HUE032843T2 - Szénhidrátok átalakítása hidroximetil-furfurallá (HMF) és származékaivá - Google Patents

Szénhidrátok átalakítása hidroximetil-furfurallá (HMF) és származékaivá Download PDF

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Publication number
HUE032843T2
HUE032843T2 HUE11190670A HUE11190670A HUE032843T2 HU E032843 T2 HUE032843 T2 HU E032843T2 HU E11190670 A HUE11190670 A HU E11190670A HU E11190670 A HUE11190670 A HU E11190670A HU E032843 T2 HUE032843 T2 HU E032843T2
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HU
Hungary
Prior art keywords
hmf
fructose
acid
column
ester
Prior art date
Application number
HUE11190670A
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English (en)
Inventor
Alexandra Sanborn
Stephen Howard
Original Assignee
Archer-Daniels-Midland Company
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First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=40386123&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=HUE032843(T2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Archer-Daniels-Midland Company filed Critical Archer-Daniels-Midland Company
Publication of HUE032843T2 publication Critical patent/HUE032843T2/hu

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C07D307/50—Preparation from natural products
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/42—Singly bound oxygen atoms
    • C07D307/44—Furfuryl alcohol
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/54—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Saccharide Compounds (AREA)
  • Furan Compounds (AREA)
  • Catalysts (AREA)

Claims (5)

  1. S z: 5¾ b a<i almi tgé «y po « to k 1 Eîj&amp;ràs : -hidyoxnneo I -J-fw UiisKkdnd (ÜMH é»réoek 2.5· fatálaikat Urna vyá (i DCA) való sotidálására 3 HMF észter szervez savval való kombinálásával. 85-110 *C kô.zê émelt höntéaékl.««!.» sa U'fe X400-1000 ρχ.»* nu^teî feebalt-eceták mangánétól es náírluro-bmmkl jelenlétében.
  2. 2. Az I. igénypont szerinti eljárás, aboi a HMF éfâter tartalmaz továbbá Hbli d-
  3. 3. Ji&amp; \, vagy 2. igänypöbbsgsribb eljárás:, abat s lIMF:és#srtg|jr esatep alkatengásávgl áá^afe ep1 szénhidnitiorrâs átatakiiasa során, amely îarta!mazJî&amp;: AgyÄtih yrätföÄ Is sgy oklosszer IbbrislegMsIbgiv ?· . tóink ogskü aeenltsd .dies %*. ·. oldAs .i fob* v m î >«,< v .n^at eg) nz »ltd Kuo su kata bisalrmoa egy sxems sav jekn&amp;ében. igy 2-htdro>dmetll» 5» fat fumídehid megfeleld éberét kapjuk.
  4. 4. Ar. 1. igénypont szeriem .:00¾¾. ahol a 2.S~Uiráiidikarboosav termékei szűrés és hepárotáz «ián lényegében bs/ta Fí.X'A sém nvetpfc ki,
  5. 5. A 4. igénypont szedeti eljárás, áltól a kÄbibräjlbsfäs Äozökag ÂfâAsszitepoF kMsiáiyw fruktözt. magas rVsiktóztariájmi: ,|gkorjl^Ä'iÄ%. FytóbA, 41##j|fl; Ä'IÄt- mápC fruktóztnnalmy kiÄfep irmmftásí którerméMeb és melléktermékeil IXdiÉts yáig glökbg vagy udéz. kristályosításának űddolgozóátamaít és melaszt tartalmaz. i. Aa S, Ippypottt szer bűt eyárásypöi s .véohidrát fórrá'· magái tektőSaítalmú kiikoriéaszdftip. .?>. Á szilárd fázisú katalizátort káltoncserélő gyanta tormában biztosítjuk, amely kai ioncserélő gyantát továbbá 20 %--«ál alacsonyabb, csökkentett vmartalom jellemzi. 4. A 3, 5 vagy ö, igénypontok bármelyike szerinti eljárás, ahol a szerves sav eeetsav. propmnsav. vajsav, citrom- vagy szerves disav. *» 4 ‘ tgenvooot wmtís «liánra, ahoi az észtét képződé«*.· imt-i40 °C közötti trememékkteo. körülbelül 90-150 perc alatt történik, és az észtert márts túlnyomásos OMpnnol oxilálluk 3358-0195 kPa í-OO 1000 font négy >etbüsdskt ioomaseo es 8^-it0 "f bőmetOktetve kootlbebil lOO-löO puc közottt időtartamlg.
HUE11190670A 2007-12-12 2008-12-12 Szénhidrátok átalakítása hidroximetil-furfurallá (HMF) és származékaivá HUE032843T2 (hu)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US99694607P 2007-12-12 2007-12-12
US601207P 2007-12-14 2007-12-14

Publications (1)

Publication Number Publication Date
HUE032843T2 true HUE032843T2 (hu) 2017-11-28

Family

ID=40386123

Family Applications (1)

Application Number Title Priority Date Filing Date
HUE11190670A HUE032843T2 (hu) 2007-12-12 2008-12-12 Szénhidrátok átalakítása hidroximetil-furfurallá (HMF) és származékaivá

Country Status (12)

Country Link
US (1) US20090156841A1 (hu)
EP (4) EP2944632A1 (hu)
JP (2) JP2011506478A (hu)
KR (1) KR101576313B1 (hu)
CN (1) CN101896476A (hu)
BR (1) BRPI0819406B1 (hu)
CA (1) CA2708232C (hu)
ES (1) ES2611596T5 (hu)
HU (1) HUE032843T2 (hu)
MX (1) MX2010006504A (hu)
MY (1) MY169437A (hu)
WO (1) WO2009076627A2 (hu)

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* Cited by examiner, † Cited by third party
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