HU185706B - Process for the isolation of flavour and colouring substances from paprika - Google Patents
Process for the isolation of flavour and colouring substances from paprika Download PDFInfo
- Publication number
- HU185706B HU185706B HU821113A HU111382A HU185706B HU 185706 B HU185706 B HU 185706B HU 821113 A HU821113 A HU 821113A HU 111382 A HU111382 A HU 111382A HU 185706 B HU185706 B HU 185706B
- Authority
- HU
- Hungary
- Prior art keywords
- extraction
- process according
- gas phase
- paprika
- pressure
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 40
- 235000008534 Capsicum annuum var annuum Nutrition 0.000 title claims abstract description 27
- 239000000796 flavoring agent Substances 0.000 title claims description 22
- 239000001511 capsicum annuum Substances 0.000 title claims description 20
- 235000019634 flavors Nutrition 0.000 title claims description 13
- 238000004040 coloring Methods 0.000 title claims description 12
- 239000000126 substance Substances 0.000 title claims description 9
- 240000008384 Capsicum annuum var. annuum Species 0.000 title 1
- 238000002955 isolation Methods 0.000 title 1
- 238000000605 extraction Methods 0.000 claims abstract description 42
- 239000002904 solvent Substances 0.000 claims abstract description 39
- 240000004160 Capsicum annuum Species 0.000 claims abstract description 26
- 235000007862 Capsicum baccatum Nutrition 0.000 claims abstract description 5
- 239000001728 capsicum frutescens Substances 0.000 claims abstract description 3
- 239000000975 dye Substances 0.000 claims description 23
- 235000002566 Capsicum Nutrition 0.000 claims description 19
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical group O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 9
- 241000758706 Piperaceae Species 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 9
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 8
- 239000001569 carbon dioxide Substances 0.000 claims description 8
- 239000006002 Pepper Substances 0.000 claims description 7
- 241000722363 Piper Species 0.000 claims description 7
- 235000016761 Piper aduncum Nutrition 0.000 claims description 7
- 235000017804 Piper guineense Nutrition 0.000 claims description 7
- 235000008184 Piper nigrum Nutrition 0.000 claims description 7
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 claims description 6
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 5
- 239000005977 Ethylene Substances 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 2
- 238000000638 solvent extraction Methods 0.000 claims description 2
- 239000011347 resin Substances 0.000 claims 2
- 229920005989 resin Polymers 0.000 claims 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 1
- 239000007858 starting material Substances 0.000 claims 1
- 229910052717 sulfur Inorganic materials 0.000 claims 1
- 239000011593 sulfur Substances 0.000 claims 1
- 239000007789 gas Substances 0.000 description 18
- 239000000284 extract Substances 0.000 description 17
- 235000008504 concentrate Nutrition 0.000 description 11
- 239000012141 concentrate Substances 0.000 description 11
- 239000007788 liquid Substances 0.000 description 11
- YKPUWZUDDOIDPM-SOFGYWHQSA-N capsaicin Chemical class COC1=CC(CNC(=O)CCCC\C=C\C(C)C)=CC=C1O YKPUWZUDDOIDPM-SOFGYWHQSA-N 0.000 description 10
- 239000012071 phase Substances 0.000 description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 7
- 239000003086 colorant Substances 0.000 description 6
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 6
- 235000013599 spices Nutrition 0.000 description 6
- 229960002504 capsaicin Drugs 0.000 description 4
- 235000017663 capsaicin Nutrition 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- 235000013355 food flavoring agent Nutrition 0.000 description 4
- 241000208293 Capsicum Species 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000001390 capsicum minimum Substances 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 239000002537 cosmetic Substances 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 239000013557 residual solvent Substances 0.000 description 3
- 239000000341 volatile oil Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical class N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 239000000576 food coloring agent Substances 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 238000000199 molecular distillation Methods 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000001044 red dye Substances 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 1
- 241000324343 Causa Species 0.000 description 1
- GQPLMRYTRLFLPF-UHFFFAOYSA-N Nitrous Oxide Chemical class [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 description 1
- 208000002193 Pain Diseases 0.000 description 1
- 229930013930 alkaloid Natural products 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 150000008282 halocarbons Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 235000014666 liquid concentrate Nutrition 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000013622 meat product Nutrition 0.000 description 1
- 229960001730 nitrous oxide Drugs 0.000 description 1
- 239000002674 ointment Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0203—Solvent extraction of solids with a supercritical fluid
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/11—Natural spices, flavouring agents or condiments; Extracts thereof obtained by solvent extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
- A23L5/42—Addition of dyes or pigments, e.g. in combination with optical brighteners
- A23L5/43—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Extraction Or Liquid Replacement (AREA)
- Seasonings (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE3114593A DE3114593C1 (de) | 1981-04-10 | 1981-04-10 | Verfahren zur Gewinnung von Aroma- und Farbstoffen aus Paprika |
Publications (2)
Publication Number | Publication Date |
---|---|
HUT28336A HUT28336A (en) | 1983-12-28 |
HU185706B true HU185706B (en) | 1985-03-28 |
Family
ID=6129907
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HU821113A HU185706B (en) | 1981-04-10 | 1982-04-09 | Process for the isolation of flavour and colouring substances from paprika |
Country Status (6)
Country | Link |
---|---|
US (1) | US4400398A (en, 2012) |
DE (1) | DE3114593C1 (en, 2012) |
ES (1) | ES8303049A1 (en, 2012) |
GR (1) | GR76386B (en, 2012) |
HU (1) | HU185706B (en, 2012) |
IT (1) | IT1150772B (en, 2012) |
Families Citing this family (35)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4504503A (en) * | 1981-09-09 | 1985-03-12 | Lever Brothers Company | Fractionation of butterfat using a liquefied gas or a gas in the supercritical state |
JPS60176563A (ja) * | 1984-02-22 | 1985-09-10 | San Ei Chem Ind Ltd | 親油性食用色素の製造法 |
DE3570971D1 (en) * | 1984-03-08 | 1989-07-20 | Givaudan & Cie Sa | Preparation of flavouring extracts |
US4675198A (en) * | 1984-12-31 | 1987-06-23 | The Procter & Gamble Co. | Removal of textured vegetable product off-flavor by supercritical fluid or liquid extraction |
US4647466A (en) * | 1985-06-19 | 1987-03-03 | The Procter & Gamble Company | Process for the production of citrus flavor and aroma compositions |
US4781936A (en) * | 1986-07-09 | 1988-11-01 | Del Monte Corporation | Coloring compositions |
DE3743058A1 (de) * | 1987-12-18 | 1989-06-29 | Krupp Gmbh | Verfahren zur kontinuierlichen extraktion von hoch- bzw. nichtsiedenden aber schmelzenden organischen stoffgemischen |
WO1990001270A1 (en) * | 1988-08-11 | 1990-02-22 | Tothne Papay Valeria | Process for producing light- and heat-resistant, biologically active extracts, juices and products rich in vitamin c, flavour, aroma and colouring substances, as well as for producing pharmaceuticals, cosmetics, foodstuff, nutriments, fodder and materials yielding biological protection containing the above extracts, juices |
DE3902415C2 (de) * | 1988-09-12 | 1994-03-10 | Intech Dr Jodlbauer Ges Fuer I | Verfahren zur Herstellung eines dunkelgefärbten Lebensmittels |
US5092964A (en) * | 1989-02-03 | 1992-03-03 | Campbell Soup Company | Production of low cholesterol butter oil by vapor sparging |
US4997668A (en) * | 1989-05-02 | 1991-03-05 | Campbell Soup Company | Production of low-cholesterol milk fat by solvent extraction |
US5338557A (en) * | 1989-05-16 | 1994-08-16 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of The Environment | Microwave extraction of volatile oils |
CA1336968C (en) * | 1989-05-16 | 1995-09-12 | J. R. Jocelyn Pare | Microwave-assisted natural products extraction |
JPH04144664A (ja) * | 1990-10-05 | 1992-05-19 | Mori Seiyu Kk | レッドペッパーの辛味成分と赤色色素成分の抽出製造方法 |
CA2072400C (en) * | 1991-07-05 | 2003-08-19 | Jayaprakash B. Nair | Supercritical extraction of taxanes |
US5519947A (en) * | 1992-02-10 | 1996-05-28 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of The Environment | Microwave-assisted generation of volatiles, of supercritical fluid, and apparatus therefor |
US5732476A (en) * | 1992-02-10 | 1998-03-31 | Pare; J.R. Jocelyn | Microwave-assisted separations using volatiles, and apparatus therefor |
CA2060931C (en) * | 1992-02-10 | 1996-12-17 | J. R. Jocelyn Pare | Microwave-assisted generation of volatiles, of supercritical fluid, and apparatus therefor |
US5675909A (en) * | 1992-02-10 | 1997-10-14 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of Environment | Microwave-assisted separations using volatiles |
US5884417A (en) * | 1992-02-10 | 1999-03-23 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of The Environment | Microwave-assisted separations using volatiles |
ES2046952B1 (es) * | 1992-07-21 | 1994-11-16 | Superextractos S L | Procedimiento e instalacion para la extraccion de componentes del pimenton por medio de co2 |
US5629045A (en) * | 1992-09-17 | 1997-05-13 | Richard L. Veech | Biodegradable nosiogenic agents for control of non-vertebrate pests |
DE4429506B4 (de) * | 1994-08-19 | 2007-09-13 | Degussa Gmbh | Verfahren zur Extraktion natürlicher Carotinoid-Farbstoffe |
US6060060A (en) * | 1997-01-31 | 2000-05-09 | Bmb Patent Holding Corporation | Analgesic compositions from sweet peppers and methods of use thereof |
US6111108A (en) * | 1997-07-01 | 2000-08-29 | Midwest Research Institute | Extraction of biologically active components from Camptotheca acuminata with supercritical fluids |
US6086888A (en) * | 1998-12-22 | 2000-07-11 | Bmb Patent Holding Corporation | Analgesic compositions from sweet bell peppers and methods of use thereof |
DE10252168B4 (de) * | 2002-11-09 | 2007-01-11 | Degussa Ag | Verwendung eines Verfahrens zur selektiven Abtrennung von flüchtigen Aromastoffen aus einphasigen, flüssigen Ausgangsmaterialien mit einem Fett- und/oder Öl-Gehalt ≦20 Gew.-% |
US7097867B2 (en) | 2003-03-24 | 2006-08-29 | Council Of Scientific And Industrial Research | Process of extracting chili (capsicum) oleoresin |
US7074990B2 (en) * | 2003-06-27 | 2006-07-11 | Agricultural Research Organization, The Volcani Center | Carotenoids rich paprika cultivars |
JP4526244B2 (ja) | 2003-06-30 | 2010-08-18 | ブラザー工業株式会社 | インクジェットヘッド及びインクジェットプリンタ並びにインクジェットヘッドの製造方法 |
BRPI0504594A (pt) * | 2005-10-18 | 2007-07-17 | Univ Rio De Janeiro | processo de extração de carotenóides |
JP2009531331A (ja) * | 2006-03-23 | 2009-09-03 | ハーバルサイエンス シンガポール ピーティーイー. リミテッド | 桂皮種を含む抽出物および方法 |
JP5550907B2 (ja) * | 2006-10-27 | 2014-07-16 | ビー・エム・ビー・パテント・ホールデイング・コーポレイシヨン | 治療組成物およびカプシアノシド型化合物による治療方法 |
KR101526890B1 (ko) * | 2007-04-02 | 2015-06-10 | 주식회사 뉴로피드 | 고추품종으로부터 색소물질 및 캅사이신을 추출하는 방법 |
DE102007033907A1 (de) * | 2007-07-20 | 2009-01-22 | Uhde High Pressure Technologies Gmbh | Naturstoffextraktion |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1493190C3 (de) * | 1963-04-16 | 1980-10-16 | Studiengesellschaft Kohle Mbh, 4330 Muelheim | Verfahren zur Trennung von Stoffgemischen |
US3526509A (en) * | 1966-10-20 | 1970-09-01 | Nisshin Sangyo Co | Capturing and preserving flavor of alcoholic beverages |
US4104409A (en) * | 1971-06-03 | 1978-08-01 | Studiengesellschaft Kohle Mbh | Production of hop extracts |
US4123559A (en) * | 1971-06-03 | 1978-10-31 | Studiengesellschaft Kohle Mbh | Process for the production of spice extracts |
DE2127611C3 (de) * | 1971-06-03 | 1974-11-14 | Studiengesellschaft Kohle Mbh, 4330 Muelheim | Verfahren zur Herstellung von Gewürzextrakten mit natürlicher Zusammensetzung |
CA1012408A (en) * | 1972-11-14 | 1977-06-21 | Dieter Schwengers | Method for degreasing crushed highly starchy fatty vegetable material |
AT331374B (de) * | 1972-12-22 | 1976-08-25 | Studiengesellschaft Kohle Mbh | Verfahren zur gewinnung von fetten und olen aus pflanzlichen und tierischen produkten |
DE2340566C2 (de) * | 1973-08-10 | 1985-11-07 | Peter, Siegfried, Prof.Dr., 8520 Erlangen | Verfahren zur Trennung von Komponenten von Stoffgemischen mit niedrigem Dampfdruck mit Hilfe eines komprimierten Gases unter überkritischen Bedingungen und einer weiteren, den Trenneffekt beeinflussenden Substanz |
HU174943B (hu) * | 1976-06-30 | 1980-04-28 | Vepex Foevallalkozasi Iroda Rt | Sposob poluchenija koncentratov rastitel'nogo belka i pigmenta |
DE2709033C2 (de) * | 1977-03-02 | 1984-07-26 | Degussa Ag, 6000 Frankfurt | Kamillenextrakte und ihre Herstellung |
DE2844781A1 (de) * | 1978-10-13 | 1980-04-24 | Hag Ag | Verfahren zur extraktiven bearbeitung von pflanzlichen und tierischen materialien |
-
1981
- 1981-04-10 DE DE3114593A patent/DE3114593C1/de not_active Expired
-
1982
- 1982-01-20 GR GR67058A patent/GR76386B/el unknown
- 1982-02-25 ES ES509898A patent/ES8303049A1/es not_active Expired
- 1982-04-05 US US06/365,473 patent/US4400398A/en not_active Expired - Fee Related
- 1982-04-06 IT IT20598/82A patent/IT1150772B/it active
- 1982-04-09 HU HU821113A patent/HU185706B/hu unknown
Also Published As
Publication number | Publication date |
---|---|
HUT28336A (en) | 1983-12-28 |
IT8220598A1 (it) | 1983-10-06 |
US4400398A (en) | 1983-08-23 |
ES509898A0 (es) | 1983-02-01 |
IT1150772B (it) | 1986-12-17 |
DE3114593C1 (de) | 1982-12-09 |
GR76386B (en, 2012) | 1984-08-06 |
IT8220598A0 (it) | 1982-04-06 |
ES8303049A1 (es) | 1983-02-01 |
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