JP2010526803A - カチオン光開始剤用増感剤 - Google Patents
カチオン光開始剤用増感剤 Download PDFInfo
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- JP2010526803A JP2010526803A JP2010507021A JP2010507021A JP2010526803A JP 2010526803 A JP2010526803 A JP 2010526803A JP 2010507021 A JP2010507021 A JP 2010507021A JP 2010507021 A JP2010507021 A JP 2010507021A JP 2010526803 A JP2010526803 A JP 2010526803A
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
- C07D317/32—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D317/34—Oxygen atoms
- C07D317/36—Alkylene carbonates; Substituted alkylene carbonates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/68—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the catalysts used
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
- C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
- C08G65/08—Saturated oxiranes
- C08G65/10—Saturated oxiranes characterised by the catalysts used
- C08G65/105—Onium compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/101—Inks specially adapted for printing processes involving curing by wave energy or particle radiation, e.g. with UV-curing following the printing
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D171/00—Coating compositions based on polyethers obtained by reactions forming an ether link in the main chain; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D171/00—Coating compositions based on polyethers obtained by reactions forming an ether link in the main chain; Coating compositions based on derivatives of such polymers
- C09D171/02—Polyalkylene oxides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J171/00—Adhesives based on polyethers obtained by reactions forming an ether link in the main chain; Adhesives based on derivatives of such polymers
- C09J171/02—Polyalkylene oxides
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
- G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
- G03F7/004—Photosensitive materials
- G03F7/038—Macromolecular compounds which are rendered insoluble or differentially wettable
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Epoxy Resins (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Paints Or Removers (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Polymerisation Methods In General (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Abstract
Description
Qは、少なくとも2つの共役芳香族環を有し、価数xを有している多環式の芳香族化合物の残基を表わす;
Yは、1つ以上の酸素原子、硫黄原子、フェニレン基、カルボニル基、エポキシド基を途中に有することができる脂肪族の炭素鎖、または直鎖もしくは環式カルボネート基である;
pは0または1である;
R1とR2は互いに同じか相違することができ、それぞれ水素原子、アルキル基、ヒドロキシアルキル基、アルコキシアルキル基、アルコキシカルボニルアルキル基、またはYの炭素原子に結合して縮合環を形成するC2−C5炭素鎖である;
R3は水素原子またはアルキル基を表わす;
また、mとnは互いに同じか相違することができ、それぞれ0または1から4であり、(m+n)は0または1から4の数である。
ガラス質の固形物が58g得られた。
生成物はIRによって分析され、1790cm−1に非常に強いカルボネート・ピークを示した。
明るい褐色の粉末が14.05g得られた。
生成物はIRによって分析され、1781cm−1に非常に強いカルボネート・ピークを示した。
ガラス質の固形物が65g得られた。
生成物はIRによって分析され、1793cm−1に非常に強いカルボネート・ピークを示した。
ワニス配合物が以下に基づいて調製された。
Omnicat 440 光開始剤、IGM製 2.0%
Tegorad 2100 湿潤剤 TEGO製 0.1%
増感剤 2%
UVACURE 1500 脂環式エポキシド CYTEC製 95.9%
黒色インク配合物が以下に基づいて調製された。
Omnicat 440 光開始剤 IGM製 2.0%
Special black 250 顔料 15.0%
OXT 221 ジオキセタンモノマー10.0%
Solsperse 32000 顔料分散物 1.25%
増感剤 2%
UVACURE 1500 脂環式エポキシド CYTEC製 69.75%
ワニス塗料が以下に基づいて調製された。
Omnicat 440 光開始剤 IGM製 1.0%
Tegorad 2100 湿潤剤 TEGO製 0.1%
実施例1 0―20%
UVACURE 1500 脂環式エポキシド CYTEC製 残部
白色フレキソ印刷インキが以下に基づいて調製された;
二酸化チタン(FINNITITAN RDI/S Kemira製)40.0%
UVACURE 1500 脂環式エポキシド CYTEC製 40.3%
プロピレンカーボネート 12%
Omnicat 440 光開始剤 IGM製 2%
増感剤 2%
Solsperse 32000 顔料分散剤溶液 2.5%
ポリエチレン・ワックス 1.2%
Claims (23)
- 少なくとも2つの共役芳香族環を有し、その少なくとも1つは環状カルボネート基を含む置換基を有する、多環式芳香族化合物。
- 以下の式(I)を有する請求項1記載の化合物:
式中、
Qは、少なくとも2つの共役芳香族環を有し、価数xを有している多環式の芳香族化合物の残基を表わす;
Yは、1つ以上の酸素原子、硫黄原子、フェニレン基、カルボニル基、エポキシド基を途中に有することができる脂肪族の炭素鎖、または直鎖もしくは環式カルボネート基である;
pは0または1である;
R1とR2は互いに同じか相違することができ、それぞれ水素原子、アルキル基、ヒドロキシアルキル基、アルコキシアルキル基、アルコキシカルボニルアルキル基、またはYの炭素原子に結合して縮合環を形成するC2−C5炭素鎖である;
R3は水素原子またはアルキル基を表わす;
また、mとnは互いに同じか相違することができ、それぞれ0または1から4であり、(m+n)は0または1から4の数である。 - Y1はメチレン基を表す、請求項3記載の化合物。
- Qの共役芳香族環は縮合環である、請求項1から4のいずれか1項記載の化合物。
- 共役芳香族環は、置換されるか置換されていないナフタレンまたはアントラセン環システムである、請求項1から5のいずれか1項記載の化合物。
- Qがアントラセンまたはナフタレン環システムの残基を表わし、それは置換されていないか、または少なくとも1つのアルキル置換基を有し;
m+n=1;
R1、R2およびR3はすべて水素原子を表わし;
YはY1−O−であり;
Y1は、1から3の炭素原子を有するアルキレン基を表す、請求項2記載の化合物。 - Qがアントラセンまたはナフタレン環システムの残基を表わし、それは置換されていないか、または少なくとも1つのアルキル置換基を有し;
m+n=1;
R1およびR2は両者とも水素原子を表わし;
Y1は、1から3の炭素原子を有するアルキレン基を表す、請求項3記載の化合物。 - 共役芳香族環がビフェニルである、請求項1記載の化合物。
- カチオン性光開始剤および請求項1から11のいずれか1項記載の化合物を含む組成物。
- 前記の光開始剤がヨードニウム塩である、請求項12記載の組成物。
- カチオン性光開始剤、請求項1から11のいずれか1項記載の化合物、およびカチオン重合可能なモノマーまたはオリゴマーを含む、カチオン硬化可能な組成物。
- 前記の光開始剤がヨードニウム塩である、請求項14記載の組成物。
- 請求項1から11のいずれか1項記載の化合物が、組成物の合計の重合可能な成分の1から50重量%を構成する、請求項14または15記載の組成物。
- 請求項1から11のいずれか1項記載の化合物が、組成物の合計の0.5から3重量%を構成する、請求項14または15記載の組成物。
- コーティング組成物として配合される、請求項14から17のいずれか1項記載の組成物。
- 印刷インキとして配合される、請求項14から17のいずれか1項記載の組成物。
- インクジェットインキとして配合される、請求項14から17のいずれか1項記載の組成物。
- 接着剤、リリースコーティング、またはプライマーとして配合される、請求項14から17のいずれか1項記載の組成物。
- 硬化されたコーティング組成物を調製するプロセスであって、基体へ請求項14から21のいずれか1項記載の組成物を適用し、コーティングを硬化するのに十分な硬化用放射線にコーティングされた基体を暴露することを含むプロセス。
- 硬化用放射線が紫外線である、請求項22記載のプロセス。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB0709119.2 | 2007-05-11 | ||
GB0709119A GB2449124A (en) | 2007-05-11 | 2007-05-11 | Sensitiser for cationic photoinitiators |
PCT/IB2008/001187 WO2008139315A2 (en) | 2007-05-11 | 2008-05-09 | Sensitizer for cationic photoinitiators |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2010526803A true JP2010526803A (ja) | 2010-08-05 |
JP5371151B2 JP5371151B2 (ja) | 2013-12-18 |
Family
ID=38219270
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2010507021A Active JP5371151B2 (ja) | 2007-05-11 | 2008-05-09 | カチオン光開始剤用増感剤 |
Country Status (5)
Country | Link |
---|---|
US (1) | US8785515B2 (ja) |
EP (1) | EP2150542B1 (ja) |
JP (1) | JP5371151B2 (ja) |
GB (1) | GB2449124A (ja) |
WO (1) | WO2008139315A2 (ja) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2011063652A (ja) * | 2009-09-15 | 2011-03-31 | Toshiba Tec Corp | 感光性インクおよびそれを用いた硬化物 |
JP2014524468A (ja) * | 2011-08-22 | 2014-09-22 | ダウ グローバル テクノロジーズ エルエルシー | 環状炭酸塩モノマーおよびそれより調製されるポリマー |
JP2018118946A (ja) * | 2017-01-27 | 2018-08-02 | デクセリアルズ株式会社 | フルオレン誘導体、及びその製造方法、樹脂組成物、並びに物品 |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2423521A (en) * | 2005-02-25 | 2006-08-30 | Sun Chemical Ltd | Energy-curable coating composition |
WO2010089264A1 (de) * | 2009-02-05 | 2010-08-12 | Basf Se | Verfahren zur herstellung von biscarbonaten |
DE102010037592A1 (de) * | 2010-09-16 | 2012-03-22 | Steinemann Technology Ag | Verfahren zur Herstellung eines Laminats und dazu gehörige Bogenlaminiermaschine |
WO2017048984A1 (en) | 2015-09-15 | 2017-03-23 | G3 Enterprises, Inc. | Apparatus and methods for alternative coatings applicable to metal |
WO2018055609A1 (en) * | 2016-09-21 | 2018-03-29 | Massivit 3D Printing Technologies Ltd | Method and apparatus for manufacturing 3d objects |
US11267977B2 (en) | 2017-08-10 | 2022-03-08 | Sun Chemical Corporation | UV-curable compositions comprising acylphosphine oxide photoinitiators |
US11707763B2 (en) * | 2018-11-20 | 2023-07-25 | G3 Enterprises, Inc. | Apparatus and methods using coatings for metal applications |
WO2022055625A1 (en) | 2020-09-10 | 2022-03-17 | Sun Chemical Corporation | Led energy curable ink compositions |
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JP2006208607A (ja) * | 2005-01-26 | 2006-08-10 | Fuji Photo Film Co Ltd | パターン形成材料、並びにパターン形成装置及び永久パターン形成方法 |
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-
2007
- 2007-05-11 GB GB0709119A patent/GB2449124A/en not_active Withdrawn
-
2008
- 2008-05-09 EP EP08750928A patent/EP2150542B1/en active Active
- 2008-05-09 JP JP2010507021A patent/JP5371151B2/ja active Active
- 2008-05-09 US US12/598,113 patent/US8785515B2/en active Active
- 2008-05-09 WO PCT/IB2008/001187 patent/WO2008139315A2/en active Application Filing
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JPH1045743A (ja) * | 1996-08-02 | 1998-02-17 | Kyowa Hakko Kogyo Co Ltd | カリックスアレン誘導体及びその製造方法 |
JP2006208607A (ja) * | 2005-01-26 | 2006-08-10 | Fuji Photo Film Co Ltd | パターン形成材料、並びにパターン形成装置及び永久パターン形成方法 |
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Cited By (4)
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JP2011063652A (ja) * | 2009-09-15 | 2011-03-31 | Toshiba Tec Corp | 感光性インクおよびそれを用いた硬化物 |
JP2014524468A (ja) * | 2011-08-22 | 2014-09-22 | ダウ グローバル テクノロジーズ エルエルシー | 環状炭酸塩モノマーおよびそれより調製されるポリマー |
JP2018118946A (ja) * | 2017-01-27 | 2018-08-02 | デクセリアルズ株式会社 | フルオレン誘導体、及びその製造方法、樹脂組成物、並びに物品 |
JP7072789B2 (ja) | 2017-01-27 | 2022-05-23 | デクセリアルズ株式会社 | フルオレン誘導体、及びその製造方法、樹脂組成物、並びに物品 |
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WO2008139315A2 (en) | 2008-11-20 |
US20100129563A1 (en) | 2010-05-27 |
US8785515B2 (en) | 2014-07-22 |
GB0709119D0 (en) | 2007-06-20 |
WO2008139315A3 (en) | 2009-01-08 |
EP2150542A2 (en) | 2010-02-10 |
JP5371151B2 (ja) | 2013-12-18 |
GB2449124A (en) | 2008-11-12 |
EP2150542B1 (en) | 2013-01-16 |
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