IL100116A - Method and device for the production of iron oxide particles - Google Patents
Method and device for the production of iron oxide particlesInfo
- Publication number
- IL100116A IL100116A IL10011691A IL10011691A IL100116A IL 100116 A IL100116 A IL 100116A IL 10011691 A IL10011691 A IL 10011691A IL 10011691 A IL10011691 A IL 10011691A IL 100116 A IL100116 A IL 100116A
- Authority
- IL
- Israel
- Prior art keywords
- iron
- oxidizing gas
- injector
- iron oxide
- containing compound
- Prior art date
Links
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 title claims description 98
- 239000002245 particle Substances 0.000 title claims description 31
- 238000000034 method Methods 0.000 title claims description 28
- 238000004519 manufacturing process Methods 0.000 title claims description 17
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 108
- 229910052742 iron Inorganic materials 0.000 claims description 53
- 150000001875 compounds Chemical class 0.000 claims description 42
- 230000001590 oxidative effect Effects 0.000 claims description 36
- 238000007254 oxidation reaction Methods 0.000 claims description 18
- 230000003647 oxidation Effects 0.000 claims description 17
- 239000000463 material Substances 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 12
- 229910052918 calcium silicate Inorganic materials 0.000 claims description 6
- 239000000378 calcium silicate Substances 0.000 claims description 6
- OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 claims description 6
- 238000000354 decomposition reaction Methods 0.000 claims description 4
- 230000002028 premature Effects 0.000 claims description 3
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 claims description 2
- 125000005594 diketone group Chemical group 0.000 claims description 2
- KTWOOEGAPBSYNW-UHFFFAOYSA-N ferrocene Chemical class [Fe+2].C=1C=C[CH-]C=1.C=1C=C[CH-]C=1 KTWOOEGAPBSYNW-UHFFFAOYSA-N 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- -1 polytetrafluoroethylene Polymers 0.000 claims description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 2
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 claims 1
- 239000013522 chelant Substances 0.000 claims 1
- 229940087654 iron carbonyl Drugs 0.000 claims 1
- 239000007789 gas Substances 0.000 description 35
- 239000003054 catalyst Substances 0.000 description 18
- 239000000047 product Substances 0.000 description 11
- 239000003380 propellant Substances 0.000 description 10
- 239000007787 solid Substances 0.000 description 8
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 6
- 239000012159 carrier gas Substances 0.000 description 6
- 229910052760 oxygen Inorganic materials 0.000 description 6
- 239000001301 oxygen Substances 0.000 description 6
- 239000012717 electrostatic precipitator Substances 0.000 description 4
- 150000002506 iron compounds Chemical class 0.000 description 4
- 239000012265 solid product Substances 0.000 description 4
- 230000008016 vaporization Effects 0.000 description 4
- 230000003197 catalytic effect Effects 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 238000009834 vaporization Methods 0.000 description 3
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 2
- 241000555745 Sciuridae Species 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 229910052796 boron Inorganic materials 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 239000000446 fuel Substances 0.000 description 2
- 230000009931 harmful effect Effects 0.000 description 2
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 2
- 239000012716 precipitator Substances 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- 238000011144 upstream manufacturing Methods 0.000 description 2
- CDVAIHNNWWJFJW-UHFFFAOYSA-N 3,5-diethoxycarbonyl-1,4-dihydrocollidine Chemical compound CCOC(=O)C1=C(C)NC(C)=C(C(=O)OCC)C1C CDVAIHNNWWJFJW-UHFFFAOYSA-N 0.000 description 1
- GDDNTTHUKVNJRA-UHFFFAOYSA-N 3-bromo-3,3-difluoroprop-1-ene Chemical compound FC(F)(Br)C=C GDDNTTHUKVNJRA-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 230000003466 anti-cipated effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000007767 bonding agent Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000000567 combustion gas Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 229940125782 compound 2 Drugs 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- AXZAYXJCENRGIM-UHFFFAOYSA-J dipotassium;tetrabromoplatinum(2-) Chemical compound [K+].[K+].[Br-].[Br-].[Br-].[Br-].[Pt+2] AXZAYXJCENRGIM-UHFFFAOYSA-J 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 239000008246 gaseous mixture Substances 0.000 description 1
- 239000002241 glass-ceramic Substances 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 150000002505 iron Chemical class 0.000 description 1
- YWBREQLMDUVNIR-UHFFFAOYSA-N iron(2+);hexacyanide Chemical compound [Fe+2].[Fe+2].[Fe+2].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] YWBREQLMDUVNIR-UHFFFAOYSA-N 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical class OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229910001487 potassium perchlorate Inorganic materials 0.000 description 1
- 239000012255 powdered metal Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000004449 solid propellant Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J12/00—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
- B01J12/02—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor for obtaining at least one reaction product which, at normal temperature, is in the solid state
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G49/00—Compounds of iron
- C01G49/02—Oxides; Hydroxides
- C01G49/06—Ferric oxide [Fe2O3]
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00132—Controlling the temperature using electric heating or cooling elements
- B01J2219/00135—Electric resistance heaters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/0015—Controlling the temperature by thermal insulation means
- B01J2219/00155—Controlling the temperature by thermal insulation means using insulating materials or refractories
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Nanotechnology (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Composite Materials (AREA)
- General Physics & Mathematics (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Physics & Mathematics (AREA)
- Inorganic Chemistry (AREA)
- Catalysts (AREA)
- Compounds Of Iron (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US07/618,772 US5169620A (en) | 1990-11-27 | 1990-11-27 | Method and apparatus for the manufacture of iron oxide particles |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IL100116A0 IL100116A0 (en) | 1992-08-18 |
| IL100116A true IL100116A (en) | 1996-05-14 |
Family
ID=24479077
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL10011691A IL100116A (en) | 1990-11-27 | 1991-11-21 | Method and device for the production of iron oxide particles |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US5169620A (fr) |
| EP (1) | EP0488157A3 (fr) |
| JP (1) | JP3605418B2 (fr) |
| IL (1) | IL100116A (fr) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6471937B1 (en) * | 1998-09-04 | 2002-10-29 | Praxair Technology, Inc. | Hot gas reactor and process for using same |
| US20040094250A1 (en) * | 2002-11-14 | 2004-05-20 | Estes-Cox Corporation | Composite propellant compositions |
| CN107879380A (zh) * | 2017-11-17 | 2018-04-06 | 金川集团股份有限公司 | 一种利用羰基铁生产高纯氧化铁的方法 |
| CN112408493A (zh) * | 2020-11-25 | 2021-02-26 | 正太新材料科技有限责任公司 | 一种高遮盖力的氧化铁红制备方法及应用 |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2851347A (en) * | 1949-10-21 | 1958-09-09 | Basf Ag | Manufacture of iron powder |
| US2772956A (en) * | 1954-06-28 | 1956-12-04 | Int Nickel Co | Production of carbonyl iron powder |
| US2900245A (en) * | 1957-01-24 | 1959-08-18 | Gen Aniline & Film Corp | Production of finely divided metals |
| US2938781A (en) * | 1957-12-27 | 1960-05-31 | Gen Aniline & Film Corp | Production of magnetic iron particles |
| US3361525A (en) * | 1961-11-03 | 1968-01-02 | Laporte Titanium Ltd | Manufacture of oxides of the elements titanium, zirconium, iron, aluminum and silicon |
| US4073874A (en) * | 1973-04-28 | 1978-02-14 | Mitsubishi Kinzoku K.K. | Recovery of chlorine from iron chloride |
| AT345252B (de) * | 1975-10-31 | 1978-09-11 | Unibra Sa | Verfahren zur herstellung von magnetoxiden |
| US4056386A (en) * | 1977-04-19 | 1977-11-01 | The United States Of America As Represented By The Secretary Of The Navy | Method for decomposing iron pentacarbonyl |
| JPS5771892A (en) * | 1980-10-20 | 1982-05-04 | Nissan Motor | Composite propellant powder containing combustion speed accelerator |
| DE3428121A1 (de) * | 1984-07-31 | 1986-02-13 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von eisenpulver |
| JPS61122106A (ja) * | 1984-11-19 | 1986-06-10 | Ube Ind Ltd | 微粉末状マグネシウム酸化物の製造方法 |
| JPH068170B2 (ja) * | 1985-10-29 | 1994-02-02 | 宇部興産株式会社 | 高純度酸化マグネシウム微粉末の製造方法 |
| US4608239A (en) * | 1985-12-06 | 1986-08-26 | Eastman Kodak Company | Removal of iron pentacarbonyl from gaseous streams containing carbon monoxide |
| JPS62171926A (ja) * | 1986-01-22 | 1987-07-28 | Mitsubishi Gas Chem Co Inc | マグネタイト微粒子の製造方法 |
| JPH0832563B2 (ja) * | 1986-03-14 | 1996-03-29 | バスフ アクチェン ゲゼルシャフト | 針状α−Ｆｅ▲下２▼Ｏ▲下３▼の製造方法 |
| US4854981A (en) * | 1987-04-30 | 1989-08-08 | United Technologies Corporation | Iron oxide catalyst and method for making same |
| US4881994A (en) * | 1987-04-30 | 1989-11-21 | United Technologies Corporation | Iron oxide catalyst propellant, and method for making same |
| US5047382A (en) * | 1988-12-12 | 1991-09-10 | United Technologies Corporation | Method for making iron oxide catalyst |
| US5004504A (en) * | 1990-02-26 | 1991-04-02 | Basf | Transparent iron oxide pigments |
-
1990
- 1990-11-27 US US07/618,772 patent/US5169620A/en not_active Expired - Lifetime
-
1991
- 1991-11-21 IL IL10011691A patent/IL100116A/en not_active IP Right Cessation
- 1991-11-26 EP EP19910120168 patent/EP0488157A3/en not_active Withdrawn
- 1991-11-26 JP JP33610791A patent/JP3605418B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP0488157A3 (en) | 1993-06-30 |
| US5169620A (en) | 1992-12-08 |
| IL100116A0 (en) | 1992-08-18 |
| JP3605418B2 (ja) | 2004-12-22 |
| EP0488157A2 (fr) | 1992-06-03 |
| JPH04300216A (ja) | 1992-10-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FF | Patent granted | ||
| KB | Patent renewed | ||
| RH | Patent void |