HUP0100690A1 - Eljárás lítium-átmenetifém-vegyületek előállítására - Google Patents

Eljárás lítium-átmenetifém-vegyületek előállítására

Info

Publication number
HUP0100690A1
HUP0100690A1 HU0100690A HUP0100690A HUP0100690A1 HU P0100690 A1 HUP0100690 A1 HU P0100690A1 HU 0100690 A HU0100690 A HU 0100690A HU P0100690 A HUP0100690 A HU P0100690A HU P0100690 A1 HUP0100690 A1 HU P0100690A1
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HU
Hungary
Prior art keywords
transition metal
value
metal compounds
production
compound
Prior art date
Application number
HU0100690A
Other languages
English (en)
Inventor
Mathias Benz
Daniel Duff
Ulrich Krynitz
Wolfgang Kummer
Ricarda Leiberich
Juliane Meese-Marktscheffel
Evelyn Pross
Christoph Schild
Josef Schmoll
Wolfgang Schweda
Viktor Stoller
Original Assignee
H.C.Starck Gmbh & Co. Kg
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from PCT/EP1998/000697 external-priority patent/WO1998037023A1/de
Application filed by H.C.Starck Gmbh & Co. Kg filed Critical H.C.Starck Gmbh & Co. Kg
Publication of HUP0100690A1 publication Critical patent/HUP0100690A1/hu
Publication of HUP0100690A3 publication Critical patent/HUP0100690A3/hu

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/12—Complex oxides containing manganese and at least one other metal element
    • C01G45/1221—Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof
    • C01G45/1228—Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof of the type (MnO2)-, e.g. LiMnO2 or Li(MxMn1-x)O2
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/80—Compounds containing nickel, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G53/82—Compounds containing nickel, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/12—Complex oxides containing manganese and at least one other metal element
    • C01G45/1221—Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/20—Compounds containing manganese, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G45/22—Compounds containing manganese, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C01G51/40—Complex oxides containing cobalt and at least one other metal element
    • C01G51/42—Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C01G51/40—Complex oxides containing cobalt and at least one other metal element
    • C01G51/42—Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2
    • C01G51/44—Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2 containing manganese
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C01G51/80—Compounds containing cobalt, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G51/82—Compounds containing cobalt, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/40—Complex oxides containing nickel and at least one other metal element
    • C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/40—Complex oxides containing nickel and at least one other metal element
    • C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • C01G53/44—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/40—Complex oxides containing nickel and at least one other metal element
    • C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • C01G53/44—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
    • C01G53/50—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (MnO2)n-, e.g. Li(NixMn1-x)O2 or Li(MyNixMn1-x-y)O2
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/10—Nitrates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/74—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by peak-intensities or a ratio thereof only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/50—Agglomerated particles
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)

Abstract

A találmány szerinti eljárás (I) általános képletű lítium-átmenetifém-vegyületek LiX(M1yM21-y)nOnz, (I) - amely képletben M1 jelentése nikkel-,kobalt- vagy mangánatom, M2 jelentése króm-, kobalt-, vas-, mangán-,molibdén- vagy alumíniumatom, azzal a megkötéssel, hogy M2 jelentéseM1 jelentésétől eltérő, n értéke 2, ha M1 jelentése mangánatom,egyébként 1, x értéke 0,9 és 1,2 közötti szám, y értéke 0,5 és 1,0közötti szám, és z értéke 1,9 és 2,1 közötti szám - előállításáraszolgál, amelynek során oxigéntartalmú átmenetifém-vegyületek és egyoxigéntartalmú lítiumvegyület alapos keveredésű elegyét, amelyetszilárd, por alakú átmenetifém-vegyület lítiumvegyület oldatávalvégzett kezelése és szárítás útján kapnak, kalcinálják. Az eljárás során legalább az M1-vegyületet legalább 20 m2/g BETfajlagos felületű porként alkalmazzák, és a kalcinálást mozgatottágyban folytatják le. Ó
HU0100690A 1998-02-09 1998-08-13 Method for producing lithium-transition metal mixtures HUP0100690A3 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
PCT/EP1998/000697 WO1998037023A1 (de) 1997-02-19 1998-02-09 Verfahren zur herstellung von lithium-übergangsmetallaten
PCT/EP1998/005150 WO1999040029A1 (de) 1998-02-09 1998-08-13 Verfahren zur herstellung von lithium-übergangsmetallaten

Publications (2)

Publication Number Publication Date
HUP0100690A1 true HUP0100690A1 (hu) 2001-06-28
HUP0100690A3 HUP0100690A3 (en) 2005-03-29

Family

ID=8166867

Family Applications (1)

Application Number Title Priority Date Filing Date
HU0100690A HUP0100690A3 (en) 1998-02-09 1998-08-13 Method for producing lithium-transition metal mixtures

Country Status (12)

Country Link
US (1) US6875416B1 (hu)
EP (1) EP1058673B1 (hu)
JP (1) JP4122710B2 (hu)
KR (1) KR100544541B1 (hu)
CN (1) CN1191994C (hu)
AT (1) ATE264271T1 (hu)
AU (1) AU744558B2 (hu)
CA (1) CA2320155C (hu)
DE (1) DE59811208D1 (hu)
HU (1) HUP0100690A3 (hu)
IL (1) IL137350A0 (hu)
WO (1) WO1999040029A1 (hu)

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KR102725031B1 (ko) * 2017-11-27 2024-11-01 주식회사 엘지에너지솔루션 양극 첨가제, 이의 제조 방법, 이를 포함하는 양극 및 리튬 이차 전지
KR102388848B1 (ko) * 2017-11-30 2022-04-20 주식회사 엘지에너지솔루션 양극 첨가제, 이의 제조 방법, 이를 포함하는 양극 및 리튬 이차 전지
KR102396972B1 (ko) * 2019-05-06 2022-05-12 산동 지스톤 뉴 머티리얼 테크놀로지 컴퍼니 리미티드. 전이 금속 리튬 산화물을 제조하기 위한 방법 및 장치
CN110112400B (zh) * 2019-05-06 2022-10-21 山东泽石新材料科技有限公司 一种过渡金属锂氧化物的制备方法及装置
CN110697801B (zh) 2019-10-29 2020-12-04 山东泽石新材料科技有限公司 一种过渡金属锂氧化合物的制备方法及装置
KR20220127517A (ko) 2021-03-11 2022-09-20 에스케이온 주식회사 리튬 이차 전지용 양극 활물질의 제조 방법
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CN119361889B (zh) * 2024-12-10 2025-09-26 中国科学技术大学 基于电化学的废旧电池回收提锂系统及方法

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HU231726B1 (hu) * 2022-01-28 2025-11-28 Guangdong Brunp Recycling Technology Co., Ltd. Eljárás alumíniummal dópolt katódanyag prekurzor előállítására

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US6875416B1 (en) 2005-04-05
KR100544541B1 (ko) 2006-01-24
EP1058673B1 (de) 2004-04-14
HK1034952A1 (en) 2001-11-09
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AU9262298A (en) 1999-08-23
CA2320155A1 (en) 1999-08-12
EP1058673A1 (de) 2000-12-13
DE59811208D1 (de) 2004-05-19
IL137350A0 (en) 2001-07-24
JP2002502795A (ja) 2002-01-29
CN1284932A (zh) 2001-02-21
ATE264271T1 (de) 2004-04-15
HUP0100690A3 (en) 2005-03-29

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