JP2001288378A

JP2001288378A - メチン化合物を含むハロゲン化銀写真乳剤およびハロゲン化銀写真感光材料

メチン化合物を含むハロゲン化銀写真乳剤およびハロゲン化銀写真感光材料

Info

Publication number: JP2001288378A
Authority: JP; Japan
Prior art keywords: group; silver halide; silver; emulsion; layer
Prior art date: 2000-02-02
Legal status : Pending

Application number

JP2000084512A

Other languages

English (en)

Japanese (ja)

Other versions

JP2001288378A5 (enExample

Inventor

Naoyuki Hanaki

直幸花木

Takanori Hioki

孝徳日置

Kiyoshi Morimoto

潔守本

Current Assignee

Fujifilm Holdings Corp

Original Assignee

Fuji Photo Film Co Ltd

Priority date

2000-02-02

Filing date

2000-03-24

Publication date

2001-10-16

2000-03-24 Application filed by Fuji Photo Film Co Ltd filed Critical Fuji Photo Film Co Ltd

2000-03-24 Priority to JP2000084512A priority Critical patent/JP2001288378A/ja

2001-02-02 Priority to US09/773,689 priority patent/US6582895B2/en

2001-10-16 Publication of JP2001288378A publication Critical patent/JP2001288378A/ja

2005-11-24 Publication of JP2001288378A5 publication Critical patent/JP2001288378A5/ja

Status Pending legal-status Critical Current

Links

-1 Methine compound Chemical class 0.000 title claims abstract description 305
229910052709 silver Inorganic materials 0.000 title claims abstract description 164
239000004332 silver Substances 0.000 title claims abstract description 164
239000000839 emulsion Substances 0.000 title claims abstract description 144
239000000463 material Substances 0.000 title claims abstract description 39
125000003118 aryl group Chemical group 0.000 claims abstract description 30
125000000623 heterocyclic group Chemical group 0.000 claims abstract description 30
125000000217 alkyl group Chemical group 0.000 claims abstract description 26
125000001424 substituent group Chemical group 0.000 claims abstract description 17
229910052717 sulfur Inorganic materials 0.000 claims abstract description 17
238000000034 method Methods 0.000 claims description 92
230000001235 sensitizing effect Effects 0.000 claims description 55
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 54
150000001875 compounds Chemical group 0.000 claims description 41
230000003595 spectral effect Effects 0.000 claims description 17
229910052801 chlorine Inorganic materials 0.000 claims description 16
125000001309 chloro group Chemical group Cl* 0.000 claims description 14
125000005647 linker group Chemical group 0.000 claims description 8
125000004430 oxygen atom Chemical group O* 0.000 claims description 8
125000004434 sulfur atom Chemical group 0.000 claims description 8
125000003545 alkoxy group Chemical group 0.000 claims description 7
125000003277 amino group Chemical group 0.000 claims description 6
125000000547 substituted alkyl group Chemical group 0.000 claims description 6
238000010521 absorption reaction Methods 0.000 claims description 5
125000004104 aryloxy group Chemical group 0.000 claims description 5
125000005844 heterocyclyloxy group Chemical group 0.000 claims description 4
125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 4
238000006467 substitution reaction Methods 0.000 claims description 4
125000004429 atom Chemical group 0.000 claims description 2
229910052711 selenium Inorganic materials 0.000 abstract description 14
125000001434 methanylylidene group Chemical group [H]C#[*] 0.000 abstract description 8
229910052760 oxygen Inorganic materials 0.000 abstract 1
239000010410 layer Substances 0.000 description 169
239000000975 dye Substances 0.000 description 142
235000013339 cereals Nutrition 0.000 description 130
125000004432 carbon atom Chemical group C* 0.000 description 100
IOLCXVTUBQKXJR-UHFFFAOYSA-M potassium bromide Chemical compound [K+].[Br-] IOLCXVTUBQKXJR-UHFFFAOYSA-M 0.000 description 100
206010070834 Sensitisation Diseases 0.000 description 90
230000008313 sensitization Effects 0.000 description 90
239000000243 solution Substances 0.000 description 73
108010010803 Gelatin Proteins 0.000 description 65
229920000159 gelatin Polymers 0.000 description 65
239000008273 gelatin Substances 0.000 description 65
235000019322 gelatine Nutrition 0.000 description 65
235000011852 gelatine desserts Nutrition 0.000 description 65
239000007864 aqueous solution Substances 0.000 description 55
239000002245 particle Substances 0.000 description 50
239000000126 substance Substances 0.000 description 50
230000009467 reduction Effects 0.000 description 43
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 32
239000006185 dispersion Substances 0.000 description 31
230000035945 sensitivity Effects 0.000 description 31
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 30
239000000203 mixture Substances 0.000 description 28
238000002360 preparation method Methods 0.000 description 28
231100000489 sensitizer Toxicity 0.000 description 28
JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 26
239000011248 coating agent Substances 0.000 description 25
238000000576 coating method Methods 0.000 description 25
229910021612 Silver iodide Inorganic materials 0.000 description 24
238000012545 processing Methods 0.000 description 22
230000005291 magnetic effect Effects 0.000 description 20
238000011161 development Methods 0.000 description 19
230000018109 developmental process Effects 0.000 description 19
DZVCFNFOPIZQKX-LTHRDKTGSA-M merocyanine Chemical compound [Na+].O=C1N(CCCC)C(=O)N(CCCC)C(=O)C1=C\C=C\C=C/1N(CCCS([O-])(=O)=O)C2=CC=CC=C2O\1 DZVCFNFOPIZQKX-LTHRDKTGSA-M 0.000 description 19
JKFYKCYQEWQPTM-UHFFFAOYSA-N 2-azaniumyl-2-(4-fluorophenyl)acetate Chemical compound OC(=O)C(N)C1=CC=C(F)C=C1 JKFYKCYQEWQPTM-UHFFFAOYSA-N 0.000 description 17
229940045105 silver iodide Drugs 0.000 description 17
239000007787 solid Substances 0.000 description 17
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 16
230000015572 biosynthetic process Effects 0.000 description 16
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 16
238000011282 treatment Methods 0.000 description 16
239000007788 liquid Substances 0.000 description 15
238000005406 washing Methods 0.000 description 15
101710134784 Agnoprotein Proteins 0.000 description 14
239000002253 acid Substances 0.000 description 14
239000011575 calcium Substances 0.000 description 14
150000003839 salts Chemical class 0.000 description 14
QGKMIGUHVLGJBR-UHFFFAOYSA-M (4z)-1-(3-methylbutyl)-4-[[1-(3-methylbutyl)quinolin-1-ium-4-yl]methylidene]quinoline;iodide Chemical compound [I-].C12=CC=CC=C2N(CCC(C)C)C=CC1=CC1=CC=[N+](CCC(C)C)C2=CC=CC=C12 QGKMIGUHVLGJBR-UHFFFAOYSA-M 0.000 description 13
239000011230 binding agent Substances 0.000 description 13
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 12
BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical group [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 12
238000004061 bleaching Methods 0.000 description 12
229910052791 calcium Inorganic materials 0.000 description 12
230000000694 effects Effects 0.000 description 12
239000010419 fine particle Substances 0.000 description 11
239000007800 oxidant agent Substances 0.000 description 11
NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Substances [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 11
230000005070 ripening Effects 0.000 description 11
239000011669 selenium Substances 0.000 description 11
239000000654 additive Substances 0.000 description 10
150000002500 ions Chemical class 0.000 description 10
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
229910021607 Silver chloride Inorganic materials 0.000 description 9
239000003795 chemical substances by application Substances 0.000 description 9
238000009826 distribution Methods 0.000 description 9
229910052736 halogen Inorganic materials 0.000 description 9
239000006249 magnetic particle Substances 0.000 description 9
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 9
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 9
230000008569 process Effects 0.000 description 9
ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 description 9
HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 9
239000002904 solvent Substances 0.000 description 9
238000010438 heat treatment Methods 0.000 description 8
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 7
239000003513 alkali Substances 0.000 description 7
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 7
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 7
229910052737 gold Inorganic materials 0.000 description 7
239000010931 gold Substances 0.000 description 7
125000005843 halogen group Chemical group 0.000 description 7
150000002367 halogens Chemical class 0.000 description 7
239000003112 inhibitor Substances 0.000 description 7
229910052740 iodine Inorganic materials 0.000 description 7
239000012948 isocyanate Substances 0.000 description 7
150000002513 isocyanates Chemical class 0.000 description 7
229910052757 nitrogen Inorganic materials 0.000 description 7
229920000728 polyester Polymers 0.000 description 7
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
230000032683 aging Effects 0.000 description 6
239000002216 antistatic agent Substances 0.000 description 6
229920002678 cellulose Polymers 0.000 description 6
239000001913 cellulose Substances 0.000 description 6
235000010980 cellulose Nutrition 0.000 description 6
239000000084 colloidal system Substances 0.000 description 6
150000004820 halides Chemical class 0.000 description 6
229910052751 metal Inorganic materials 0.000 description 6
239000002184 metal Substances 0.000 description 6
125000001570 methylene group Chemical group [H]C([H])([*:1])[*:2] 0.000 description 6
229910000510 noble metal Inorganic materials 0.000 description 6
229920000642 polymer Polymers 0.000 description 6
229910052700 potassium Inorganic materials 0.000 description 6
ZUNKMNLKJXRCDM-UHFFFAOYSA-N silver bromoiodide Chemical compound [Ag].IBr ZUNKMNLKJXRCDM-UHFFFAOYSA-N 0.000 description 6
239000011734 sodium Substances 0.000 description 6
GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 6
238000003860 storage Methods 0.000 description 6
239000011593 sulfur Substances 0.000 description 6
XSOKHXFFCGXDJZ-UHFFFAOYSA-N telluride(2-) Chemical compound [Te-2] XSOKHXFFCGXDJZ-UHFFFAOYSA-N 0.000 description 6
RYYXDZDBXNUPOG-UHFFFAOYSA-N 4,5,6,7-tetrahydro-1,3-benzothiazole-2,6-diamine;dihydrochloride Chemical compound Cl.Cl.C1C(N)CCC2=C1SC(N)=N2 RYYXDZDBXNUPOG-UHFFFAOYSA-N 0.000 description 5
ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical group [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 5
101100501966 Caenorhabditis elegans exc-6 gene Proteins 0.000 description 5
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 5
239000006087 Silane Coupling Agent Substances 0.000 description 5
229920005994 diacetyl cellulose Polymers 0.000 description 5
239000000986 disperse dye Substances 0.000 description 5
230000005294 ferromagnetic effect Effects 0.000 description 5
238000009472 formulation Methods 0.000 description 5
150000002430 hydrocarbons Chemical group 0.000 description 5
239000010954 inorganic particle Substances 0.000 description 5
XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 5
229910052749 magnesium Inorganic materials 0.000 description 5
239000011777 magnesium Substances 0.000 description 5
238000004519 manufacturing process Methods 0.000 description 5
239000006224 matting agent Substances 0.000 description 5
229920003023 plastic Polymers 0.000 description 5
239000004033 plastic Substances 0.000 description 5
239000011347 resin Substances 0.000 description 5
229920005989 resin Polymers 0.000 description 5
229910001961 silver nitrate Inorganic materials 0.000 description 5
BZHOWMPPNDKQSQ-UHFFFAOYSA-M sodium;sulfidosulfonylbenzene Chemical compound [Na+].[O-]S(=O)(=S)C1=CC=CC=C1 BZHOWMPPNDKQSQ-UHFFFAOYSA-M 0.000 description 5
229910052712 strontium Inorganic materials 0.000 description 5
229910052714 tellurium Inorganic materials 0.000 description 5
ZUHDZBHELIKKKH-UHFFFAOYSA-N (2,3,4,5,6-pentafluorophenyl)-diphenyl-selanylidene-$l^{5}-phosphane Chemical compound FC1=C(F)C(F)=C(F)C(F)=C1P(=[Se])(C=1C=CC=CC=1)C1=CC=CC=C1 ZUHDZBHELIKKKH-UHFFFAOYSA-N 0.000 description 4
CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 4
WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 4
UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 4
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 4
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 4
OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 4
KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 4
MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
230000000996 additive effect Effects 0.000 description 4
QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 4
230000005540 biological transmission Effects 0.000 description 4
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 4
ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 description 4
229910052799 carbon Inorganic materials 0.000 description 4
239000008119 colloidal silica Substances 0.000 description 4
125000004093 cyano group Chemical group *C#N 0.000 description 4
SWXVUIWOUIDPGS-UHFFFAOYSA-N diacetone alcohol Chemical compound CC(=O)CC(C)(C)O SWXVUIWOUIDPGS-UHFFFAOYSA-N 0.000 description 4
235000014113 dietary fatty acids Nutrition 0.000 description 4
ZOMNIUBKTOKEHS-UHFFFAOYSA-L dimercury dichloride Chemical class Cl[Hg][Hg]Cl ZOMNIUBKTOKEHS-UHFFFAOYSA-L 0.000 description 4
208000028659 discharge Diseases 0.000 description 4
238000004993 emission spectroscopy Methods 0.000 description 4
239000000194 fatty acid Substances 0.000 description 4
229930195729 fatty acid Natural products 0.000 description 4
150000004665 fatty acids Chemical class 0.000 description 4
239000011630 iodine Substances 0.000 description 4
229920000620 organic polymer Polymers 0.000 description 4
239000003960 organic solvent Substances 0.000 description 4
238000006116 polymerization reaction Methods 0.000 description 4
229920001296 polysiloxane Polymers 0.000 description 4
239000011591 potassium Substances 0.000 description 4
239000004576 sand Substances 0.000 description 4
239000012748 slip agent Substances 0.000 description 4
235000012247 sodium ferrocyanide Nutrition 0.000 description 4
GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 4
238000003756 stirring Methods 0.000 description 4
CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 4
125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 4
125000004964 sulfoalkyl group Chemical group 0.000 description 4
238000004381 surface treatment Methods 0.000 description 4
239000004094 surface-active agent Substances 0.000 description 4
PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 description 4
239000010936 titanium Substances 0.000 description 4
238000012546 transfer Methods 0.000 description 4
AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 description 3
UGWULZWUXSCWPX-UHFFFAOYSA-N 2-sulfanylideneimidazolidin-4-one Chemical class O=C1CNC(=S)N1 UGWULZWUXSCWPX-UHFFFAOYSA-N 0.000 description 3
DLFVBJFMPXGRIB-UHFFFAOYSA-N Acetamide Chemical compound CC(N)=O DLFVBJFMPXGRIB-UHFFFAOYSA-N 0.000 description 3
QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 3
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 3
101100221809 Neurospora crassa (strain ATCC 24698 / 74-OR23-1A / CBS 708.71 / DSM 1257 / FGSC 987) cpd-7 gene Proteins 0.000 description 3
CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 3
229910019142 PO4 Inorganic materials 0.000 description 3
239000004793 Polystyrene Substances 0.000 description 3
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
RWRDLPDLKQPQOW-UHFFFAOYSA-N Pyrrolidine Chemical compound C1CCNC1 RWRDLPDLKQPQOW-UHFFFAOYSA-N 0.000 description 3
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 3
ZMZDMBWJUHKJPS-UHFFFAOYSA-M Thiocyanate anion Chemical compound [S-]C#N ZMZDMBWJUHKJPS-UHFFFAOYSA-M 0.000 description 3
235000010724 Wisteria floribunda Nutrition 0.000 description 3
SJOOOZPMQAWAOP-UHFFFAOYSA-N [Ag].BrCl Chemical compound [Ag].BrCl SJOOOZPMQAWAOP-UHFFFAOYSA-N 0.000 description 3
239000012298 atmosphere Substances 0.000 description 3
239000011324 bead Substances 0.000 description 3
125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 3
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 3
GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 3
229910052794 bromium Inorganic materials 0.000 description 3
125000001951 carbamoylamino group Chemical group C(N)(=O)N* 0.000 description 3
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 3
229910052798 chalcogen Inorganic materials 0.000 description 3
150000001787 chalcogens Chemical class 0.000 description 3
238000006243 chemical reaction Methods 0.000 description 3
239000000460 chlorine Substances 0.000 description 3
239000002131 composite material Substances 0.000 description 3
229940125904 compound 1 Drugs 0.000 description 3
239000013078 crystal Substances 0.000 description 3
238000011033 desalting Methods 0.000 description 3
MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
238000001035 drying Methods 0.000 description 3
238000010894 electron beam technology Methods 0.000 description 3
150000002148 esters Chemical class 0.000 description 3
235000019441 ethanol Nutrition 0.000 description 3
229910052731 fluorine Inorganic materials 0.000 description 3
230000026030 halogenation Effects 0.000 description 3
238000005658 halogenation reaction Methods 0.000 description 3
RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Natural products C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 description 3
229910052738 indium Inorganic materials 0.000 description 3
239000000696 magnetic material Substances 0.000 description 3
VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 3
239000011976 maleic acid Substances 0.000 description 3
239000002609 medium Substances 0.000 description 3
150000002736 metal compounds Chemical class 0.000 description 3
229910044991 metal oxide Inorganic materials 0.000 description 3
150000004706 metal oxides Chemical class 0.000 description 3
235000013336 milk Nutrition 0.000 description 3
239000008267 milk Substances 0.000 description 3
210000004080 milk Anatomy 0.000 description 3
125000004573 morpholin-4-yl group Chemical group N1(CCOCC1)* 0.000 description 3
230000003647 oxidation Effects 0.000 description 3
238000007254 oxidation reaction Methods 0.000 description 3
KDLHZDBZIXYQEI-UHFFFAOYSA-N palladium Substances [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 3
235000021317 phosphate Nutrition 0.000 description 3
229920003207 poly(ethylene-2,6-naphthalate) Polymers 0.000 description 3
229920003229 poly(methyl methacrylate) Polymers 0.000 description 3
239000011112 polyethylene naphthalate Substances 0.000 description 3
239000004926 polymethyl methacrylate Substances 0.000 description 3
229920002223 polystyrene Polymers 0.000 description 3
ZNNZYHKDIALBAK-UHFFFAOYSA-M potassium thiocyanate Chemical compound [K+].[S-]C#N ZNNZYHKDIALBAK-UHFFFAOYSA-M 0.000 description 3
229940116357 potassium thiocyanate Drugs 0.000 description 3
239000011164 primary particle Substances 0.000 description 3
125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 3
239000011241 protective layer Substances 0.000 description 3
238000011160 research Methods 0.000 description 3
GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 3
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