GB720166A - Method of preparing the tri-p-aminosalicylate of dihydrostreptomycin - Google Patents
Method of preparing the tri-p-aminosalicylate of dihydrostreptomycinInfo
- Publication number
- GB720166A GB720166A GB3587/51A GB358751A GB720166A GB 720166 A GB720166 A GB 720166A GB 3587/51 A GB3587/51 A GB 3587/51A GB 358751 A GB358751 A GB 358751A GB 720166 A GB720166 A GB 720166A
- Authority
- GB
- United Kingdom
- Prior art keywords
- dihydrostreptomycin
- aminosalicylate
- tri
- aqueous solution
- sulphate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
- C07H15/20—Carbocyclic rings
- C07H15/22—Cyclohexane rings, substituted by nitrogen atoms
- C07H15/238—Cyclohexane rings substituted by two guanidine radicals, e.g. streptomycins
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Dihydrostreptomycin tri-p-aminosalicylate is prepared by admixing in aqueous solution dihydrostreptomycin sulphate with sodium p-aminosalicylate, evaporating to dryness the resulting mixture under reduced pressure excluding light at a temperature below 40 DEG C., treating the residue so obtained with anhydrous methyl alcohol in order to dissolve and separate the dihydrostreptomycin tri-p-aminosalicylate from insoluble sodium sulphate, filtering the mixture and precipitating the desired salt by the addition thereto of anhydrous ethyl ether. Alternatively, dihydrostreptomycin and p-aminosalicyclic acid may be mixed in aqueous solution and the salt isolated as above. Specification 677,365 is referred to.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT720166X | 1950-06-14 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB720166A true GB720166A (en) | 1954-12-15 |
Family
ID=11314966
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3587/51A Expired GB720166A (en) | 1950-06-14 | 1951-02-14 | Method of preparing the tri-p-aminosalicylate of dihydrostreptomycin |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB720166A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1008284B (en) * | 1955-03-30 | 1957-05-16 | Gruenenthal Chemie | Process for the production of low-toxic basic salts of Streptomyces antibiotics |
-
1951
- 1951-02-14 GB GB3587/51A patent/GB720166A/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1008284B (en) * | 1955-03-30 | 1957-05-16 | Gruenenthal Chemie | Process for the production of low-toxic basic salts of Streptomyces antibiotics |
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