JP2010006808A5 - - Google Patents
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- Publication number
- JP2010006808A5 JP2010006808A5 JP2009146450A JP2009146450A JP2010006808A5 JP 2010006808 A5 JP2010006808 A5 JP 2010006808A5 JP 2009146450 A JP2009146450 A JP 2009146450A JP 2009146450 A JP2009146450 A JP 2009146450A JP 2010006808 A5 JP2010006808 A5 JP 2010006808A5
- Authority
- JP
- Japan
- Prior art keywords
- column
- reaction
- carbonate
- boiling point
- condensation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000006243 chemical reaction Methods 0.000 claims description 82
- -1 diaryl carbonate Chemical compound 0.000 claims description 82
- 238000000034 method Methods 0.000 claims description 56
- 238000004821 distillation Methods 0.000 claims description 44
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 38
- 238000009835 boiling Methods 0.000 claims description 30
- 238000009833 condensation Methods 0.000 claims description 27
- 230000005494 condensation Effects 0.000 claims description 27
- 238000011084 recovery Methods 0.000 claims description 18
- 150000001875 compounds Chemical class 0.000 claims description 16
- 125000005233 alkylalcohol group Chemical group 0.000 claims description 11
- 238000004519 manufacturing process Methods 0.000 claims description 9
- 238000000926 separation method Methods 0.000 claims description 8
- 239000003054 catalyst Substances 0.000 claims description 6
- 238000000746 purification Methods 0.000 claims description 4
- 238000005809 transesterification reaction Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 2
- 239000000047 product Substances 0.000 claims description 2
- 238000002844 melting Methods 0.000 claims 2
- 230000008018 melting Effects 0.000 claims 2
- 239000006227 byproduct Substances 0.000 claims 1
- 239000000203 mixture Substances 0.000 description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 15
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
- 239000000543 intermediate Substances 0.000 description 11
- 239000007788 liquid Substances 0.000 description 7
- RDOXTESZEPMUJZ-UHFFFAOYSA-N anisole Chemical compound COC1=CC=CC=C1 RDOXTESZEPMUJZ-UHFFFAOYSA-N 0.000 description 6
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 description 6
- 239000012466 permeate Substances 0.000 description 6
- 238000005373 pervaporation Methods 0.000 description 5
- 238000010992 reflux Methods 0.000 description 5
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- UZKWTJUDCOPSNM-UHFFFAOYSA-N methoxybenzene Substances CCCCOC=C UZKWTJUDCOPSNM-UHFFFAOYSA-N 0.000 description 3
- 125000003710 aryl alkyl group Chemical group 0.000 description 2
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 229930000044 secondary metabolite Natural products 0.000 description 2
- 125000005918 1,2-dimethylbutyl group Chemical group 0.000 description 1
- 125000006218 1-ethylbutyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000006176 2-ethylbutyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(C([H])([H])*)C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000004493 2-methylbut-1-yl group Chemical group CC(C*)CC 0.000 description 1
- 125000005916 2-methylpentyl group Chemical group 0.000 description 1
- 125000003542 3-methylbutan-2-yl group Chemical group [H]C([H])([H])C([H])(*)C([H])(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- 125000005917 3-methylpentyl group Chemical group 0.000 description 1
- 125000005073 adamantyl group Chemical group C12(CC3CC(CC(C1)C3)C2)* 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
- 125000001511 cyclopentyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 description 1
- ROORDVPLFPIABK-UHFFFAOYSA-N diphenyl carbonate Chemical compound C=1C=CC=CC=1OC(=O)OC1=CC=CC=C1 ROORDVPLFPIABK-UHFFFAOYSA-N 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 210000000416 exudates and transudate Anatomy 0.000 description 1
- 125000002768 hydroxyalkyl group Chemical group 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
- 125000004491 isohexyl group Chemical group C(CCC(C)C)* 0.000 description 1
- 125000001972 isopentyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- XTBFPVLHGVYOQH-UHFFFAOYSA-N methyl phenyl carbonate Chemical compound COC(=O)OC1=CC=CC=C1 XTBFPVLHGVYOQH-UHFFFAOYSA-N 0.000 description 1
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000003136 n-heptyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000001280 n-hexyl group Chemical group C(CCCCC)* 0.000 description 1
- 125000000740 n-pentyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000001971 neopentyl group Chemical group [H]C([*])([H])C(C([H])([H])[H])(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- YCWSUKQGVSGXJO-NTUHNPAUSA-N nifuroxazide Chemical group C1=CC(O)=CC=C1C(=O)N\N=C\C1=CC=C([N+]([O-])=O)O1 YCWSUKQGVSGXJO-NTUHNPAUSA-N 0.000 description 1
- 125000003538 pentan-3-yl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 125000002914 sec-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 125000003548 sec-pentyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- 125000001973 tert-pentyl group Chemical group [H]C([H])([H])C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- DPNUIZVZBWBCPB-UHFFFAOYSA-J titanium(4+);tetraphenoxide Chemical compound [Ti+4].[O-]C1=CC=CC=C1.[O-]C1=CC=CC=C1.[O-]C1=CC=CC=C1.[O-]C1=CC=CC=C1 DPNUIZVZBWBCPB-UHFFFAOYSA-J 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102008029514A DE102008029514A1 (de) | 2008-06-21 | 2008-06-21 | Verfahren zur Herstellung von Diarylcarbonaten aus Dialkylcarbonaten |
| DE102008029514.0 | 2008-06-21 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010006808A JP2010006808A (ja) | 2010-01-14 |
| JP2010006808A5 true JP2010006808A5 (enExample) | 2012-08-02 |
| JP5596307B2 JP5596307B2 (ja) | 2014-09-24 |
Family
ID=41151820
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009146450A Expired - Fee Related JP5596307B2 (ja) | 2008-06-21 | 2009-06-19 | ジアルキルカーボネートからジアリールカーボネートを製造する方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US9040732B2 (enExample) |
| EP (1) | EP2135857B1 (enExample) |
| JP (1) | JP5596307B2 (enExample) |
| KR (1) | KR101651673B1 (enExample) |
| CN (1) | CN101607908B (enExample) |
| DE (1) | DE102008029514A1 (enExample) |
| ES (1) | ES2540226T3 (enExample) |
| RU (1) | RU2515993C2 (enExample) |
| SG (2) | SG158046A1 (enExample) |
| TW (1) | TWI455923B (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102009053370A1 (de) * | 2009-11-14 | 2011-05-19 | Bayer Materialscience Ag | Verfahren zur Reinigung von Dialkylcarbonaten |
| WO2011067263A1 (en) * | 2009-12-04 | 2011-06-09 | Shell Internationale Research Maatschappij B.V. | Process for preparing diaryl carbonates |
| DE102010006657A1 (de) * | 2010-02-03 | 2011-08-04 | Bayer MaterialScience AG, 51373 | Verfahren zur Herstellung von Dialkylcarbonaten |
| WO2012076532A1 (en) * | 2010-12-08 | 2012-06-14 | Shell Internationale Research Maatschappij B.V. | Process for purifying aryl group containing carbonates |
| EP2679573B1 (en) * | 2012-06-29 | 2017-12-27 | SABIC Global Technologies B.V. | Method and apparatus for the separation of dialkyl carbonate, water and alkanol |
| EP2679572B1 (en) * | 2012-06-29 | 2017-12-13 | SABIC Global Technologies B.V. | Method and apparatus for the production of diaryl carbonate |
| KR101583145B1 (ko) * | 2013-07-18 | 2016-01-07 | 주식회사 엘지화학 | 증류 장치 |
| US9458022B2 (en) * | 2014-03-28 | 2016-10-04 | L'Air Liquide Société Anonyme Pour L'Étude Et L'Exploitation Des Procedes Georges Claude | Process and apparatus for separating NO2 from a CO2 and NO2—containing fluid |
| EP3380450B1 (en) | 2015-11-26 | 2019-10-02 | Shell International Research Maatschappij B.V. | Process for preparing a diaryl carbonate |
| DE102016116078B3 (de) * | 2016-08-29 | 2018-01-04 | Epc Engineering Consulting Gmbh | Verfahren zur Herstellung eines Polycarbonats unter Einsatz einer Strippvorrichtung |
| CN113577814B (zh) * | 2021-08-16 | 2022-10-18 | 四川中蓝国塑新材料科技有限公司 | 一种用于聚碳酸酯工业化生产的碳酸二苯酯回收装置及方法 |
Family Cites Families (48)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE258412C (enExample) | 1911-11-14 | |||
| US3642858A (en) | 1969-02-12 | 1972-02-15 | Dow Chemical Co | Carbonate synthesis from alkylene carbonates |
| US3803201A (en) | 1971-02-22 | 1974-04-09 | Dow Chemical Co | Synthesis of dimethyl carbonate |
| DE2736063A1 (de) | 1977-08-10 | 1979-02-22 | Bayer Ag | Verfahren zur herstellung aromatischer kohlensaeureester |
| DE2736062A1 (de) | 1977-08-10 | 1979-02-22 | Bayer Ag | Verfahren zur herstellung aromatischer kohlensaeureester |
| DE2740243A1 (de) | 1977-09-07 | 1979-03-15 | Bayer Ag | Verfahren zur herstellung von dialkylcarbonaten |
| JPS5463023A (en) | 1977-10-26 | 1979-05-21 | Mitsubishi Chem Ind Ltd | Ester exchange of carbonate |
| JPS54125617A (en) | 1978-03-20 | 1979-09-29 | Mitsubishi Chem Ind Ltd | Ester interchange of carbonate |
| DE3017419A1 (de) | 1980-05-07 | 1981-11-12 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung aromatischer polycarbonate |
| JPS57176932A (en) | 1981-04-24 | 1982-10-30 | Asahi Chem Ind Co Ltd | Preparation of carbonic acid ester |
| DE3302525A1 (de) | 1983-01-26 | 1984-07-26 | Basf Ag, 6700 Ludwigshafen | Destillationskolonne zur destillativen zerlegung eines aus mehreren fraktionen bestehenden zulaufproduktes |
| US4554110A (en) | 1983-12-27 | 1985-11-19 | General Electric Company | Process for the preparation of aromatic carbonates |
| US4552704A (en) | 1983-12-27 | 1985-11-12 | General Electric Company | Process for the production of aromatic carbonates |
| JPH06725B2 (ja) | 1985-01-29 | 1994-01-05 | ダイセル化学工業株式会社 | 炭酸ジフエニルの製造方法 |
| DE3809417A1 (de) | 1988-03-21 | 1989-10-12 | Henkel Kgaa | Verfahren zur kontinuierlichen veresterung von fettsaeuren |
| JPH0710314B2 (ja) | 1987-06-26 | 1995-02-08 | ジューキ株式会社 | ミシンの上下送り量制御装置 |
| JPH07100713B2 (ja) | 1987-10-02 | 1995-11-01 | 財団法人相模中央化学研究所 | １４−フルオロアントラサイクリン誘導体 |
| CA2013689C (en) | 1987-10-05 | 1997-10-28 | Shinsuke Fukuoka | Process for producing diaryl carbonate |
| JPH0193560A (ja) | 1987-10-05 | 1989-04-12 | Asahi Chem Ind Co Ltd | ジアリールカーボネートの製造法 |
| US5034557A (en) | 1988-04-16 | 1991-07-23 | Mitsui Petrochemical Industries, Ltd. | Process for production of aromatic carbonate compound |
| ATE107273T1 (de) * | 1989-12-28 | 1994-07-15 | Asahi Chemical Ind | Kontinuierliches verfahren zur herstellung aromatischer karbonate. |
| DE4006520A1 (de) | 1990-03-02 | 1991-09-05 | Bayer Ag | Verfahren zur herstellung von mindestens eine aromatische estergruppe enthaltenden kohlensaeurediestern |
| DE4036594A1 (de) | 1990-11-16 | 1992-05-21 | Bayer Ag | Verfahren zur herstellung von aromatischen kohlensaeurediestern |
| DE4226755A1 (de) | 1992-08-13 | 1994-02-17 | Bayer Ag | Verfahren zur kontinuierlichen Herstellung von Diarylcarbonaten aus Dialkylcarbonaten |
| DE4226756A1 (de) | 1992-08-13 | 1994-02-17 | Bayer Ag | Verfahren zur Herstellung von Dicarbonaten |
| JP3546098B2 (ja) * | 1995-08-23 | 2004-07-21 | 三菱化学株式会社 | ジアリールカーボネートの連続的製造方法 |
| JP3846926B2 (ja) * | 1995-12-27 | 2006-11-15 | 日本ジーイープラスチックス株式会社 | 芳香族カーボネートの連続的製造方法 |
| DE19914966A1 (de) | 1999-04-01 | 2000-10-05 | Basf Ag | Verfahren zur kontinuierlich betriebenen destillativen Abtrennung eines höherschmelzenden Stoffes |
| US6294684B1 (en) | 1999-12-08 | 2001-09-25 | General Electric Company | Method and apparatus for the continuous production of diaryl carbonates |
| JP2002020351A (ja) | 2000-07-05 | 2002-01-23 | Mitsubishi Gas Chem Co Inc | ジアリールカーボネート製造時の熱回収方法 |
| US6515187B1 (en) * | 2001-10-03 | 2003-02-04 | Atofina Chemicals, Inc. | Process for recovering acrolein or propionaldehyde from dilute aqueous streams |
| JP2004075577A (ja) | 2002-08-13 | 2004-03-11 | Mitsubishi Chemicals Corp | 芳香族カーボネート類の製造方法 |
| AU2003255152A1 (en) | 2002-08-12 | 2004-03-03 | Mitsubishi Chemical Corporation | Process for producing aromatic carbonate |
| US7151189B2 (en) | 2003-06-19 | 2006-12-19 | General Electric Company | Method and apparatus for waste stream recovery |
| US7141641B2 (en) | 2003-06-26 | 2006-11-28 | General Electric Company | Method and apparatus for production of alkyl aryl ether and diaryl carbonate |
| RU2329250C2 (ru) * | 2003-06-27 | 2008-07-20 | Асахи Касеи Кемикалз Корпорейшн | Способ получения ароматического карбоната |
| EA010603B1 (ru) | 2004-06-25 | 2008-10-30 | Асахи Касеи Кемикалз Корпорейшн | Способ промышленного производства ароматического карбоната |
| CN100594208C (zh) | 2004-06-25 | 2010-03-17 | 旭化成化学株式会社 | 芳香族碳酸酯的工业制备方法 |
| EP1767516A4 (en) | 2004-07-13 | 2008-08-13 | Asahi Kasei Chemicals Corp | METHOD FOR THE LARGE MANUFACTURE OF AROMATIC CARBONATE |
| US7777067B2 (en) | 2004-07-13 | 2010-08-17 | Asahi Kasei Chemicals Corporation | Industrial process for production of an aromatic carbonate |
| BRPI0513330A (pt) | 2004-07-14 | 2008-05-06 | Asahi Kasei Chemicals Corp | processo para a produção de um carbonato aromático, e, carbonato aromático |
| JP4224104B2 (ja) | 2004-07-14 | 2009-02-12 | 旭化成ケミカルズ株式会社 | 芳香族カーボネート類を工業的に製造する方法 |
| JP2007326782A (ja) | 2004-09-21 | 2007-12-20 | Asahi Kasei Chemicals Corp | 副生アルコール類の工業的分離装置 |
| CN100554240C (zh) * | 2004-09-27 | 2009-10-28 | 旭化成化学株式会社 | 芳香族碳酸酯的工业制备方法 |
| US7378540B2 (en) * | 2005-10-21 | 2008-05-27 | Catalytic Distillation Technologies | Process for producing organic carbonates |
| JP5344927B2 (ja) * | 2006-11-28 | 2013-11-20 | 旭化成ケミカルズ株式会社 | 高品質芳香族ポリカーボネートを工業的規模で製造する方法 |
| EP1995233A3 (de) * | 2007-05-25 | 2010-06-02 | Bayer MaterialScience AG | Verfahren zur Herstellung von Diaryl- oder Arylalkylcarbonaten aus Dialkylcarbonaten |
| DE102007044033A1 (de) * | 2007-09-14 | 2009-03-19 | Bayer Materialscience Ag | Verfahren zur Herstellung von Diaryl- oder Alkylarylcarbonaten aus Dialkylcarbonaten |
-
2008
- 2008-06-21 DE DE102008029514A patent/DE102008029514A1/de not_active Withdrawn
-
2009
- 2009-06-06 EP EP20090007511 patent/EP2135857B1/de not_active Not-in-force
- 2009-06-06 ES ES09007511.0T patent/ES2540226T3/es active Active
- 2009-06-12 US US12/483,669 patent/US9040732B2/en not_active Expired - Fee Related
- 2009-06-19 KR KR1020090055010A patent/KR101651673B1/ko not_active Expired - Fee Related
- 2009-06-19 SG SG200904220-1A patent/SG158046A1/en unknown
- 2009-06-19 SG SG2013048012A patent/SG192423A1/en unknown
- 2009-06-19 JP JP2009146450A patent/JP5596307B2/ja not_active Expired - Fee Related
- 2009-06-19 TW TW098120528A patent/TWI455923B/zh not_active IP Right Cessation
- 2009-06-19 RU RU2009123374/04A patent/RU2515993C2/ru not_active IP Right Cessation
- 2009-06-22 CN CN200910146211.5A patent/CN101607908B/zh not_active Expired - Fee Related
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