JP4430672B2 - 熱転写シート装置を有する部分酸化用反応器 - Google Patents
熱転写シート装置を有する部分酸化用反応器 Download PDFInfo
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Description
1個以上の立方形のサーモプレート装置を有し、前記装置はそれぞれ2個以上の長方形の、互いに平行に、間隙を解放して配置されたサーモプレートから形成され、前記間隙に不均一粒子状触媒を充填することができ、前記間隙を流体反応混合物が流動し、反応熱が熱媒体により吸収され、熱媒体はサーモプレートを流動し、サーモプレート(2)がそれぞれ2つの長方形金属シートから形成され、金属シートはその縦方向の面および端部の面でロールシーム溶接により接合され、ロールシームの上の外部に突出する金属シートの縁部がロールシームの外側縁部でまたはロールシーム自体で除去されており、その際少なくとも部分的に蒸発し、および
サーモプレート装置の圧力を解放し、前記装置を完全に包囲し、シリンダージャケットおよびフードを有する大部分シリンダー状シェルを有し、前記フードは両方の端部でジャケットを閉鎖し、長手方向の軸がサーモプレートの平面に平行に配列し、および
1個以上の封止部品を有し、前記部品は流体反応混合物が、フードにより境界付けられる反応器内部空間の流動を除いて間隙のみを流動するように配置されている。
Claims (28)
- 不均一粒子触媒の存在での流体反応混合物の部分酸化用反応器において、前記反応器が1個以上の立方形のサーモプレート装置(1)を有し、前記装置はそれぞれ2個以上の長方形の、互いに平行に、間隙(3)を解放して配置されたサーモプレート(2)から形成され、前記間隙に不均一粒子状触媒を充填することができ、前記間隙を流体反応混合物が流動し、反応熱が熱媒体により吸収され、熱媒体はサーモプレート(2)を流動し、
サーモプレート(2)がそれぞれ2つの長方形金属シートから形成され、金属シートはその縦方向の面および端部の面でロールシーム溶接により接合され、ロールシームの上の外部に突出する金属シートの縁部がロールシームの外側縁部でまたはロールシーム自体で除去されており、その際少なくとも部分的に蒸発し、および
サーモプレート装置(1)の圧力を解放し、前記装置を完全に包囲し、シリンダージャケット(4)およびフード(15、16)を有する大部分シリンダー状シェル(4,15,16)を有し、前記フードは両方の端部でジャケットを閉鎖し、長手方向の軸がサーモプレート(2)の平面に平行に配列し、および
1個以上の封止部品(7、23)を有し、前記部品は流体反応混合物が、フード(15,16)により境界付けられる反応器内部空間の流動を除いて、間隙(3)のみを流動するように配置されていることを特徴とする、流体反応混合物の部分酸化用反応器。 - それぞれ同じ寸法を有する2個以上の立方形サーモプレート装置(1)を有する請求項1記載の反応器。
- 4,7、10または14個のサーモプレート装置(1)を有する請求項2記載の反応器。
- サーモプレート装置(1)が、それぞれ圧力が安定な長方形安定化フレーム(5)内に配置されている請求項1から3までのいずれか1項記載の反応器。
- 隣接するサーモプレート装置(1)の長方形安定化フレーム(5)が溶接され、一緒に封止される請求項4記載の反応器。
- 用意された封止部品が保持ベース(7)であり、保持ベースがサーモプレート装置(1)と大部分シリンダーシェル(4)の間の中間の空間(6)をサーモプレート(1)の下側端部で封止する請求項1から5までのいずれか1項記載の反応器。
- 金属金属シートカバー(8)がサーモプレート装置(1)と大部分がシリンダーシェル(4)の間の中間の空間(6)をサーモプレート(1)の上側端部で封止する請求項6記載の反応器。
- 金属金属シートカバー(8)がオリフィス(9)を有する請求項7記載の反応器。
- サーモプレート装置(1)とシェル(4)の間の中間の空間(6)が不活性材料で充填される請求項1から8までのいずれか1項記載の反応器。
- 不活性材料が膨張パーライトおよび/または膨張バーミキュライトである請求項9記載の反応器。
- サーモプレート装置(1)と大部分がシリンダーシェル(4)の間の中間の空間(6)にガスを使用して圧力を負荷する請求項1から10までのいずれか1項記載の反応器。
- 負荷される圧力が実質的に一定である請求項11記載の反応器。
- 圧力の実質的に一定の負荷を窒素の圧力を調節した供給および除去により行う請求項12記載の反応器。
- 中間の空間(6)に不活性または工程に内在するガス、特に窒素または循環ガスを連続的に供給することにより圧力を負荷する請求項11記載の反応器。
- 圧力の負荷に使用されるガスを流体反応混合物とサーモプレート装置(1)からの出口で結合する請求項14記載の反応器。
- 保持ベース(7)の中または上に半径方向の膨張の補正装置(10)が備えられている請求項6記載の反応器。
- 金属金属シートカバー(8)の中または上に軸方向の膨張および/または半径方向の膨張の補正装置(10)が備えられている請求項7または8記載の反応器。
- サーモプレート装置1個当たり1個以上の熱媒体の分配装置(11)および1個以上の収集装置(12)を使用する請求項1から17までのいずれか1項記載の反応器。
- サーモプレート装置1個当たり1個の熱媒体の分配装置(11)および2個の収集装置(12)を使用する請求項1から18までのいずれか1項記載の反応器。
- 熱媒体の分配装置および収集装置が同じ規格の幅を有する請求項1から19までのいずれか1項記載の反応器。
- 熱媒体の分配装置(11)および収集装置(12)が刻み目のあるベースに溶接される請求項1から19までのいずれか1項記載の反応器。
- 包囲する、大部分シリンダーシェル(4)に対するサーモプレート装置(1)の熱膨張を調節するための補正を有する、サーモプレート(2)を流動する熱媒体の分配装置(11)および収集装置(12)が備えられている請求項1から19までのいずれか1項記載の反応器。
- 包囲する、大部分シリンダーシェル(4)に対するサーモプレート装置(1)の熱膨張を、サーモプレート(2)を流動する熱媒体の分配装置(11)および収集装置(12)の適当な湾曲した形状の構成の管により調節する請求項1から18までのいずれか1項記載の反応器。
- サーモプレート装置1個当たり2個の触媒保持格子を使用する請求項1から22までのいずれか1項記載の反応器。
- 触媒保持格子を反応器に存在するマンホールにより反応器ジャケットに導入できる請求項1から23までのいずれか1項記載の反応器。
- 有利に軸方向の熱膨張を調節する1個以上の補正装置(13)が大部分シリンダーシェル(4,15,16)のシリンダージャケット(4)に備えられている請求項1から24までのいずれか1項記載の反応器。
- サーモプレート(2)を流動する熱媒体により反応熱を除去し、熱媒体が少なくとも部分的に蒸発する、流体反応混合物の部分酸化を実施するための請求項1から25までのいずれか1項記載の反応器を使用する方法。
- 反応器を始動するサーモプレート装置(1)を同じ熱媒体ネットワークにより加熱し、反応の運転の経過中に、前記ネットワークに、少なくとも部分的に蒸発した熱担持媒体によって熱が除去される請求項27記載の方法。
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US48950503P | 2003-07-24 | 2003-07-24 | |
DE10333866 | 2003-07-24 | ||
DE200410017151 DE102004017151A1 (de) | 2004-04-07 | 2004-04-07 | Reaktor für Partialoxidationen mit Thermoblechplattenmodulen |
PCT/EP2004/008151 WO2005009608A1 (de) | 2003-07-24 | 2004-07-21 | Reaktor für partialoxidationen mit thermoblechplattenmodulen |
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JP4430672B2 true JP4430672B2 (ja) | 2010-03-10 |
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JP (1) | JP4430672B2 (ja) |
KR (1) | KR101125883B1 (ja) |
CN (1) | CN1826173B (ja) |
BR (1) | BRPI0412785B1 (ja) |
CA (1) | CA2532646C (ja) |
MX (1) | MXPA06000337A (ja) |
MY (1) | MY150013A (ja) |
WO (1) | WO2005009608A1 (ja) |
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WO2006097904A2 (en) * | 2005-03-17 | 2006-09-21 | Sasol Technology (Proprietary) Limited | Plate-type fluid bed reactor |
KR100787173B1 (ko) * | 2006-11-10 | 2007-12-21 | 연세대학교 산학협력단 | 금속을 이용하는 산화 반응기 |
ES2428793T3 (es) * | 2007-10-01 | 2013-11-11 | Deg Engineering Gmbh | Reactor o intercambiador de calor con espaciadores y termochapas para la realización de reacciones con un fuerte tono térmico |
FR2922124B1 (fr) * | 2007-10-10 | 2010-11-05 | Inst Francais Du Petrole | Reacteur en lit fixe a couches minces pour le traitement chimique de solide catalytique finement divise |
JP5239667B2 (ja) * | 2008-09-16 | 2013-07-17 | 三菱化学株式会社 | プレート式反応器及びそれを用いる反応生成物の製造方法 |
DE102010040923A1 (de) | 2010-09-16 | 2012-03-22 | Basf Se | Verfahren zur Herstellung von Acrylsäure aus Ethanol und Formaldehyd |
DE102010040921A1 (de) | 2010-09-16 | 2012-03-22 | Basf Se | Verfahren zur Herstellung von Acrylsäure aus Methanol und Essigsäure |
DE102010048405A1 (de) | 2010-10-15 | 2011-05-19 | Basf Se | Verfahren zum Langzeitbetrieb einer heterogen katalysierten partiellen Gasphasenoxidation von Proben zu Acrolein |
JP5795994B2 (ja) * | 2012-07-09 | 2015-10-14 | 住友精密工業株式会社 | 熱交換器 |
EP2901071B1 (de) * | 2012-09-18 | 2016-08-17 | Basf Se | Verfahren und anlage zum aufheizen von erdgas |
US20140121403A1 (en) | 2012-10-31 | 2014-05-01 | Celanese International Corporation | Integrated Process for the Production of Acrylic Acids and Acrylates |
US9120743B2 (en) | 2013-06-27 | 2015-09-01 | Celanese International Corporation | Integrated process for the production of acrylic acids and acrylates |
DE102016005999A1 (de) * | 2016-05-18 | 2017-11-23 | Universität Paderborn | Kissenplatten-Wärmeübertrager |
CN113405381B (zh) * | 2021-06-24 | 2022-12-27 | 中航工程集成设备有限公司 | 一种分块圆形换热装置及换热器 |
EP4374957A1 (de) * | 2022-11-25 | 2024-05-29 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Reaktor und herstellungsverfahren dafür |
EP4374958A1 (de) * | 2022-11-25 | 2024-05-29 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Reaktor und herstellungsverfahren dafür |
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DE3227222C1 (de) * | 1982-07-21 | 1984-05-03 | Keiper Automobiltechnik Gmbh & Co Kg, 5630 Remscheid | Gelenkbeschlag fuer Sitze mit verstellbarer Rueckenlehne,insbesondere Kraftfahrzeugsitze |
US5916492A (en) * | 1997-03-27 | 1999-06-29 | Dow Corning Corporation | Structured packing containing liquid-vapor contact column |
KR100569622B1 (ko) * | 1998-09-12 | 2006-04-11 | 데구사 아게 | 기체-액체 반응의 수행방법 및 상응하는 유동 반응기 |
DE19848208A1 (de) * | 1998-10-20 | 2000-04-27 | Deg Engineering Gmbh | Reaktor für die katalytische Umsetzung von Reaktionsmedien, insbesondere von gasförmigen Reaktionsmedien |
JP2001038195A (ja) * | 1999-06-28 | 2001-02-13 | Basf Ag | 熱交換板を備えた反応器 |
DE19952964A1 (de) * | 1999-11-03 | 2001-05-10 | Basf Ag | Verfahren zur katalytischen Gasphasenoxidation zu (Meth)Acrolein und/oder (Meth)Acrylsäure |
DE10019381B4 (de) * | 2000-04-19 | 2006-05-18 | Daun, Klaus-Dieter, Dipl.-Ing. | Reaktor für die katalytische Umsetzung von Reaktionsmedien, insbesondere von gasförmigen Reaktionsmedien |
EP1153653A1 (en) | 2000-05-11 | 2001-11-14 | Methanol Casale S.A. | Reactor for exothermic or endothermic heterogeneous reactions |
US6497856B1 (en) * | 2000-08-21 | 2002-12-24 | H2Gen Innovations, Inc. | System for hydrogen generation through steam reforming of hydrocarbons and integrated chemical reactor for hydrogen production from hydrocarbons |
DE10108380A1 (de) * | 2001-02-21 | 2002-09-05 | Deg Intense Technologies & Ser | Reaktor zur Durchführung von katalysierten Reaktionen |
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JP2006528543A (ja) | 2006-12-21 |
WO2005009608A1 (de) | 2005-02-03 |
MY150013A (en) | 2013-11-15 |
ZA200600576B (en) | 2007-01-31 |
CA2532646C (en) | 2012-09-11 |
BRPI0412785B1 (pt) | 2014-11-18 |
BRPI0412785A (pt) | 2006-09-26 |
EP1651344A1 (de) | 2006-05-03 |
MXPA06000337A (es) | 2006-03-30 |
KR101125883B1 (ko) | 2012-03-21 |
KR20060059972A (ko) | 2006-06-02 |
CA2532646A1 (en) | 2005-02-03 |
EP1651344B1 (de) | 2016-10-19 |
CN1826173A (zh) | 2006-08-30 |
CN1826173B (zh) | 2011-05-25 |
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