HUP9700188A1 - Eljárás benzoldikarbonsav-dikloridok előállítására, és a köztitermék - Google Patents

Eljárás benzoldikarbonsav-dikloridok előállítására, és a köztitermék

Info

Publication number
HUP9700188A1
HUP9700188A1 HU9700188A HUP9700188A HUP9700188A1 HU P9700188 A1 HUP9700188 A1 HU P9700188A1 HU 9700188 A HU9700188 A HU 9700188A HU P9700188 A HUP9700188 A HU P9700188A HU P9700188 A1 HUP9700188 A1 HU P9700188A1
Authority
HU
Hungary
Prior art keywords
benzenedicarboxylic acid
acid dichloride
triiodo
amino
carbon atoms
Prior art date
Application number
HU9700188A
Other languages
English (en)
Inventor
Massimo Gagna
Marina Mauro
Carlo Felice Viscardi
Original Assignee
Fructamine S.P.A.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from ITMI951044A external-priority patent/IT1274546B/it
Priority claimed from ITRM950550 external-priority patent/IT1281320B1/it
Application filed by Fructamine S.P.A. filed Critical Fructamine S.P.A.
Publication of HUP9700188A1 publication Critical patent/HUP9700188A1/hu
Publication of HUP9700188A3 publication Critical patent/HUP9700188A3/hu
Publication of HU216548B publication Critical patent/HU216548B/hu

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
    • C07C227/18—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions involving amino or carboxyl groups, e.g. hydrolysis of esters or amides, by formation of halides, salts or esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C381/00—Compounds containing carbon and sulfur and having functional groups not covered by groups C07C301/00 - C07C337/00
    • C07C381/10—Compounds containing sulfur atoms doubly-bound to nitrogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

A találmány eljárásra vőnatkőzik 5-aminő-2,4,6-trijód-1,3-benzőldikarbőnsav-diklőrid előállítására, őly módőn, hőgy 5-aminő-2,4,6-trijód-1,3-benzőldikarbőnsavat és tiőnil-klőridőt heterőgénfázisban reagáltatnak 7-16 szénatőmős, egyenes vagy elágazó szénláncúalifás szénhidrőgének, 7-8 szénatőmős arőmás szénhidrőgének, 1,1,1-triklór-etán, n-bűtil-acetát és diglim (dietilénglikől-éter) közülválasztőtt őldószerben, katalitikűs mennyiségű tercier aminjelenlétében.ŕ
HU9700188A 1995-05-23 1996-05-17 Eljárás benzoldikarbonsav-dikloridok előállítására, és a köztitermék HU216548B (hu)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ITMI951044A IT1274546B (it) 1995-05-23 1995-05-23 Processo per la preparazione del dicloruro dell'acido 5-ammino-2,4,- 6-triiodoisoftalico
ITRM950550 IT1281320B1 (it) 1995-08-04 1995-08-04 Procedimento di preparazione di dicloruro dell'acido 5-ammino-2,4,6- triiodo-1,3-benzendicarbossilico per reazione dell'acido

Publications (3)

Publication Number Publication Date
HUP9700188A1 true HUP9700188A1 (hu) 1998-01-28
HUP9700188A3 HUP9700188A3 (en) 1998-03-02
HU216548B HU216548B (hu) 1999-07-28

Family

ID=26331277

Family Applications (1)

Application Number Title Priority Date Filing Date
HU9700188A HU216548B (hu) 1995-05-23 1996-05-17 Eljárás benzoldikarbonsav-dikloridok előállítására, és a köztitermék

Country Status (22)

Country Link
US (1) US5616795A (hu)
EP (1) EP0773924B1 (hu)
JP (1) JP4012566B2 (hu)
KR (1) KR100255914B1 (hu)
CN (1) CN1157367C (hu)
AT (1) ATE176663T1 (hu)
AU (1) AU702895B2 (hu)
BR (1) BR9606488A (hu)
CA (1) CA2195636C (hu)
CZ (1) CZ290345B6 (hu)
DE (2) DE69601525T2 (hu)
DK (1) DK0773924T3 (hu)
ES (1) ES2103252T3 (hu)
GR (1) GR970300027T1 (hu)
HU (1) HU216548B (hu)
IL (1) IL118359A (hu)
MX (1) MX9700548A (hu)
NO (1) NO313696B1 (hu)
PL (1) PL182447B1 (hu)
SI (1) SI9620012A (hu)
SK (1) SK8797A3 (hu)
WO (1) WO1996037459A1 (hu)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1271107B (it) * 1994-11-29 1997-05-26 Zambon Spa Processo per la preparazione di un intermedio utile nella sintesi di composti organici
IT1292037B1 (it) * 1997-05-30 1999-01-25 Bracco Spa Processo per la preparazione di 5-(acetil 62,3-diidrossipropil)- ammino)-n,n'-bis(2,3-diidrossipropil)-2,4,6-triiodo-1,3-benzen-
EP1966110B1 (en) 2005-12-19 2013-04-24 Ge Healthcare As Purification process of iodixanol
GB0717189D0 (en) * 2007-09-04 2007-10-17 Syngenta Participations Ag Novel processes and compounds
EP2240432B1 (en) * 2008-01-14 2012-07-04 Mallinckrodt LLC Process for the preparation of iosimenol
EP2230227A1 (en) 2009-03-20 2010-09-22 Bracco Imaging S.p.A Process for the preparation of triiodinated carboxylic aromatic derivatives
EP2243767A1 (en) * 2009-04-21 2010-10-27 Bracco Imaging S.p.A Process for the iodination of aromatic compounds
US7999134B2 (en) 2009-07-21 2011-08-16 Ge Healthcare As Crystallization of iodixanol using milling
US7999135B2 (en) 2009-07-21 2011-08-16 Ge Healthcare As Crystallization of iodixanol using ultrasound
KR101699226B1 (ko) 2009-11-26 2017-01-24 호비온 차이나 홀딩 리미티드 이오딕사놀의 제조 및 정제
EP2394984A1 (en) 2010-06-10 2011-12-14 Bracco Imaging S.p.A Process for the iodination of phenolic derivatives
DK2931696T3 (en) 2012-12-11 2018-12-17 Bracco Imaging Spa CONTINUOUS PROCEDURE FOR THE PREPARATION OF (S) -2-ACETYLOXYPROPIONIC ACID
KR102265049B1 (ko) 2013-11-05 2021-06-16 브라코 이미징 에스.피.에이. 이오파미돌의 제조 방법
JP6546609B2 (ja) 2014-06-10 2019-07-17 ブラッコ・イメージング・ソシエタ・ペル・アチオニＢｒａｃｃｏ Ｉｍａｇｉｎｇ Ｓ．Ｐ．Ａ． （ｓ）−２−アセチルオキシプロピオン酸およびその誘導体の製造方法
CN104230731B (zh) * 2014-09-24 2016-01-20 武汉理工大学 造影剂中间体三碘异酞酰氯的制备方法
JP7012722B2 (ja) 2016-12-05 2022-01-28 ブラッコ・イメージング・ソシエタ・ペル・アチオニ 放射線画像診断剤中間体の機械化学的合成

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH608189A5 (hu) * 1974-12-13 1978-12-29 Savac Ag
IT1193211B (it) * 1979-08-09 1988-06-15 Bracco Ind Chimica Spa Derivati dell'acido 2,4,6-triiodo-isoftalico,metodo per la loro preparazione e mezzi di contrasto che li contengono
IT1207226B (it) * 1979-08-09 1989-05-17 Bracco Ind Chimica Spa Derivati dell'acido 2,4,6-triiodo-isoftalico, metodo per la loro preparazione e mezzi di contrasto che li contengono.
US4396598A (en) * 1982-01-11 1983-08-02 Mallinckrodt, Inc. Triiodoisophthalamide X-ray contrast agent
FR2541676A1 (fr) * 1983-02-25 1984-08-31 Guerbet Sa Composes non-ioniques a structures benzenique iodee ou bromee et produits opacifiants en contenant
US5191120A (en) * 1989-12-13 1993-03-02 Mallinckrodt Medical, Inc. Process for preparing nonionic X-ray contrast agents
US5075502A (en) * 1989-12-13 1991-12-24 Mallinckrodt, Inc. Nonionic x-ray contrast agents, compositions and methods
IT1271107B (it) * 1994-11-29 1997-05-26 Zambon Spa Processo per la preparazione di un intermedio utile nella sintesi di composti organici

Also Published As

Publication number Publication date
US5616795A (en) 1997-04-01
AU702895B2 (en) 1999-03-11
KR100255914B1 (ko) 2000-05-01
DE69601525T2 (de) 1999-06-24
DE69601525D1 (de) 1999-03-25
IL118359A0 (en) 1996-09-12
NO970261L (no) 1997-05-02
CN1157367C (zh) 2004-07-14
JP4012566B2 (ja) 2007-11-21
ES2103252T3 (es) 1999-04-01
GR970300027T1 (en) 1997-09-30
PL182447B1 (pl) 2002-01-31
ATE176663T1 (de) 1999-02-15
BR9606488A (pt) 1997-11-25
SI9620012A (en) 1997-06-30
NO970261D0 (no) 1997-01-21
SK8797A3 (en) 1997-08-06
CZ18797A3 (en) 1997-07-16
HU216548B (hu) 1999-07-28
MX9700548A (es) 1997-05-31
DE773924T1 (de) 1997-12-18
CZ290345B6 (cs) 2002-07-17
JPH10508874A (ja) 1998-09-02
WO1996037459A1 (en) 1996-11-28
NO313696B1 (no) 2002-11-18
AU5897896A (en) 1996-12-11
CA2195636A1 (en) 1996-11-28
CA2195636C (en) 2007-10-30
ES2103252T1 (es) 1997-09-16
DK0773924T3 (da) 1999-09-20
EP0773924B1 (en) 1999-02-10
PL318311A1 (en) 1997-06-09
CN1154689A (zh) 1997-07-16
HUP9700188A3 (en) 1998-03-02
EP0773924A1 (en) 1997-05-21
IL118359A (en) 2000-10-31

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HPC4 Succession in title of patentee

Owner name: BRACCO IMAGING S.P.A., IT