JP2006346800A - Vitrified bond grindstone and method of producing the same - Google Patents

Vitrified bond grindstone and method of producing the same Download PDF

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JP2006346800A
JP2006346800A JP2005174979A JP2005174979A JP2006346800A JP 2006346800 A JP2006346800 A JP 2006346800A JP 2005174979 A JP2005174979 A JP 2005174979A JP 2005174979 A JP2005174979 A JP 2005174979A JP 2006346800 A JP2006346800 A JP 2006346800A
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vitrified bond
bond material
grindstone
vitrified
impregnated
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JP4734041B2 (en
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Ryogo Umaji
良吾 馬路
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Disco Corp
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Disco Abrasive Systems Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24DTOOLS FOR GRINDING, BUFFING OR SHARPENING
    • B24D3/00Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents
    • B24D3/02Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent
    • B24D3/04Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent and being essentially inorganic
    • B24D3/14Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent and being essentially inorganic ceramic, i.e. vitrified bondings
    • B24D3/18Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent and being essentially inorganic ceramic, i.e. vitrified bondings for porous or cellular structure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24DTOOLS FOR GRINDING, BUFFING OR SHARPENING
    • B24D18/00Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for
    • B24D18/0054Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for by impressing abrasive powder in a matrix
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24DTOOLS FOR GRINDING, BUFFING OR SHARPENING
    • B24D7/00Bonded abrasive wheels, or wheels with inserted abrasive blocks, designed for acting otherwise than only by their periphery, e.g. by the front face; Bushings or mountings therefor
    • B24D7/06Bonded abrasive wheels, or wheels with inserted abrasive blocks, designed for acting otherwise than only by their periphery, e.g. by the front face; Bushings or mountings therefor with inserted abrasive blocks, e.g. segmental
    • B24D7/066Grinding blocks; their mountings or supports
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00Materials not provided for elsewhere
    • C09K3/14Anti-slip materials; Abrasives
    • C09K3/1409Abrasive particles per se
    • C09K3/1418Abrasive particles per se obtained by division of a mass agglomerated by sintering

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Polishing Bodies And Polishing Tools (AREA)

Abstract

<P>PROBLEM TO BE SOLVED: To provide a vitrified bond grindstone which effectively grinds even a difficult-to-machine material without frequent dressing, to thereby protect a workpiece from degrading, and to provide a method of producing the vitrified bond grindstone. <P>SOLUTION: According to the method, flowable abrasive grain 2 which is obtained by kneading a vitrified bond material containing at least SiO<SB>2</SB>as a main ingredient, an organic bond material, abrasive grain, and liquid together, is impregnated into a sponge member 1 formed of a resin, and the organic bond material and the sponge member are oxidized, followed by sintering the abrasive grain with the vitrified bond material, to thereby form the vitrified bond grindstone having pores. By virtue of formation of the pores, the vitrified bond grindstone easily generates a self-edging function, and therefore frequent dressing is dispensed with, to thereby improve the productivity. Thus by using the vitrified bond grindstone, a ground surface of the workpiece is free from surface burning or tears, and the quality of the workpiece is improved. <P>COPYRIGHT: (C)2007,JPO&INPIT

Description

本発明は、自生発刃作用が良好なビトリファイドボンド砥石及びその製造方法に関するものである。   The present invention relates to a vitrified bond grindstone with a good self-generated blade action and a method for producing the same.

IC、LSI等のデバイスが表面に複数形成されたウェーハは、裏面が研削されて所定の厚さに形成された後に、ダイシング装置等によって個々のデバイスに分割され、各種電子機器に利用されている。   A wafer on which a plurality of devices such as IC and LSI are formed on the front surface is ground into a predetermined thickness by grinding the back surface, and then divided into individual devices by a dicing apparatus or the like and used for various electronic devices. .

研削の対象となるウェーハは、シリコン、窒化珪素、ガリウム砒素、サファイア、リチウムタンタレート、炭化珪素等で形成されている。一方、研削砥石には、ビトリファイドボンド砥石、レジンボンド砥石、メタルボンド砥石等があり、これらの砥石の中からウェーハの材料に適した砥石が選択されて研削に使用される。窒化珪素、サファイア、炭化珪素は硬度が高いため、これらの材料によって形成されるウェーハを研削する際には、ビトリファイドボンド砥石やメタルボンド砥石等の、ダイヤモンド砥粒が強固に保持された構成の砥石が用いられる(例えば特許文献1参照)。   A wafer to be ground is formed of silicon, silicon nitride, gallium arsenide, sapphire, lithium tantalate, silicon carbide, or the like. On the other hand, there are vitrified bond grindstones, resin bond grindstones, metal bond grindstones, and the like as grinding grindstones. A grindstone suitable for the material of the wafer is selected from these grindstones and used for grinding. Since silicon nitride, sapphire, and silicon carbide have high hardness, when grinding a wafer formed of these materials, a grindstone with a structure in which diamond abrasive grains are firmly held, such as vitrified bond grindstone and metal bond grindstone Is used (see, for example, Patent Document 1).

特開2003−136410号公報JP 2003-136410 A

しかし、ビトリファイドボンドやメタルボンドによって砥粒が強固に保持された構成の砥石には自生発刃作用が生じにくいことから、比較的短時間で目詰まりを起こし、頻繁にドレッシングを行う必要があるため、生産性が低いという問題がある。   However, since the self-generated blade action is unlikely to occur on a grindstone with a structure in which abrasive grains are firmly held by vitrified bond or metal bond, clogging occurs in a relatively short time and frequent dressing needs to be performed. There is a problem that productivity is low.

また、自生発刃作用が生じにくいことに起因して、被研削物の研削面に面焼けやムシレといった現象が生じ、被研削物の品質を低下させるという問題もある。   In addition, due to the fact that the self-generated blade action is less likely to occur, there is a problem that phenomena such as surface burn and stuffiness occur on the ground surface of the workpiece and the quality of the workpiece is reduced.

そこで、本発明が解決しようとする課題は、難削材であっても頻繁にドレッシングすることなく効率良く研削し、被研削物の品質を低下させないようにすることである。   Therefore, the problem to be solved by the present invention is to efficiently grind even difficult-to-cut materials without frequent dressing so as not to deteriorate the quality of the object to be ground.

第一の発明は、気孔を有するビトリファイドボンド砥石であって、少なくともSiOを主成分とするビトリファイドボンド材と有機物ボンド材と砥粒と液体とを混練した流動性砥粒を樹脂で形成されたスポンジ部材に含浸させ、有機物ボンド材とスポンジ部材とを酸化させると共に砥粒を該ビトリファイドボンド材で焼結したことを特徴とする。 The first invention is a vitrified bond grindstone having pores, wherein fluidized abrasive grains obtained by kneading a vitrified bond material mainly composed of at least SiO 2 , an organic bond material, abrasive grains, and a liquid are formed of a resin. A sponge member is impregnated to oxidize the organic bond material and the sponge member and to sinter the abrasive grains with the vitrified bond material.

第二の発明は、気孔を有するビトリファイドボンド砥石の製造方法であって、少なくともSiOを主成分とするビトリファイドボンド材と有機物ボンド材と砥粒と液体とを混練して流動性砥粒を形成し、気孔を有する樹脂で形成されたスポンジ部材に流動性砥粒を含浸させて含浸スポンジ体を構成する含浸スポンジ体形成工程と、含浸スポンジ体を構成する液体を蒸発させると共に有機物ボンド材を固化させる固化工程と、固化工程後の含浸スポンジ体を焼結して有機物ボンド材とスポンジ部材とを酸化させると共にビトリファイドボンド材によって砥粒を焼結させて気孔を有する焼結体を形成する焼結工程とから構成されることを特徴とする。 A second invention is a method for producing a vitrified bond grindstone having pores, wherein a flowable abrasive is formed by kneading at least a SiO 2 based vitrified bond material, an organic bond material, an abrasive and a liquid. And impregnating sponge body formed by impregnating fluid abrasive grains into a sponge member made of resin having pores, and forming an impregnated sponge body, and evaporating the liquid constituting the impregnated sponge body and solidifying the organic bond material Sintering to form a sintered body having pores by sintering the impregnated sponge body after the solidifying process, oxidizing the organic bond material and the sponge member, and sintering the abrasive grains by vitrified bond material It is characterized by comprising a process.

含浸スポンジ体形成工程において、砥粒は粒径2μm以下のダイヤモンド砥粒にグリーンカーボランダム、ホワイトアランダムのフィラーが混入されて構成されることが好ましい。また、含浸スポンジ体形成工程において、液体は重量比55%の水と重量比10%のアルコールとで構成され、有機物ボンド材は重量比5%のアクリル系ボンド材であることが好ましい。   In the impregnation sponge body forming step, the abrasive grains are preferably constituted by mixing diamond abrasive grains having a particle size of 2 μm or less with green carborundum or white alundum filler. In the impregnated sponge body forming step, the liquid is preferably composed of water having a weight ratio of 55% and alcohol having a weight ratio of 10%, and the organic bond material is preferably an acrylic bond material having a weight ratio of 5%.

固化工程においては、含浸スポンジ体を50°Cで2時間加熱して液体を蒸発させ、有機物ボンド材を120°Cで2時間加熱して焼結させることが好ましい。   In the solidification step, the impregnated sponge body is preferably heated at 50 ° C. for 2 hours to evaporate the liquid, and the organic bond material is preferably heated at 120 ° C. for 2 hours to be sintered.

焼結工程においては、固化工程後の含浸スポンジ体を400°Cで1時間焼結して有機物ボンド材とスポンジ部材とを酸化させ、700°Cで4時間焼結して焼結体を形成することが好ましい。   In the sintering process, the impregnated sponge body after the solidification process is sintered at 400 ° C. for 1 hour to oxidize the organic bond material and the sponge member, and sintered at 700 ° C. for 4 hours to form a sintered body. It is preferable to do.

焼結工程後は、焼結体を切削ブレードで切削して整形し、研削ホイールに固着される砥石とすることがある。   After the sintering step, the sintered body may be cut and shaped with a cutting blade to form a grindstone that is fixed to the grinding wheel.

本発明では、スポンジ部材に流動性砥粒を含浸させて焼結することにより、内部に気孔を有するビトリファイドボンド砥石が構成されるため、気孔により砥粒が脱落しやすくなり、自生発刃作用が生じやすい。したがって、目詰まりを起こしにくく、ドレッシングを頻繁に行う必要がないため、難削材でも効率良く研削することができる。また、自生発刃作用が良好であることから、被研削物の研削面に面焼けやムシレが生じず、被研削物の品質を向上させることができる。   In the present invention, a vitrified bond grindstone having pores is formed by impregnating the sponge member with fluid abrasive grains and sintering, so that the abrasive grains are easily dropped by the pores, and the self-generated blade action is achieved. Prone to occur. Therefore, clogging is unlikely to occur, and it is not necessary to perform dressing frequently, so even difficult-to-cut materials can be ground efficiently. In addition, since the self-generated blade action is good, the surface of the object to be ground is not burnt or blurred, and the quality of the object to be ground can be improved.

最初に、SiOを主成分とするビトリファイドボンド材と、アクリル樹脂等からなる有機物ボンド材と、砥粒と、液体とを混練して流動性砥粒を形成する。砥粒としてはダイヤモンド砥粒が代表的なものとして挙げられる。グリーンカーボランダム(緑色炭化珪素質)やホワイトアランダム(白色アルミナ質)等のフィラーを混入させてもよい。液体としては水やアルコールがある。 First, a fluidized abrasive grain is formed by kneading a vitrified bond material mainly composed of SiO 2 , an organic bond material made of an acrylic resin or the like, abrasive grains, and a liquid. As an abrasive grain, a diamond abrasive grain is mentioned as a typical thing. A filler such as green carborundum (green silicon carbide) or white alundum (white alumina) may be mixed. Liquids include water and alcohol.

そして、図1に示すようにウレタン等の樹脂で形成され気孔を有するスポンジ部材1に上記流動性砥粒を含浸させて含浸スポンジ体を形成する(含浸スポンジ体形成工程)。例えば、図2に示すように、流動性砥粒2を容器3に貯めておき、その流動性砥粒2にスポンジ部材1を浸漬することによって、スポンジ部材1に流動性砥粒を含浸させる。   Then, as shown in FIG. 1, an impregnated sponge body is formed by impregnating the sponge member 1 formed of a resin such as urethane and having pores with the fluid abrasive grains (impregnation sponge body forming step). For example, as shown in FIG. 2, the fluid abrasive 2 is stored in a container 3, and the sponge member 1 is immersed in the fluid abrasive 2 to impregnate the sponge member 1 with the fluid abrasive.

次に、流動性砥粒2を含浸したスポンジ部材1を構成する液体を加熱により蒸発させ、含浸スポンジ体に含まれる有機物ボンド材を固化させる(固化工程)。そして更に、固化工程によって液体が蒸発し有機物ボンド材が固化した含浸スポンジ体を焼結し、有機物ボンド材とスポンジ部材とを酸化させると共に、ビトリファイドボンド材によって砥粒を焼結させる。そうすると、気孔を有する焼結体が形成され、この焼結体がビトリファイドボンド砥石となる。   Next, the liquid constituting the sponge member 1 impregnated with the flowable abrasive grains 2 is evaporated by heating to solidify the organic bond material contained in the impregnated sponge body (solidification step). Further, the impregnated sponge body in which the liquid is evaporated and the organic bond material is solidified in the solidification step is sintered, the organic bond material and the sponge member are oxidized, and the abrasive grains are sintered by the vitrified bond material. Then, a sintered body having pores is formed, and this sintered body becomes a vitrified bond grindstone.

例えば図3に示すように、形成されたビトリファイドボンド砥石4は、高速回転する切削ブレード5を切削ライン6に沿って縦横に切り込ませて個片化することにより整形され、複数のセグメント状ビトリファイドボンド砥石7となる。   For example, as shown in FIG. 3, the formed vitrified bond grindstone 4 is shaped by cutting a cutting blade 5 that rotates at high speed vertically and horizontally along a cutting line 6 into pieces, and a plurality of segmented vitrified particles are formed. The bond grindstone 7 is obtained.

そして、複数のセグメント状ビトリファイドボンド砥石7は、例えば図4に示す研削ホイール814の下面に複数固着される。そして、この研削ホイール814は、例えば図5に示す研削装置8に用いられる。   A plurality of segmented vitrified bond grindstones 7 are fixed to the lower surface of the grinding wheel 814 shown in FIG. 4, for example. And this grinding wheel 814 is used for the grinding apparatus 8 shown, for example in FIG.

この研削装置8は、被研削物を保持するチャックテーブル80と、チャックテーブル80に保持された被研削物に対して研削加工を施す研削手段81とを備えている。研削手段81は、ハウジング810によって回転可能に支持され垂直方向の軸心を有するスピンドル811の上端にモータ812が連結されると共に、スピンドル811の下端に設けられたホイールマウント813に研削ホイール814が装着された構成となっている。研削ホイール814には、セグメント状ビトリファイドボンド砥石7が複数固着されており、モータ812の回転によって研削ホイール814も回転する構成となっている。   The grinding apparatus 8 includes a chuck table 80 that holds an object to be ground, and a grinding unit 81 that performs grinding on the object to be ground held on the chuck table 80. The grinding means 81 is rotatably supported by a housing 810, and a motor 812 is connected to the upper end of a spindle 811 having a vertical axis, and a grinding wheel 814 is attached to a wheel mount 813 provided at the lower end of the spindle 811. It has been configured. A plurality of segmented vitrified bond grindstones 7 are fixed to the grinding wheel 814, and the grinding wheel 814 is also rotated by the rotation of the motor 812.

ハウジング810は、昇降板820に連結された支持部821によって支持されており、昇降板820は、垂直方向に配設されたガイドレール822に摺接すると共に、内部のナット(図示せず)が垂直方向に配設されたボールネジ823に螺合している。ボールネジ823の一端にはパルスモータ824が連結されており、パルスモータ824の回動によってボールネジ823が回動するのに伴い昇降板820がガイドレール822にガイドされて昇降し、研削手段81も昇降する構成となっている。   The housing 810 is supported by a support portion 821 connected to the elevating plate 820. The elevating plate 820 is in sliding contact with a guide rail 822 arranged in the vertical direction, and an internal nut (not shown) is vertical. Screwed into a ball screw 823 disposed in the direction. A pulse motor 824 is connected to one end of the ball screw 823. As the ball screw 823 is rotated by the rotation of the pulse motor 824, the elevating plate 820 is guided by the guide rail 822, and the grinding means 81 is also moved up and down. It is the composition to do.

図示の例のように表面にデバイス保護用の保護テープTが貼着されたウェーハWの裏面を研削する場合は、保護テープTが貼着された表面側がチャックテーブル80に保持される。そして、チャックテーブル80が水平方向に移動して研削手段81の直下に位置付けられ、チャックテーブル80が回転すると共に、研削ホイール814が回転しながら研削手段81が下降することにより、回転するセグメント状ビトリファイドボンド砥石7がウェーハWの裏面に接触して当該裏面が研削される。   When grinding the back surface of the wafer W having the protective tape T for protecting the device attached to the surface as in the illustrated example, the front surface side to which the protective tape T is attached is held by the chuck table 80. Then, the chuck table 80 moves in the horizontal direction and is positioned immediately below the grinding means 81. The chuck table 80 rotates, and the grinding means 81 descends while the grinding wheel 814 rotates, so that the segmented vitrified rotates. The bond grindstone 7 contacts the back surface of the wafer W and the back surface is ground.

セグメント状ビトリファイドボンド砥石7は、スポンジ部材に流動性砥粒を含浸させ焼結して形成されているため、内部には多数の気孔が形成されている。したがって、砥粒が脱落しやすく、自生発刃作用が良好であるため、ウェーハWがサファイアや炭化珪素等の難削材により形成されている場合でも、効率良く研削することができる。また、自生発刃作用が良好であることから、ウェーハの被研削面に面焼けやムシレが生じず、ウェーハの品質を向上させることができる。   Since the segmented vitrified bond grindstone 7 is formed by impregnating and sintering a flowable abrasive grain in a sponge member, a large number of pores are formed inside. Therefore, since the abrasive grains are easy to fall off and the self-generated blade action is good, even when the wafer W is formed of a difficult-to-cut material such as sapphire or silicon carbide, it can be efficiently ground. In addition, since the self-generated blade action is good, the surface to be ground of the wafer is not burnt or blurred, and the quality of the wafer can be improved.

なお、チャックテーブル80を研削してチャックテーブル80の上面とセグメント状ビトリファイドボンド砥石7の下面(研削面)とを一致させるセルフグラインドの場合においては、チャックテーブル80が炭化珪素等の難削材で形成されていても、チャックテーブル80を効率良く研削することができる。   In the case of self-grinding in which the chuck table 80 is ground so that the upper surface of the chuck table 80 and the lower surface (grinding surface) of the segmented vitrified bond grindstone 7 are aligned, the chuck table 80 is made of a difficult-to-cut material such as silicon carbide. Even if formed, the chuck table 80 can be ground efficiently.

ビトリファイドボンド砥石の製造方法の例を以下に示す。まず、含浸スポンジ体形成工程においては、それぞれ体積比で、粒径が2μm以下のダイヤモンド砥粒を35%、グリーンカーボランダム、ホワイトアランダムのフィラーを5%、SiOを主成分とするビトリファイドボンド材を60%の割合で混練し、重量比30%の粉末混練物を生成する。そして、重量比5%のアクリル系ボンド材(有機物ボンド材)、重量比55%の水、重量比10%のアルコールを混練し、重量比100%の流動性砥粒とし、この流動性砥粒をスポンジ部材に含浸させて含浸スポンジ体とする。 The example of the manufacturing method of a vitrified bond grindstone is shown below. First, in the impregnated sponge body forming step, a vitrified bond containing 35% of diamond abrasive grains each having a volume ratio of 2 μm or less, 5% of green carborundum and white alundum filler, and SiO 2 as a main component. The material is kneaded at a ratio of 60% to produce a powder kneaded product with a weight ratio of 30%. Then, an acrylic bond material (organic bond material) having a weight ratio of 5%, water having a weight ratio of 55%, and alcohol having a weight ratio of 10% are kneaded to obtain fluid abrasive grains having a weight ratio of 100%. Is impregnated into a sponge member to obtain an impregnated sponge body.

次に、固化工程では、含浸スポンジ体を50°Cで2時間加熱することにより、水及びアルコールの水分を蒸発させる。そして、120°Cで1時間加熱することにより、アクリル系ボンド材を固化させる。   Next, in the solidifying step, the impregnated sponge body is heated at 50 ° C. for 2 hours to evaporate water and alcohol. Then, the acrylic bond material is solidified by heating at 120 ° C. for 1 hour.

焼結工程では、固化工程後の含浸スポンジ体を400°Cで1時間加熱して有機物ボンド材とスポンジ部材とを酸化させる。更に、700°Cで4時間焼結して焼結体を形成する。この焼結体がビトリファイドボンド砥石となる。   In the sintering process, the impregnated sponge body after the solidification process is heated at 400 ° C. for 1 hour to oxidize the organic bond material and the sponge member. Furthermore, it sinters at 700 degreeC for 4 hours, and forms a sintered compact. This sintered body becomes a vitrified bond grindstone.

スポンジ部材を示す斜視図である。It is a perspective view which shows a sponge member. 同スポンジ部材を流動性砥粒に浸漬する状態を示す斜視図である。It is a perspective view which shows the state which immerses the sponge member in a fluid abrasive grain. 焼結体を成型する状態を示す斜視図である。It is a perspective view which shows the state which shape | molds a sintered compact. セグメント状ビトリファイドボンド砥石が固着された研削ホイールを示す斜視図である。It is a perspective view which shows the grinding wheel with which the segment-like vitrified bond grindstone was fixed. 同研削ホイールを搭載した研削装置を示す斜視図である。It is a perspective view which shows the grinding device carrying the grinding wheel.

符号の説明Explanation of symbols

1:スポンジ部材
2:流動性砥粒
3:容器
4:ビトリファイドボンド砥石
5:切削ブレード
6:切削ライン
7:セグメント状ビトリファイドボンド砥石
8:研削装置
80:チャックテーブル
81:研削手段
810:ハウジング 811:スピンドル 812:モータ
813:ホイールマウント 814:研削ホイール
820:昇降板 821:支持部 822:ガイドレール 823:ボールネジ
824:パルスモータ
1: Sponge member 2: Flowable abrasive grain 3: Container 4: Vitrified bond grindstone 5: Cutting blade 6: Cutting line 7: Segmented vitrified bond grindstone 8: Grinding device 80: Chuck table 81: Grinding means 810: Housing 811 Spindle 812: Motor 813: Wheel mount 814: Grinding wheel 820: Lift plate 821: Supporting part 822: Guide rail 823: Ball screw 824: Pulse motor

Claims (7)

気孔を有するビトリファイドボンド砥石であって、
少なくともSiOを主成分とするビトリファイドボンド材と有機物ボンド材と砥粒と液体とを混練した流動性砥粒を樹脂で形成されたスポンジ部材に含浸させ、該有機物ボンド材と該スポンジ部材とを酸化させると共に該砥粒を該ビトリファイドボンド材で焼結したビトリファイドボンド砥石。
A vitrified bond grindstone having pores,
A sponge member formed of a resin is impregnated with a fluid abrasive particle obtained by kneading at least a SiO 2 -based vitrified bond material, an organic bond material, abrasive particles, and a liquid, and the organic bond material and the sponge member are impregnated. A vitrified bond grindstone in which the abrasive grains are oxidized and sintered with the vitrified bond material.
気孔を有するビトリファイドボンド砥石の製造方法であって、
少なくともSiOを主成分とするビトリファイドボンド材と有機物ボンド材と砥粒と液体とを混練して流動性砥粒を形成し、気孔を有する樹脂で形成されたスポンジ部材に該流動性砥粒を含浸させて含浸スポンジ体を構成する含浸スポンジ体形成工程と、
該含浸スポンジ体を構成する液体を蒸発させると共に該有機物ボンド材を固化させる固化工程と、
該固化工程後の含浸スポンジ体を焼結して該有機物ボンド材と該スポンジ部材とを酸化させると共に該ビトリファイドボンド材によって該砥粒を焼結させて気孔を有する焼結体を形成する焼結工程と
から構成されるビトリファイドボンド砥石の製造方法。
A method for producing a vitrified bond grindstone having pores,
A fluidized abrasive is formed by kneading a vitrified bond material containing at least SiO 2 as a main component, an organic bond material, an abrasive and a liquid, and the fluid abrasive is applied to a sponge member formed of a resin having pores. An impregnation sponge body forming step of impregnating and constituting an impregnation sponge body; and
A solidification step of evaporating the liquid constituting the impregnated sponge body and solidifying the organic bond material;
Sintering the impregnated sponge body after the solidification step to oxidize the organic bond material and the sponge member and to sinter the abrasive grains with the vitrified bond material to form a sintered body having pores The manufacturing method of the vitrified bond grindstone comprised from a process.
前記含浸スポンジ体形成工程において、前記砥粒は粒径2μm以下のダイヤモンド砥粒にグリーンカーボランダム、ホワイトアランダムのフィラーが混入されて構成される請求項2に記載のビトリファイドボンド砥石の製造方法。   3. The method for producing a vitrified bond grindstone according to claim 2, wherein in the impregnation sponge body forming step, the abrasive grains are configured by mixing diamond abrasive grains having a particle diameter of 2 μm or less with green carborundum and white alundum fillers. 前記含浸スポンジ体形成工程において、前記液体は重量比55%の水と重量比10%のアルコールとで構成され、前記有機物ボンド材は重量比5%のアクリル系ボンド材である請求項3に記載のビトリファイドボンド砥石の製造方法。   The said impregnation sponge body formation process WHEREIN: The said liquid is comprised with the water of 55% of weight ratio, and the alcohol of 10% of weight ratio, The said organic substance bond material is an acrylic type bond material of 5% of weight ratio. Method for manufacturing a vitrified bond whetstone. 前記固化工程において、前記含浸スポンジ体を50°Cで2時間加熱して前記液体を蒸発させ、前記有機物ボンド材を120°Cで2時間加熱して焼結させる請求項2、3または4に記載のビトリファイドボンド砥石の製造方法。   5. In the solidification step, the impregnated sponge body is heated at 50 ° C. for 2 hours to evaporate the liquid, and the organic bond material is heated at 120 ° C. for 2 hours to be sintered. The manufacturing method of the vitrified bond grindstone of description. 前記焼結工程において、前記固化工程後の含浸スポンジ体を400°Cで1時間焼結して前記有機物ボンド材と前記スポンジ部材とを酸化させ、700°Cで4時間焼結して前記焼結体を形成する請求項2、3、4または5に記載のビトリファイドボンド砥石の製造方法。   In the sintering step, the impregnated sponge body after the solidification step is sintered at 400 ° C. for 1 hour to oxidize the organic bond material and the sponge member, and sintered at 700 ° C. for 4 hours to perform the firing. The manufacturing method of the vitrified bond grindstone according to claim 2, 3, 4, or 5 which forms a ligature. 前記焼結工程後に、前記焼結体を切削ブレードで切削して整形し、研削ホイールに固着される砥石とする請求項2、3、4、5または6に記載のビトリファイドボンド砥石の製造方法。   The method for producing a vitrified bond grindstone according to claim 2, 3, 4, 5 or 6, wherein after the sintering step, the sintered body is cut and shaped by a cutting blade to form a grindstone fixed to a grinding wheel.
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