HUE038965T2 - Eljárás 3-metakriloxipropildimetilklórszilán elõállítására folytonos áramú reaktorban - Google Patents

Eljárás 3-metakriloxipropildimetilklórszilán elõállítására folytonos áramú reaktorban

Info

Publication number
HUE038965T2
HUE038965T2 HUE15738445A HUE15738445A HUE038965T2 HU E038965 T2 HUE038965 T2 HU E038965T2 HU E15738445 A HUE15738445 A HU E15738445A HU E15738445 A HUE15738445 A HU E15738445A HU E038965 T2 HUE038965 T2 HU E038965T2
Authority
HU
Hungary
Prior art keywords
methacryloxypropyldimethylchlorosilane
preparation
continuous flow
flow reactor
reactor
Prior art date
Application number
HUE15738445A
Other languages
English (en)
Inventor
Robert Cracknell
Melissa Matthews
Andrew Small
Adam Barter
Original Assignee
Geo Specialty Chemicals Uk Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Geo Specialty Chemicals Uk Ltd filed Critical Geo Specialty Chemicals Uk Ltd
Publication of HUE038965T2 publication Critical patent/HUE038965T2/hu

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/12Organo silicon halides
    • C07F7/121Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
    • C07F7/122Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving the formation of Si-C linkages
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/1608Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes the ligands containing silicon
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/0834Compounds having one or more O-Si linkage
    • C07F7/0838Compounds with one or more Si-O-Si sequences
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/12Organo silicon halides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/12Organo silicon halides
    • C07F7/14Preparation thereof from optionally substituted halogenated silanes and hydrocarbons hydrosilylation reactions
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04Polysiloxanes
    • C08G77/20Polysiloxanes containing silicon bound to unsaturated aliphatic groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04Polysiloxanes
    • C08G77/38Polysiloxanes modified by chemical after-treatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002Chemical plants
    • B01J2219/00027Process aspects
    • B01J2219/00033Continuous processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/30Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
    • B01J2231/32Addition reactions to C=C or C-C triple bonds
    • B01J2231/323Hydrometalation, e.g. bor-, alumin-, silyl-, zirconation or analoguous reactions like carbometalation, hydrocarbation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82Metals of the platinum group
    • B01J2531/828Platinum

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
HUE15738445A 2014-07-11 2015-07-09 Eljárás 3-metakriloxipropildimetilklórszilán elõállítására folytonos áramú reaktorban HUE038965T2 (hu)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GBGB1412406.9A GB201412406D0 (en) 2014-07-11 2014-07-11 Process

Publications (1)

Publication Number Publication Date
HUE038965T2 true HUE038965T2 (hu) 2018-12-28

Family

ID=51454035

Family Applications (1)

Application Number Title Priority Date Filing Date
HUE15738445A HUE038965T2 (hu) 2014-07-11 2015-07-09 Eljárás 3-metakriloxipropildimetilklórszilán elõállítására folytonos áramú reaktorban

Country Status (7)

Country Link
US (1) US10399997B2 (hu)
EP (1) EP3166952B1 (hu)
JP (1) JP6581177B2 (hu)
ES (1) ES2682747T3 (hu)
GB (1) GB201412406D0 (hu)
HU (1) HUE038965T2 (hu)
WO (1) WO2016005757A1 (hu)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2020094132A (ja) * 2018-12-13 2020-06-18 ダウ・東レ株式会社 加水分解性ケイ素化合物含有組成物、その電気伝導率安定化方法、その用途および製造方法
JP7298446B2 (ja) * 2019-11-07 2023-06-27 信越化学工業株式会社 アクリロイルオキシ基またはメタクリロイルオキシ基を有する有機ケイ素化合物の製造方法
WO2023113779A1 (en) 2021-12-15 2023-06-22 Gelest, Inc. High purity polysiloxane macromers and method for making the same

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL274405A (hu) 1961-02-06 1900-01-01
US3258477A (en) 1963-07-19 1966-06-28 Dow Corning Acryloxyalkylsilanes and compositions thereof
DE2851456C2 (de) * 1978-11-28 1982-09-23 Wacker-Chemie GmbH, 8000 München Verfahren zur Herstellung von Organosiliciumverbindungen
JPS604193A (ja) 1983-06-21 1985-01-10 Kanegafuchi Chem Ind Co Ltd アルコキシシランの連続的製法
US4709067A (en) * 1986-05-20 1987-11-24 Union Carbide Corporation Method for preparing methacryloxy and acryloxy containing organosilanes and organosilicones
US4780555A (en) * 1988-01-04 1988-10-25 Dow Corning Corporation Method for preparing and stabilizing acryl-functional halosilanes
JP2851477B2 (ja) 1992-03-25 1999-01-27 東レ・ダウコーニング・シリコーン株式会社 アクリロキシ基またはメタクリロキシ基含有有機ケイ素化合物の製造方法
US5488142A (en) * 1993-10-04 1996-01-30 Minnesota Mining And Manufacturing Company Fluorination in tubular reactor system
US5359113A (en) 1993-11-08 1994-10-25 Dow Corning Corporation Method for maintaining catalytic activity during a hydrosilylation reaction
JP3445370B2 (ja) 1994-07-18 2003-09-08 東レ・ダウコーニング・シリコーン株式会社 メタクリロキシプロピルジメチルクロロシランの製造方法
DE4434200C2 (de) 1994-09-24 2002-06-27 Degussa Verfahren zur Herstellung von 3-Acryloxypropylalkoxysilanen
US5824195A (en) 1995-07-10 1998-10-20 Chisso Corporation Process for distilling crude acrylic silane solution
US5550272A (en) 1995-10-02 1996-08-27 General Electric Company Method for hydrosilating unsaturated monomers
JPH09143187A (ja) 1995-11-21 1997-06-03 Toray Dow Corning Silicone Co Ltd 高純度メタクリロキシプロピルジメチルクロロシランの製造方法
JP3611668B2 (ja) 1996-04-26 2005-01-19 東レ・ダウコーニング・シリコーン株式会社 アクリル官能性シランの重合禁止剤
US5811565A (en) 1996-04-26 1998-09-22 Dow Corning Toray Silicone Co., Ltd. Method for purifying 3-methacryloxypropyldimethylhalosilanes and 3-methacryloxypropylmethyldihalosilanes
JP4025384B2 (ja) * 1996-12-02 2007-12-19 東レ・ダウコーニング株式会社 3−メタクリロキシプロピルジメチルハロシランまたは3−メタクリロキシプロピルメチルジハロシランの精製方法
JP4123334B2 (ja) * 2001-09-27 2008-07-23 信越化学工業株式会社 カルボン酸3−(ジメチルクロロシリル)プロピルエステルの製造方法
JP4297708B2 (ja) * 2003-03-25 2009-07-15 東レ・ダウコーニング株式会社 アクリロキシ基もしくはメタクリロキシ基含有有機ケイ素化合物の蒸留方法
DE102007023760A1 (de) * 2006-08-10 2008-02-14 Evonik Degussa Gmbh Anlage, Reaktor und Verfahren zur kontinuierlichen industriellen Herstellung von 3-Methacryloxypropylalkoxysilanen
DE102007023757A1 (de) 2006-08-10 2008-02-14 Evonik Degussa Gmbh Anlage und Verfahen zur kontinuierlichen industriellen Herstellung von Organosilanen
CN101157700B (zh) * 2007-11-15 2011-05-04 上海化学试剂研究所 甲基丙烯酰氧丙基二甲基氯硅烷的制备方法
JP5720103B2 (ja) 2010-03-18 2015-05-20 東レ株式会社 シリコーンハイドロゲル、眼用レンズおよびコンタクトレンズ
US9695093B2 (en) * 2014-06-11 2017-07-04 Alireza Shekarriz Hydrothermal conversion process

Also Published As

Publication number Publication date
JP6581177B2 (ja) 2019-09-25
JP2017528424A (ja) 2017-09-28
ES2682747T3 (es) 2018-09-21
EP3166952A1 (en) 2017-05-17
EP3166952B1 (en) 2018-06-06
WO2016005757A1 (en) 2016-01-14
US10399997B2 (en) 2019-09-03
US20170197995A1 (en) 2017-07-13
GB201412406D0 (en) 2014-08-27

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