JP2006511687A - 熱硬化性複合材組成物、方法、及び物品 - Google Patents
熱硬化性複合材組成物、方法、及び物品 Download PDFInfo
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- JP2006511687A JP2006511687A JP2005508292A JP2005508292A JP2006511687A JP 2006511687 A JP2006511687 A JP 2006511687A JP 2005508292 A JP2005508292 A JP 2005508292A JP 2005508292 A JP2005508292 A JP 2005508292A JP 2006511687 A JP2006511687 A JP 2006511687A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K11/00—Use of ingredients of unknown constitution, e.g. undefined reaction products
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- Health & Medical Sciences (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
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- Compositions Of Macromolecular Compounds (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Abstract
Description
当技術分野で公知の熱硬化性成形用組成物は一般に無機の充填材及び/又は繊維を含有する熱硬化性樹脂である。加熱すると、熱硬化性モノマーは最初、その充填材含有モノマー組成物を溶融加工して物品を成形することができるように十分に低い粘度を示す。さらに加熱すると、熱硬化性モノマーは反応し硬化して高い剛性を有する硬い樹脂を形成する。
Q(J−K)y
式中、Qは一価、二価又は多価フェノールの残基、好ましくは一価又は二価フェノールの残基、さらに好ましくは一価フェノールの残基であり、yは1〜100であり、Jは次式を有する繰返し構造単位からなる。
インターカレーションすることができれば使用できる。1種以上のかかる材料の混合物も使用できる。
50〜150ミリ当量である。特に好ましいのは、モンモリロナイト、ノントロナイト、バイデライト、ヴォルコンスキー石、ヘクトライト、サポナイト、ソーコナイト、マガディアイト、及びケニアイトのような無機層状ケイ酸塩であり、ヘクトライト及びモンモリロナイトは材料100グラム当たり20〜150ミリ当量有する。好ましい膨潤性層状無機材料は式単位当たり0.2〜1.2電荷の範囲の負電荷を層上に有する無機層状ケイ酸塩であり、最も好ましいのは式単位当たり0.2〜0.9電荷の範囲の負電荷を層上に有し、それと釣り合った数の交換可能な陽イオンを層間空間に有する無機層状ケイ酸塩である。
(−−)nSiR(4−n−m)R1 m
式中、(−−)は層状材料の表面との原子価結合であり、mは0、1又は2であり、nは1、2、又は3であるが、mとnの和は3に等しく、R1は非加水分解性の有機基(例えば、アルキル、アルコキシアルキル、アルキルアリール、アリールアルキル、及びアルコキシアリール)であり、Rは各々同一であるか又は異なり、硬化性組成物の1以上の成分と反応性の有機基である。R基の代表例としては、アミノ、カルボキシ、アシルハロゲン化物、アシルオキシ、ヒドロキシ、イソシアナト、ウレイド、ハロ、エポキシ、エピクロロヒドリル、などがある。好ましいオルガノシラン介在化合物としては、国際公開第93/11190号第9〜21頁に開示されている長鎖枝分かれ第四アンモニウム塩及び/又は適切に官能化されたオルガノシラン化合物がある。
Claims (10)
- 官能化ポリ(アリーレンエーテル)、オレフィン性不飽和モノマー及びナノ充填材を含んでなる硬化性組成物。
- 官能化ポリ(アリーレンエーテル)が次式の構造を有する封鎖ポリ(アリーレンエーテル)である、請求項1記載の組成物。
Q(J−K)y
式中、Qは一価、二価又は多価のフェノールの残基であり、yは1〜100であり、Jは次式を有する繰返し構造単位からなる。
- Qが一価フェノールの残基である、請求項2記載の組成物。
- 官能化ポリ(アリーレンエーテル)及びオレフィン性不飽和モノマーの合計100重量部当たり約1〜約90重量部の官能化ポリ(アリーレンエーテル)を含んでいる、請求項1乃至請求項3いずれか1項記載の組成物。
- オレフィン性不飽和モノマーがアルケニル芳香族モノマー、アクリロイルモノマー、アリルモノマー、又はこれらの混合物からなる、請求項1乃至請求項4いずれか1項記載の組成物。
- 官能化ポリ(アリーレンエーテル)及びオレフィン性不飽和モノマーの合計100重量部当たり約10〜約99重量部のオレフィン性不飽和モノマーを含んでいる、請求項1乃至請求項5いずれか1項記載の組成物。
- ナノ充填材が、金属酸化物、金属炭化物、サーメット材料、セラミック、ガラス、ペロブスカイト、層状無機材料、繊維状無機材料、及びこれらの組合せから選択される、請求項1乃至請求項6いずれか1項記載の組成物。
- 組成物の総重量を基準にして約0.5〜約80重量%のナノ充填材を含んでいる、請求項1乃至請求項7いずれか1項記載の組成物。
- さらに、100℃以下のガラス転移温度を有するポリマー状添加剤を含んでいる、請求項1乃至請求項8いずれか1項記載の組成物。
- 請求項1乃至請求項9いずれか1項記載の組成物を硬化させることにより形成された硬化組成物。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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US31980502P | 2002-12-20 | 2002-12-20 | |
US31987203P | 2003-01-16 | 2003-01-16 | |
PCT/US2003/039894 WO2005019340A1 (en) | 2002-12-20 | 2003-12-16 | Thermoset composite composition, method, and article |
Publications (1)
Publication Number | Publication Date |
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JP2006511687A true JP2006511687A (ja) | 2006-04-06 |
Family
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Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2005508292A Withdrawn JP2006511687A (ja) | 2002-12-20 | 2003-12-16 | 熱硬化性複合材組成物、方法、及び物品 |
Country Status (5)
Country | Link |
---|---|
US (1) | US7250477B2 (ja) |
EP (1) | EP1578868A1 (ja) |
JP (1) | JP2006511687A (ja) |
AU (1) | AU2003304442A1 (ja) |
WO (1) | WO2005019340A1 (ja) |
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-
2003
- 2003-12-11 US US10/733,062 patent/US7250477B2/en active Active
- 2003-12-16 JP JP2005508292A patent/JP2006511687A/ja not_active Withdrawn
- 2003-12-16 WO PCT/US2003/039894 patent/WO2005019340A1/en active Application Filing
- 2003-12-16 AU AU2003304442A patent/AU2003304442A1/en not_active Abandoned
- 2003-12-16 EP EP03816946A patent/EP1578868A1/en not_active Withdrawn
Also Published As
Publication number | Publication date |
---|---|
US7250477B2 (en) | 2007-07-31 |
WO2005019340A1 (en) | 2005-03-03 |
EP1578868A1 (en) | 2005-09-28 |
US20040122153A1 (en) | 2004-06-24 |
AU2003304442A1 (en) | 2005-03-10 |
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