JP2009529549A - 不均一系触媒による水素化を利用する芳香族アミンの製造方法及び装置 - Google Patents

不均一系触媒による水素化を利用する芳香族アミンの製造方法及び装置 Download PDF

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JP2009529549A
JP2009529549A JP2008558673A JP2008558673A JP2009529549A JP 2009529549 A JP2009529549 A JP 2009529549A JP 2008558673 A JP2008558673 A JP 2008558673A JP 2008558673 A JP2008558673 A JP 2008558673A JP 2009529549 A JP2009529549 A JP 2009529549A
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reaction
catalyst
channels
cooling medium
channel
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Japanese (ja)
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JP2009529549A5 (enExample
Inventor
シュテファン・シューベルト
ラルフ・シェレン
レスラウ・ムレクスコ
シュテファン・ロウエ
ペーター・レーナー
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Bayer AG
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Bayer Technology Services GmbH
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/248—Reactors comprising multiple separated flow channels
    • B01J19/249—Plate-type reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/30—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
    • C07C209/32—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
    • C07C209/36—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups by reduction of nitro groups bound to carbon atoms of six-membered aromatic rings in presence of hydrogen-containing gases and a catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00783—Laminate assemblies, i.e. the reactor comprising a stack of plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00835—Comprising catalytically active material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00871—Modular assembly
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00873—Heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/0095—Control aspects
    • B01J2219/00952—Sensing operations
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2451—Geometry of the reactor
    • B01J2219/2453—Plates arranged in parallel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2451—Geometry of the reactor
    • B01J2219/2456—Geometry of the plates
    • B01J2219/2458—Flat plates, i.e. plates which are not corrugated or otherwise structured, e.g. plates with cylindrical shape
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2461—Heat exchange aspects
    • B01J2219/2462—Heat exchange aspects the reactants being in indirect heat exchange with a non reacting heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2476—Construction materials
    • B01J2219/2477—Construction materials of the catalysts
    • B01J2219/2479—Catalysts coated on the surface of plates or inserts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2008558673A 2006-03-14 2007-03-01 不均一系触媒による水素化を利用する芳香族アミンの製造方法及び装置 Pending JP2009529549A (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102006011497A DE102006011497A1 (de) 2006-03-14 2006-03-14 Verfahren und Vorrichtung zur Herstellung von aromatischen Aminen durch eine heterogen katalysierte Hydrierung
PCT/EP2007/001751 WO2007104434A1 (de) 2006-03-14 2007-03-01 Verfahren und vorrichtung zur herstellung von aromatischen aminen durch eine heterogen katalysierte hydrierung

Publications (2)

Publication Number Publication Date
JP2009529549A true JP2009529549A (ja) 2009-08-20
JP2009529549A5 JP2009529549A5 (enExample) 2009-12-10

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ID=38055102

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JP2008558673A Pending JP2009529549A (ja) 2006-03-14 2007-03-01 不均一系触媒による水素化を利用する芳香族アミンの製造方法及び装置

Country Status (8)

Country Link
US (1) US20090093655A1 (enExample)
EP (1) EP2125192A1 (enExample)
JP (1) JP2009529549A (enExample)
CN (1) CN101400438A (enExample)
BR (1) BRPI0708889A2 (enExample)
DE (1) DE102006011497A1 (enExample)
RU (1) RU2008140366A (enExample)
WO (1) WO2007104434A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010260858A (ja) * 2009-04-29 2010-11-18 Bayer Materialscience Ag 芳香族アミンの製造方法

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012160072A1 (de) 2011-05-24 2012-11-29 Basf Se Verfahren zur herstellung von polyisocyanaten aus biomasse
US8933262B2 (en) 2011-05-24 2015-01-13 Basf Se Process for preparing polyisocyanates from biomass

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5566545A (en) * 1978-11-11 1980-05-20 Bayer Ag Catalytic hydrogenation of nitrobenzene
JPH06154588A (ja) * 1992-03-12 1994-06-03 Bayer Ag 流れの方向に短い触媒床を有する固定床反応器
WO2003099429A1 (en) * 2002-05-21 2003-12-04 Battelle Memorial Institute Reactors having varying cross-section, methods of making same, and methods of conducting reactions with varying local contact time
WO2004091771A1 (de) * 2003-04-16 2004-10-28 Uhde Gmbh Mikroreaktor in plattenbauweise mit einem katalysator

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10036602A1 (de) * 2000-07-27 2002-02-14 Cpc Cellular Process Chemistry Mikroreaktor für Reaktionen zwischen Gasen und Flüssigkeiten
DE10110465B4 (de) * 2001-03-05 2005-12-08 Vodafone Pilotentwicklung Gmbh Reaktor
DE10347439A1 (de) * 2003-10-13 2005-05-04 Bayer Materialscience Ag Verfahren zur Herstellung von aromatischen Aminen durch heterogen katalysierte Hydrierung

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5566545A (en) * 1978-11-11 1980-05-20 Bayer Ag Catalytic hydrogenation of nitrobenzene
JPH06154588A (ja) * 1992-03-12 1994-06-03 Bayer Ag 流れの方向に短い触媒床を有する固定床反応器
WO2003099429A1 (en) * 2002-05-21 2003-12-04 Battelle Memorial Institute Reactors having varying cross-section, methods of making same, and methods of conducting reactions with varying local contact time
JP2006508783A (ja) * 2002-05-21 2006-03-16 バッテル メモリアル インスティチュート 変化する断面を有する反応装置、その製造方法および局所的接触時間を変化させて反応を行う方法
WO2004091771A1 (de) * 2003-04-16 2004-10-28 Uhde Gmbh Mikroreaktor in plattenbauweise mit einem katalysator
JP2006523522A (ja) * 2003-04-16 2006-10-19 ウーデ ゲゼルシャフト ミット ベシュレンクテル ハフツング 触媒を備えたプレート構造のマイクロ型反応器

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010260858A (ja) * 2009-04-29 2010-11-18 Bayer Materialscience Ag 芳香族アミンの製造方法

Also Published As

Publication number Publication date
RU2008140366A (ru) 2010-04-20
DE102006011497A1 (de) 2007-09-20
CN101400438A (zh) 2009-04-01
BRPI0708889A2 (pt) 2011-06-28
EP2125192A1 (de) 2009-12-02
US20090093655A1 (en) 2009-04-09
WO2007104434A1 (de) 2007-09-20

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