JP2005520817A5 - - Google Patents
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- Publication number
- JP2005520817A5 JP2005520817A5 JP2003567891A JP2003567891A JP2005520817A5 JP 2005520817 A5 JP2005520817 A5 JP 2005520817A5 JP 2003567891 A JP2003567891 A JP 2003567891A JP 2003567891 A JP2003567891 A JP 2003567891A JP 2005520817 A5 JP2005520817 A5 JP 2005520817A5
- Authority
- JP
- Japan
- Prior art keywords
- klg
- ester
- ascorbic acid
- separated
- unreacted
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 8
- 229960005070 ascorbic acid Drugs 0.000 description 4
- 235000010323 ascorbic acid Nutrition 0.000 description 4
- 239000011668 ascorbic acid Substances 0.000 description 4
- -1 KLG ester Chemical class 0.000 description 3
- 238000000034 method Methods 0.000 description 2
- 238000004587 chromatography analysis Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/074,829 US6476239B1 (en) | 2002-02-12 | 2002-02-12 | Process for the preparation of ascorbic acid |
| PCT/US2003/003973 WO2003068764A1 (en) | 2002-02-12 | 2003-02-10 | Process for the prepatation of ascorbic acid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2005520817A JP2005520817A (ja) | 2005-07-14 |
| JP2005520817A5 true JP2005520817A5 (enExample) | 2006-03-30 |
Family
ID=22121915
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2003567891A Pending JP2005520817A (ja) | 2002-02-12 | 2003-02-10 | アスコルビン酸の製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US6476239B1 (enExample) |
| EP (1) | EP1474410B1 (enExample) |
| JP (1) | JP2005520817A (enExample) |
| CN (1) | CN1285584C (enExample) |
| AT (1) | ATE332297T1 (enExample) |
| AU (1) | AU2003219729A1 (enExample) |
| DE (1) | DE60306622T2 (enExample) |
| WO (1) | WO2003068764A1 (enExample) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6864376B2 (en) | 2000-12-22 | 2005-03-08 | Eastman Chemical Company | Process for producing ascorbic acid |
| US6872314B2 (en) * | 2003-08-29 | 2005-03-29 | Eastman Chemical Company | Dewatering process |
| PT103123A (pt) * | 2004-05-19 | 2005-11-30 | Univ Do Porto | Processo industrial de producao de acetais num reactor adsorptivo de leito movel simulado |
| EP2373391A1 (en) * | 2008-12-08 | 2011-10-12 | Novo Nordisk A/S | Counter current purification of polypeptides |
| PT104496B (pt) * | 2009-04-08 | 2011-03-14 | Univ Do Porto | Reactor de membranas adsorptivo de leito móvel simulado, novo processo híbrido de saparação e respectivas utilizações |
| US8658845B2 (en) | 2012-05-23 | 2014-02-25 | Orochem Technologies, Inc. | Process and adsorbent for separating ethanol and associated oxygenates from a biofermentation system |
| JP6411334B2 (ja) * | 2012-05-23 | 2018-10-24 | ランザテク・ニュージーランド・リミテッド | 発酵及び疑似移動床プロセス |
| US8704016B2 (en) | 2012-05-23 | 2014-04-22 | Orochem Technologies, Inc. | SMB process for the purification of ethanol and butanediol with integrated regeneration |
| US20160297747A1 (en) | 2015-04-08 | 2016-10-13 | Invista North America S.A.R.L. | Materials and methods for the selective recovery of monovalent products from aqueous solutions using continuous ion exchange |
| WO2016164767A1 (en) | 2015-04-10 | 2016-10-13 | Invista North America S.A.R.L. | Process for separation of diamines and/or omega-aminoacids from a feed mixture |
| US11097206B2 (en) * | 2016-12-09 | 2021-08-24 | Orochem Technologies Inc. | Method for producing purified steviol product using simulated moving bed chromatography |
| CN113015578B (zh) | 2018-09-18 | 2023-11-21 | 英威达纺织(英国)有限公司 | 用于从水性混合物中回收胺及其衍生物的系统和方法 |
| CN110327883A (zh) * | 2019-07-13 | 2019-10-15 | 安徽科技学院 | 脱除维生素c溶液色素碳素材料及制备方法及其脱色方法 |
| CN110423229A (zh) * | 2019-08-08 | 2019-11-08 | 安徽丰原发酵技术工程研究有限公司 | 一种以古龙酸为原料的碱转化法制备维生素c的方法 |
| CN110386908A (zh) * | 2019-08-08 | 2019-10-29 | 安徽丰原发酵技术工程研究有限公司 | 一种以古龙酸盐为原料的碱转化法制备维生素c的方法 |
| CN110343080A (zh) * | 2019-08-08 | 2019-10-18 | 安徽丰原发酵技术工程研究有限公司 | 一种以古龙酸为原料的含氮碱转化法制备维生素c的方法 |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2185383A (en) | 1937-04-28 | 1940-01-02 | Charles Pflzer & Company | Preparation of levo-ascorbic acid |
| US2491065A (en) | 1941-12-01 | 1949-12-13 | Tno | Process for producing ascorbic acid from 2-keto-levo-gulonic acid or its derivatives |
| US2462251A (en) | 1945-05-16 | 1949-02-22 | Merck & Co Inc | Process for preparing ascorbic acids |
| US2956070A (en) | 1958-04-29 | 1960-10-11 | American Oil Co | Organic chemical reactions involving liberation of water |
| FI69248C (fi) | 1976-12-21 | 1986-01-10 | Mitsubishi Chem Ind | Foerfarande foer reglering av operationsprocessen av en simulerad roerlig baedd |
| US4764276A (en) | 1984-07-30 | 1988-08-16 | Advanced Separation Technologies Incorporated | Device for continuous contacting of fluids and solids |
| JPH0669521B2 (ja) | 1986-12-23 | 1994-09-07 | 三菱化成エンジニアリング株式会社 | クロマト分離法 |
| US4923616A (en) | 1987-09-24 | 1990-05-08 | Mitsubishi Petrochemical Company, Ltd. | Method of separating chemical components in simulated moving bed |
| JPH0746097B2 (ja) | 1988-05-17 | 1995-05-17 | 三菱化成エンジニアリング株式会社 | クロマト分離法 |
| FR2648136B1 (fr) | 1989-06-12 | 1994-06-17 | Rhone Poulenc Sante | Procede de preparation de l'acide ascorbique |
| EP0671405A1 (de) | 1994-01-18 | 1995-09-13 | F. Hoffmann-La Roche Ag | Herstellung von 2-Keto-L-gulonsäureestern |
| US5405992A (en) * | 1994-04-28 | 1995-04-11 | Uop | Process for concurrent esterification and separation using a simulated moving bed |
| JPH08188578A (ja) * | 1994-11-11 | 1996-07-23 | Takeda Chem Ind Ltd | L−アスコルビン酸の製造方法 |
| US6146534A (en) | 1996-08-19 | 2000-11-14 | Reilly Industries, Inc. | Thermally-managed separation and dewatering processes for recovering acid products |
| US5502248A (en) * | 1995-02-27 | 1996-03-26 | Uop | Process for concurrent hydrolysis of esters and separation of products using a simulated moving bed |
| DE19547073C1 (de) | 1995-12-16 | 1996-11-14 | Merck Patent Gmbh | Verfahren zur Herstellung von Ascorbinsäure |
| US6035396A (en) | 1996-07-01 | 2000-03-07 | Iomega Corporation | Method for sharing a storage medium between computers having disparate operating systems |
| EP1000050A1 (de) | 1997-07-16 | 2000-05-17 | Enco Engineering Chur Ag | Verfahren zur herstellung von ascorbat |
| DE19919203A1 (de) | 1999-04-28 | 2000-11-02 | Basf Ag | Verfahren zur Herstellung von L-Ascorbinsäure |
| US6153791A (en) | 1999-08-02 | 2000-11-28 | Archer-Daniels-Midland Company | Process for purifying 2-keto-L-gulonic acid |
| DE19938980A1 (de) | 1999-08-19 | 2001-02-22 | Basf Ag | Verfahren zur Herstellung von 2-Keto-L-gulonsäureestern |
| US6740762B2 (en) * | 2001-08-24 | 2004-05-25 | Eastman Chemical Company | Process for ascorbic acids using alkaline earth silicate catalysts |
-
2002
- 2002-02-12 US US10/074,829 patent/US6476239B1/en not_active Expired - Lifetime
-
2003
- 2003-02-10 EP EP03716000A patent/EP1474410B1/en not_active Expired - Lifetime
- 2003-02-10 AU AU2003219729A patent/AU2003219729A1/en not_active Abandoned
- 2003-02-10 JP JP2003567891A patent/JP2005520817A/ja active Pending
- 2003-02-10 AT AT03716000T patent/ATE332297T1/de not_active IP Right Cessation
- 2003-02-10 DE DE60306622T patent/DE60306622T2/de not_active Expired - Lifetime
- 2003-02-10 WO PCT/US2003/003973 patent/WO2003068764A1/en not_active Ceased
- 2003-02-10 CN CN03803807.2A patent/CN1285584C/zh not_active Expired - Fee Related
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