JP2006528612A - サーモプレート装置を有する反応器中でc3および/またはc4前駆化合物の不均一接触部分酸化により(メタ)アクロレインおよび/または(メタ)アクリル酸を製造する方法 - Google Patents
サーモプレート装置を有する反応器中でc3および/またはc4前駆化合物の不均一接触部分酸化により(メタ)アクロレインおよび/または(メタ)アクリル酸を製造する方法 Download PDFInfo
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Abstract
Description
1個以上の立方形のサーモプレート装置を有し、前記装置はそれぞれ2個以上の長方形の、互いに平行に、間隙を解放して配置されたサーモプレートから形成され、前記間隙に不均一粒子状触媒を充填することができ、前記間隙を流体反応混合物が流動し、反応熱が熱媒体により吸収され、熱媒体はサーモプレートを流動し、その際少なくとも部分的に蒸発し、および
サーモプレート装置の圧力を解放し、前記装置を完全に包囲し、シリンダージャケットおよびフードを有する大部分シリンダー状シェルを有し、前記フードは両方の端部でジャケットを閉鎖し、長手方向の軸がサーモプレートの平面に平行に配列し、および
1個以上の封止部品を有し、前記部品は流体反応混合物が、フードにより境界付けられる反応器内部空間の流動を除いて間隙のみを流動するように配置されている。
Claims (29)
- 反応器中で不均一粒子状触媒の存在でC3および/またはC4前駆化合物から(メタ)アクロレインおよび/または(メタ)アクリル酸を生じる気相部分酸化法であり、前記反応器が
1個以上の立方形のサーモプレート装置(1)を有し、前記装置はそれぞれ2個以上の長方形の、互いに平行に、間隙(3)を解放して配置されたサーモプレート(2)から形成され、前記間隙に不均一粒子状触媒を充填することができ、前記間隙を流体反応混合物が流動し、反応熱が熱媒体により吸収され、熱媒体はサーモプレート(2)を流動し、その際少なくとも部分的に蒸発し、および
サーモプレート装置(1)の圧力を解放し、前記装置を完全に包囲し、シリンダージャケット(4)およびフード(15、16)を有する大部分シリンダー状シェル(4,15,16)を有し、前記フードは両方の端部でジャケットを閉鎖し、長手方向の軸がサーモプレート(2)の平面に平行に配列し、および
1個以上の封止部品(7、23)を有し、前記部品は流体反応混合物が、フード(15,16)により境界付けられる反応器内部空間の流動を除いて、間隙(3)のみを流動するように配置されていることを特徴とする、反応器中で不均一粒子状触媒の存在でC3および/またはC4前駆化合物から(メタ)アクロレインおよび/または(メタ)アクリル酸を生じる気相部分酸化法。 - 反応器がそれぞれ同じ寸法を有する2個以上の立方形サーモプレート装置(1)を有する請求項1記載の方法。
- 反応器が4,7、10または14個のサーモプレート装置(1)を有する請求項2記載の方法。
- サーモプレート(2)がそれぞれ2つの長方形金属シートから形成され、金属シートはその縦方向の面および端部の面でロールシーム溶接により接合され、ロールシームの上の外部に突出する金属シートの縁部がロールシームの外側縁部でまたはロールシーム自体で除去されている請求項1から3までのいずれか1項記載の方法。
- サーモプレート装置(1)が、それぞれ圧力が安定な長方形安定化フレーム(5)内に配置されている請求項1から4までのいずれか1項記載の方法。
- 隣接するサーモプレート装置(1)の長方形安定化フレーム(5)が互いに気密に溶接される請求項5記載の方法。
- 封止部品として保持ベース(7)が用意され、保持ベースがサーモプレート装置(1)と大部分シリンダーシェル(4)の間の中間空間(6)をサーモプレート(1)の下側端部で封止する請求項1から6までのいずれか1項記載の方法。
- 金属シートカバー(8)がサーモプレート装置(1)と大部分シリンダーシェル(4)の間の中間空間(6)をサーモプレート(1)の上側端部で封止する請求項7記載の方法。
- 金属シートカバー(8)がオリフィス(9)を有する請求項8記載の方法。
- シェル(4)のサーモプレート装置(1)の間の中間空間(6)が不活性材料で充填される請求項1から9までのいずれか1項記載の方法。
- 不活性材料が膨張パーライトおよび/または膨張バーミキュライトである請求項10記載の方法。
- サーモプレート装置(1)と大部分シリンダーシェル(4)の間の中間空間(6)にガスを使用して圧力を負荷する請求項1から11までのいずれか1項記載の方法。
- 負荷される圧力が実質的に一定である請求項12記載の方法。
- 圧力の実質的に一定の負荷を窒素の圧力を調節した供給および除去により行う請求項13記載の方法。
- 中間空間(6)に工程に不活性または工程に内在するガス、特に窒素または循環ガスを連続的に供給することにより圧力を負荷する請求項12記載の方法。
- 圧力の負荷に使用されるガスを流体反応混合物とサーモプレート装置(1)からの出口で結合する請求項15記載の方法。
- 保持ベース(7)の中または上に半径方向の膨張の補正装置(10)が備えられている請求項1から16までのいずれか1項記載の方法。
- 金属シートカバー(8)の中または上に軸方向の膨張および/または半径方向の膨張の補正装置(10)が備えられている請求項1から17までのいずれか1項記載の方法。
- サーモプレート装置1個当たり1個以上の熱媒体の分配装置(11)および1個以上の収集装置(12)を使用する請求項1から18までのいずれか1項記載の方法。
- サーモプレート装置1個当たり1個の熱媒体の分配装置(11)および2個の収集装置(12)を使用する請求項1から19までのいずれか1項記載の方法。
- 熱媒体の分配装置および収集装置が均一な寸法を有する請求項1から20までのいずれか1項記載の方法。
- 熱媒体の分配装置(11)および収集装置(12)が刻み目のあるベースに溶接される請求項1から20までのいずれか1項記載の方法。
- 包囲する、大部分シリンダーシェル(4)に対するサーモプレート装置(1)の熱膨張を受け入れるためのそれぞれ1つの補正装置を有する、サーモプレート(2)を流動する熱媒体の分配装置(11)および収集装置(12)が備えられている請求項1から20までのいずれか1項記載の方法。
- 包囲する、大部分シリンダーシェル(4)に対するサーモプレート装置(1)の熱膨張を、サーモプレート(2)を流動する熱媒体の分配装置(11)および収集装置(12)の適当な湾曲した形状の構成の管により受け入れる請求項1から19までのいずれか1項記載の方法。
- サーモプレート装置1個当たり2個の触媒保持格子を使用する請求項1から23までのいずれか1項記載の方法。
- 触媒保持格子を反応器に存在するマンホールにより反応器ジャケットに導入できる請求項1から24までのいずれか1項記載の方法。
- 有利に軸方向の熱膨張を受け入れる1個以上の補正装置(13)が大部分シリンダーシェル(4,15,16)のシリンダージャケット(4)に備えられている請求項1から25までのいずれか1項記載の方法。
- サーモプレート(2)を流動する熱媒体により反応熱を除去し、熱媒体が少なくとも部分的に蒸発する、請求項1から26までのいずれか1項記載の方法。
- 反応器を始動するためのサーモプレート装置(1)の加熱を同じ熱媒体ネットワークから行い、前記ネットワークに、反応の運転の経過中に、少なくとも部分的に蒸発した熱担持媒体により熱が除去される請求項27記載の方法。
Applications Claiming Priority (7)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US48951003P | 2003-07-24 | 2003-07-24 | |
US60/489,510 | 2003-07-24 | ||
DE10333867.5 | 2003-07-24 | ||
DE10333867 | 2003-07-24 | ||
DE102004017150.5 | 2004-04-07 | ||
DE102004017150A DE102004017150A1 (de) | 2004-04-07 | 2004-04-07 | Verfahren zur Herstellung von (Meth)acrolein und/oder (Meth)acrylsäure durch heterogen katalysierte Partialoxidation von C3- und/oder C4-Vorläuferverbindungen in einem Reaktor mit Thermoblechplattenmodulen |
PCT/EP2004/008289 WO2005009609A1 (de) | 2003-07-24 | 2004-07-23 | Verfahren zur herstellung von (meth)acrolein und/oder (meth)acrylsäure durch heterogen katalysierte partialoxidation von c3- und/oder c4-vorläuferverbindungen in einem reaktor mit thermoblechplattenmodulen |
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JP2006528612A true JP2006528612A (ja) | 2006-12-21 |
JP4758895B2 JP4758895B2 (ja) | 2011-08-31 |
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JP2006520811A Expired - Fee Related JP4758895B2 (ja) | 2003-07-24 | 2004-07-23 | サーモプレート装置を有する反応器中でc3および/またはc4前駆化合物の不均一接触部分酸化により(メタ)アクロレインおよび/または(メタ)アクリル酸を製造する方法 |
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EP (1) | EP1663478B1 (ja) |
JP (1) | JP4758895B2 (ja) |
KR (1) | KR101126005B1 (ja) |
BR (1) | BRPI0412854A (ja) |
MY (1) | MY137914A (ja) |
TW (1) | TWI338590B (ja) |
WO (1) | WO2005009609A1 (ja) |
Cited By (1)
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JP2022508538A (ja) * | 2018-10-01 | 2022-01-19 | ヒタチ ゾウセン イノバ エトガス ゲゼルシャフト ミット ベシュレンクテル ハフツング | 固定床装置 |
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CN107519834A (zh) * | 2017-10-20 | 2017-12-29 | 德清四海化工有限公司 | 一种催化剂制备装置 |
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DE3227222C1 (de) * | 1982-07-21 | 1984-05-03 | Keiper Automobiltechnik Gmbh & Co Kg, 5630 Remscheid | Gelenkbeschlag fuer Sitze mit verstellbarer Rueckenlehne,insbesondere Kraftfahrzeugsitze |
FR2539875B1 (fr) * | 1983-01-24 | 1986-03-21 | Ugine Kuhlmann | Procede et appareil de detection de substances toxiques dans l'eau residuaire alimentant une station de traitement biologique |
DE3732081A1 (de) * | 1987-09-24 | 1989-04-06 | Rehau Ag & Co | Plattenfoermiger waermetauscher |
JPH02265513A (ja) * | 1989-04-07 | 1990-10-30 | Nippon Sanso Kk | 断熱容器とその製造方法 |
US5916492A (en) * | 1997-03-27 | 1999-06-29 | Dow Corning Corporation | Structured packing containing liquid-vapor contact column |
BR9913593B1 (pt) * | 1998-09-12 | 2011-08-23 | processo para realização de reações de gás-lìquido e reator de circulação para esse fim. | |
DE19848208A1 (de) | 1998-10-20 | 2000-04-27 | Deg Engineering Gmbh | Reaktor für die katalytische Umsetzung von Reaktionsmedien, insbesondere von gasförmigen Reaktionsmedien |
JP2001038195A (ja) * | 1999-06-28 | 2001-02-13 | Basf Ag | 熱交換板を備えた反応器 |
DE19952964A1 (de) * | 1999-11-03 | 2001-05-10 | Basf Ag | Verfahren zur katalytischen Gasphasenoxidation zu (Meth)Acrolein und/oder (Meth)Acrylsäure |
DE10000584A1 (de) * | 2000-01-10 | 2001-07-12 | Basf Ag | Verfahren zur katalytischen Gasphasenoxidation zu Maleinsäureanhydrid |
DE10011568C1 (de) * | 2000-03-09 | 2001-06-13 | Gea Canzler Gmbh | Wärmetauscherelement |
DE10019381B4 (de) * | 2000-04-19 | 2006-05-18 | Daun, Klaus-Dieter, Dipl.-Ing. | Reaktor für die katalytische Umsetzung von Reaktionsmedien, insbesondere von gasförmigen Reaktionsmedien |
US6497856B1 (en) * | 2000-08-21 | 2002-12-24 | H2Gen Innovations, Inc. | System for hydrogen generation through steam reforming of hydrocarbons and integrated chemical reactor for hydrogen production from hydrocarbons |
DE10108380A1 (de) * | 2001-02-21 | 2002-09-05 | Deg Intense Technologies & Ser | Reaktor zur Durchführung von katalysierten Reaktionen |
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- 2004-07-23 WO PCT/EP2004/008289 patent/WO2005009609A1/de active Application Filing
- 2004-07-23 KR KR1020067001552A patent/KR101126005B1/ko not_active IP Right Cessation
- 2004-07-23 EP EP04763459.7A patent/EP1663478B1/de not_active Expired - Lifetime
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Cited By (2)
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JP2022508538A (ja) * | 2018-10-01 | 2022-01-19 | ヒタチ ゾウセン イノバ エトガス ゲゼルシャフト ミット ベシュレンクテル ハフツング | 固定床装置 |
JP7441231B2 (ja) | 2018-10-01 | 2024-02-29 | ヒタチ ゾウセン イノバ エージー | 固定床装置 |
Also Published As
Publication number | Publication date |
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WO2005009609A1 (de) | 2005-02-03 |
KR20060041273A (ko) | 2006-05-11 |
BRPI0412854A (pt) | 2006-10-03 |
EP1663478B1 (de) | 2016-10-05 |
JP4758895B2 (ja) | 2011-08-31 |
KR101126005B1 (ko) | 2012-03-19 |
MY137914A (en) | 2009-03-31 |
TWI338590B (en) | 2011-03-11 |
EP1663478A1 (de) | 2006-06-07 |
TW200515948A (en) | 2005-05-16 |
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