an SCR catalyst and/or control of multiple emissions |
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2008
- 2008-05-13 WO PCT/US2008/006082 patent/WO2008143831A2/fr active Application Filing
- 2008-05-13 CA CA002686986A patent/CA2686986A1/fr not_active Abandoned
- 2008-05-13 JP JP2010508393A patent/JP5291092B2/ja not_active Expired - Fee Related
- 2008-05-13 KR KR1020097025996A patent/KR101516836B1/ko not_active IP Right Cessation
- 2008-05-13 CN CN2008800224132A patent/CN101687173B/zh not_active Expired - Fee Related
- 2008-05-13 EP EP08754390A patent/EP2150337A2/fr not_active Withdrawn
- 2008-05-14 TW TW097117771A patent/TW200914126A/zh unknown
-
2013
- 2013-01-04 JP JP2013000083A patent/JP2013126661A/ja active Pending
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