JP2003001941A

JP2003001941A - 記録材料

記録材料

Info

Publication number: JP2003001941A
Authority: JP; Japan
Prior art keywords: recording material; layer; recording; coating; polyvinyl alcohol
Prior art date: 2001-06-26
Legal status : Pending

Application number

JP2001193131A

Other languages

English (en)

Japanese (ja)

Other versions

JP2003001941A5 (enExample

Inventor

Shinichiro Serizawa

慎一郎芹澤

Yasuhiro Ogata

安弘緒方

Current Assignee

Fujifilm Holdings Corp

Original Assignee

Fuji Photo Film Co Ltd

Priority date

2001-06-26

Filing date

2001-06-26

Publication date

2003-01-08

2001-06-26 Application filed by Fuji Photo Film Co Ltd filed Critical Fuji Photo Film Co Ltd

2001-06-26 Priority to JP2001193131A priority Critical patent/JP2003001941A/ja

2002-06-25 Priority to US10/178,895 priority patent/US7094731B2/en

2002-06-25 Priority to EP02013963A priority patent/EP1275519B1/en

2002-06-25 Priority to DE60205823T priority patent/DE60205823T2/de

2003-01-08 Publication of JP2003001941A publication Critical patent/JP2003001941A/ja

2006-03-30 Publication of JP2003001941A5 publication Critical patent/JP2003001941A5/ja

Status Pending legal-status Critical Current

Links

239000000463 material Substances 0.000 title claims abstract description 67
238000000576 coating method Methods 0.000 claims abstract description 84
239000011248 coating agent Substances 0.000 claims abstract description 80
229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 54
239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 53
239000007788 liquid Substances 0.000 claims abstract description 40
239000004848 polyfunctional curative Substances 0.000 claims abstract description 13
-1 diol compound Chemical class 0.000 claims description 85
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 46
RJDOZRNNYVAULJ-UHFFFAOYSA-L [O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[F-].[F-].[Mg++].[Mg++].[Mg++].[Al+3].[Si+4].[Si+4].[Si+4].[K+] Chemical compound [O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[F-].[F-].[Mg++].[Mg++].[Mg++].[Al+3].[Si+4].[Si+4].[Si+4].[K+] RJDOZRNNYVAULJ-UHFFFAOYSA-L 0.000 claims description 21
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
239000002904 solvent Substances 0.000 claims description 14
150000002484 inorganic compounds Chemical class 0.000 claims description 7
229910010272 inorganic material Inorganic materials 0.000 claims description 7
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 29
125000002339 acetoacetyl group Chemical group O=C([*])C([H])([H])C(=O)C([H])([H])[H] 0.000 abstract 1
239000010410 layer Substances 0.000 description 125
150000001875 compounds Chemical class 0.000 description 46
235000019422 polyvinyl alcohol Nutrition 0.000 description 45
239000000243 solution Substances 0.000 description 43
239000000975 dye Substances 0.000 description 30
239000002243 precursor Substances 0.000 description 29
238000000034 method Methods 0.000 description 28
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 27
239000002775 capsule Substances 0.000 description 24
238000002360 preparation method Methods 0.000 description 20
150000008049 diazo compounds Chemical class 0.000 description 16
239000003795 chemical substances by application Substances 0.000 description 15
239000012954 diazonium Substances 0.000 description 15
239000000839 emulsion Substances 0.000 description 13
239000007864 aqueous solution Substances 0.000 description 12
230000000052 comparative effect Effects 0.000 description 12
239000000203 mixture Substances 0.000 description 11
150000003839 salts Chemical class 0.000 description 11
108010010803 Gelatin Proteins 0.000 description 10
239000006185 dispersion Substances 0.000 description 10
229920000159 gelatin Polymers 0.000 description 10
239000008273 gelatin Substances 0.000 description 10
235000019322 gelatine Nutrition 0.000 description 10
235000011852 gelatine desserts Nutrition 0.000 description 10
239000002585 base Substances 0.000 description 9
235000014113 dietary fatty acids Nutrition 0.000 description 9
239000000194 fatty acid Substances 0.000 description 9
229930195729 fatty acid Natural products 0.000 description 9
239000002245 particle Substances 0.000 description 9
239000011230 binding agent Substances 0.000 description 8
238000006243 chemical reaction Methods 0.000 description 8
229910052751 metal Inorganic materials 0.000 description 8
239000002184 metal Substances 0.000 description 8
UHOVQNZJYSORNB-UHFFFAOYSA-N monobenzene Natural products C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 8
238000007127 saponification reaction Methods 0.000 description 8
238000011156 evaluation Methods 0.000 description 7
150000004665 fatty acids Chemical class 0.000 description 7
238000006116 polymerization reaction Methods 0.000 description 7
239000011734 sodium Substances 0.000 description 7
239000007787 solid Substances 0.000 description 7
239000000126 substance Substances 0.000 description 7
239000004698 Polyethylene Substances 0.000 description 6
125000003118 aryl group Chemical group 0.000 description 6
238000007756 gravure coating Methods 0.000 description 6
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229920000573 polyethylene Polymers 0.000 description 6
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 5
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 5
150000001768 cations Chemical class 0.000 description 5
229920001577 copolymer Polymers 0.000 description 5
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239000012948 isocyanate Substances 0.000 description 5
238000010030 laminating Methods 0.000 description 5
239000010445 mica Substances 0.000 description 5
229910052618 mica group Inorganic materials 0.000 description 5
150000007524 organic acids Chemical class 0.000 description 5
150000007530 organic bases Chemical class 0.000 description 5
229910052760 oxygen Inorganic materials 0.000 description 5
239000001301 oxygen Substances 0.000 description 5
239000000049 pigment Substances 0.000 description 5
239000011241 protective layer Substances 0.000 description 5
238000003756 stirring Methods 0.000 description 5
238000002834 transmittance Methods 0.000 description 5
FKTHNVSLHLHISI-UHFFFAOYSA-N 1,2-bis(isocyanatomethyl)benzene Chemical compound O=C=NCC1=CC=CC=C1CN=C=O FKTHNVSLHLHISI-UHFFFAOYSA-N 0.000 description 4
FJKROLUGYXJWQN-UHFFFAOYSA-N 4-hydroxybenzoic acid Chemical compound OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 4
206010068516 Encapsulation reaction Diseases 0.000 description 4
239000004952 Polyamide Substances 0.000 description 4
229920002472 Starch Polymers 0.000 description 4
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 4
239000006096 absorbing agent Substances 0.000 description 4
JPIYZTWMUGTEHX-UHFFFAOYSA-N auramine O free base Chemical class C1=CC(N(C)C)=CC=C1C(=N)C1=CC=C(N(C)C)C=C1 JPIYZTWMUGTEHX-UHFFFAOYSA-N 0.000 description 4
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 4
238000001035 drying Methods 0.000 description 4
238000005755 formation reaction Methods 0.000 description 4
229910001385 heavy metal Inorganic materials 0.000 description 4
150000002513 isocyanates Chemical class 0.000 description 4
239000003094 microcapsule Substances 0.000 description 4
150000002989 phenols Chemical class 0.000 description 4
229920002647 polyamide Polymers 0.000 description 4
229920000768 polyamine Polymers 0.000 description 4
229920000642 polymer Polymers 0.000 description 4
239000004814 polyurethane Substances 0.000 description 4
238000007639 printing Methods 0.000 description 4
229920005989 resin Polymers 0.000 description 4
239000011347 resin Substances 0.000 description 4
239000008107 starch Substances 0.000 description 4
235000019698 starch Nutrition 0.000 description 4
230000008961 swelling Effects 0.000 description 4
229920003169 water-soluble polymer Polymers 0.000 description 4
239000001993 wax Substances 0.000 description 4
FUPAJKKAHDLPAZ-UHFFFAOYSA-N 1,2,3-triphenylguanidine Chemical compound C=1C=CC=CC=1NC(=NC=1C=CC=CC=1)NC1=CC=CC=C1 FUPAJKKAHDLPAZ-UHFFFAOYSA-N 0.000 description 3
XKZQKPRCPNGNFR-UHFFFAOYSA-N 2-(3-hydroxyphenyl)phenol Chemical compound OC1=CC=CC(C=2C(=CC=CC=2)O)=C1 XKZQKPRCPNGNFR-UHFFFAOYSA-N 0.000 description 3
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
229920000877 Melamine resin Polymers 0.000 description 3
229920002396 Polyurea Polymers 0.000 description 3
239000004902 Softening Agent Substances 0.000 description 3
YSMRWXYRXBRSND-UHFFFAOYSA-N TOTP Chemical compound CC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C)OC1=CC=CC=C1C YSMRWXYRXBRSND-UHFFFAOYSA-N 0.000 description 3
229920001807 Urea-formaldehyde Polymers 0.000 description 3
239000002253 acid Substances 0.000 description 3
230000015572 biosynthetic process Effects 0.000 description 3
239000011247 coating layer Substances 0.000 description 3
238000005859 coupling reaction Methods 0.000 description 3
MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
238000009820 dry lamination Methods 0.000 description 3
230000000694 effects Effects 0.000 description 3
239000007789 gas Substances 0.000 description 3
XHQSLVIGPHXVAK-UHFFFAOYSA-K iron(3+);octadecanoate Chemical compound [Fe+3].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XHQSLVIGPHXVAK-UHFFFAOYSA-K 0.000 description 3
238000002844 melting Methods 0.000 description 3
239000012188 paraffin wax Substances 0.000 description 3
229920002635 polyurethane Polymers 0.000 description 3
125000002572 propoxy group Chemical group [*]OC([H])([H])C(C([H])([H])[H])([H])[H] 0.000 description 3
230000004043 responsiveness Effects 0.000 description 3
238000004513 sizing Methods 0.000 description 3
229910052708 sodium Inorganic materials 0.000 description 3
230000001629 suppression Effects 0.000 description 3
239000004094 surface-active agent Substances 0.000 description 3
VTIMKVIDORQQFA-UHFFFAOYSA-N 2-Ethylhexyl-4-hydroxybenzoate Chemical compound CCCCC(CC)COC(=O)C1=CC=C(O)C=C1 VTIMKVIDORQQFA-UHFFFAOYSA-N 0.000 description 2
YQUVCSBJEUQKSH-UHFFFAOYSA-N 3,4-dihydroxybenzoic acid Chemical compound OC(=O)C1=CC=C(O)C(O)=C1 YQUVCSBJEUQKSH-UHFFFAOYSA-N 0.000 description 2
PYSRRFNXTXNWCD-UHFFFAOYSA-N 3-(2-phenylethenyl)furan-2,5-dione Chemical compound O=C1OC(=O)C(C=CC=2C=CC=CC=2)=C1 PYSRRFNXTXNWCD-UHFFFAOYSA-N 0.000 description 2
229940090248 4-hydroxybenzoic acid Drugs 0.000 description 2
RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 2
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239000004925 Acrylic resin Substances 0.000 description 2
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
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IEPRKVQEAMIZSS-UHFFFAOYSA-N Di-Et ester-Fumaric acid Natural products CCOC(=O)C=CC(=O)OCC IEPRKVQEAMIZSS-UHFFFAOYSA-N 0.000 description 2
IEPRKVQEAMIZSS-WAYWQWQTSA-N Diethyl maleate Chemical compound CCOC(=O)\C=C/C(=O)OCC IEPRKVQEAMIZSS-WAYWQWQTSA-N 0.000 description 2
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QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
238000012695 Interfacial polymerization Methods 0.000 description 2
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229920000147 Styrene maleic anhydride Polymers 0.000 description 2
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
239000002250 absorbent Substances 0.000 description 2
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238000010521 absorption reaction Methods 0.000 description 2
DYRDKSSFIWVSNM-UHFFFAOYSA-N acetoacetanilide Chemical compound CC(=O)CC(=O)NC1=CC=CC=C1 DYRDKSSFIWVSNM-UHFFFAOYSA-N 0.000 description 2
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239000000440 bentonite Substances 0.000 description 2
229910000278 bentonite Inorganic materials 0.000 description 2
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YXVFYQXJAXKLAK-UHFFFAOYSA-N biphenyl-4-ol Chemical compound C1=CC(O)=CC=C1C1=CC=CC=C1 YXVFYQXJAXKLAK-UHFFFAOYSA-N 0.000 description 2
238000009835 boiling Methods 0.000 description 2
239000011575 calcium Substances 0.000 description 2
VNSBYDPZHCQWNB-UHFFFAOYSA-N calcium;aluminum;dioxido(oxo)silane;sodium;hydrate Chemical compound O.[Na].[Al].[Ca+2].[O-][Si]([O-])=O VNSBYDPZHCQWNB-UHFFFAOYSA-N 0.000 description 2
125000004432 carbon atom Chemical group C* 0.000 description 2
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125000005843 halogen group Chemical group 0.000 description 2
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KWLMIXQRALPRBC-UHFFFAOYSA-L hectorite Chemical compound [Li+].[OH-].[OH-].[Na+].[Mg+2].O1[Si]2([O-])O[Si]1([O-])O[Si]([O-])(O1)O[Si]1([O-])O2 KWLMIXQRALPRBC-UHFFFAOYSA-L 0.000 description 2
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125000000623 heterocyclic group Chemical group 0.000 description 2
IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
229910000462 iron(III) oxide hydroxide Inorganic materials 0.000 description 2
229920000126 latex Polymers 0.000 description 2
239000004816 latex Substances 0.000 description 2
239000011133 lead Substances 0.000 description 2
QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 2
150000004780 naphthols Chemical class 0.000 description 2
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230000001590 oxidative effect Effects 0.000 description 2
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230000035699 permeability Effects 0.000 description 2
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125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 2
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150000003053 piperidines Chemical class 0.000 description 2
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150000003222 pyridines Chemical class 0.000 description 2
GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
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125000001424 substituent group Chemical group 0.000 description 2
UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 description 2
KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 2
238000011282 treatment Methods 0.000 description 2
229910052725 zinc Inorganic materials 0.000 description 2
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LIZLYZVAYZQVPG-UHFFFAOYSA-N (3-bromo-2-fluorophenyl)methanol Chemical compound OCC1=CC=CC(Br)=C1F LIZLYZVAYZQVPG-UHFFFAOYSA-N 0.000 description 1
VYHXFXBVSRWDGI-UHFFFAOYSA-N 1,1,2-tricyclohexylguanidine Chemical compound C1CCCCC1N(C1CCCCC1)C(N)=NC1CCCCC1 VYHXFXBVSRWDGI-UHFFFAOYSA-N 0.000 description 1
PRZQJMWBZWAUKW-UHFFFAOYSA-N 1,3-dicyclohexyl-1,3-diazinane-2,4,6-trione Chemical compound O=C1N(C2CCCCC2)C(=O)CC(=O)N1C1CCCCC1 PRZQJMWBZWAUKW-UHFFFAOYSA-N 0.000 description 1
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YLVACWCCJCZITJ-UHFFFAOYSA-N 1,4-dioxane-2,3-diol Chemical compound OC1OCCOC1O YLVACWCCJCZITJ-UHFFFAOYSA-N 0.000 description 1
FRASJONUBLZVQX-UHFFFAOYSA-N 1,4-dioxonaphthalene Natural products C1=CC=C2C(=O)C=CC(=O)C2=C1 FRASJONUBLZVQX-UHFFFAOYSA-N 0.000 description 1
BOKGTLAJQHTOKE-UHFFFAOYSA-N 1,5-dihydroxynaphthalene Chemical compound C1=CC=C2C(O)=CC=CC2=C1O BOKGTLAJQHTOKE-UHFFFAOYSA-N 0.000 description 1
ICJNMHCSCZQNSR-UHFFFAOYSA-N 1-(2,5-dioctoxyphenyl)-3-phenyl-1,3-diazinane-2,4,6-trione Chemical compound CCCCCCCCOC1=CC=C(OCCCCCCCC)C(N2C(N(C(=O)CC2=O)C=2C=CC=CC=2)=O)=C1 ICJNMHCSCZQNSR-UHFFFAOYSA-N 0.000 description 1
TUSDEZXZIZRFGC-UHFFFAOYSA-N 1-O-galloyl-3,6-(R)-HHDP-beta-D-glucose Natural products OC1C(O2)COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC1C(O)C2OC(=O)C1=CC(O)=C(O)C(O)=C1 TUSDEZXZIZRFGC-UHFFFAOYSA-N 0.000 description 1
ATYBDUQHRWXJQD-UHFFFAOYSA-N 1-[4-(2-hydroxy-3-naphthalen-2-yloxypropyl)piperazin-1-yl]-3-naphthalen-2-yloxypropan-2-ol Chemical compound C1=CC=CC2=CC(OCC(O)CN3CCN(CC3)CC(COC=3C=C4C=CC=CC4=CC=3)O)=CC=C21 ATYBDUQHRWXJQD-UHFFFAOYSA-N 0.000 description 1
YHIJMIBVSIPDAN-UHFFFAOYSA-N 1-[4-(2-hydroxy-3-phenoxypropyl)piperazin-1-yl]-3-phenoxypropan-2-ol Chemical compound C1CN(CC(O)COC=2C=CC=CC=2)CCN1CC(O)COC1=CC=CC=C1 YHIJMIBVSIPDAN-UHFFFAOYSA-N 0.000 description 1
RUFOEHSJMQBWOD-UHFFFAOYSA-N 1-[4-(2-hydroxy-3-phenylsulfanylpropyl)piperazin-1-yl]-3-phenylsulfanylpropan-2-ol Chemical compound C1CN(CC(O)CSC=2C=CC=CC=2)CCN1CC(O)CSC1=CC=CC=C1 RUFOEHSJMQBWOD-UHFFFAOYSA-N 0.000 description 1
AAUPHOUSNSWUKE-UHFFFAOYSA-N 1-[4-[2-hydroxy-3-(4-methoxyphenoxy)propyl]piperazin-1-yl]-3-(4-methoxyphenoxy)propan-2-ol Chemical compound C1=CC(OC)=CC=C1OCC(O)CN1CCN(CC(O)COC=2C=CC(OC)=CC=2)CC1 AAUPHOUSNSWUKE-UHFFFAOYSA-N 0.000 description 1
LFYFXAZBXJEOBM-UHFFFAOYSA-N 1-[4-[2-hydroxy-3-(4-methylphenoxy)propyl]piperazin-1-yl]-3-(4-methylphenoxy)propan-2-ol Chemical compound C1=CC(C)=CC=C1OCC(O)CN1CCN(CC(O)COC=2C=CC(C)=CC=2)CC1 LFYFXAZBXJEOBM-UHFFFAOYSA-N 0.000 description 1
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