GB547409A - Process for the preparation of 4-acetamido-2-hydroxyphenylarsenoxide - Google Patents
Process for the preparation of 4-acetamido-2-hydroxyphenylarsenoxideInfo
- Publication number
- GB547409A GB547409A GB97041A GB97041A GB547409A GB 547409 A GB547409 A GB 547409A GB 97041 A GB97041 A GB 97041A GB 97041 A GB97041 A GB 97041A GB 547409 A GB547409 A GB 547409A
- Authority
- GB
- United Kingdom
- Prior art keywords
- sodium
- acetamino
- acid
- hydroxyphenylthioarsinite
- phenylarsenoxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- ILQZKQTWTGVQPB-UHFFFAOYSA-N N-(4-arsoroso-3-hydroxyphenyl)acetamide Chemical compound CC(=O)NC1=CC=C([As]=O)C(O)=C1 ILQZKQTWTGVQPB-UHFFFAOYSA-N 0.000 title abstract 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 3
- 229910052708 sodium Inorganic materials 0.000 abstract 3
- 239000011734 sodium Substances 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 2
- 230000007935 neutral effect Effects 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- NFCCUEOXFQBDCO-UHFFFAOYSA-N C(=O)(O)C=1C=C(C=CC=1OC)C=1C(=C(C(=C(C=1)[AsH][S-])O)C1=CC(=C(C=C1)OC)C(=O)O)NC(=O)C.[Na+] Chemical compound C(=O)(O)C=1C=C(C=CC=1OC)C=1C(=C(C(=C(C=1)[AsH][S-])O)C1=CC(=C(C=C1)OC)C(=O)O)NC(=O)C.[Na+] NFCCUEOXFQBDCO-UHFFFAOYSA-N 0.000 abstract 1
- QGYDDIZUDBYIOL-UHFFFAOYSA-N C(=O)(O)CC=1C(=C(C(=C(C=1)[AsH][S-])O)CC(=O)O)NC(=O)C.[Na+] Chemical compound C(=O)(O)CC=1C(=C(C(=C(C=1)[AsH][S-])O)CC(=O)O)NC(=O)C.[Na+] QGYDDIZUDBYIOL-UHFFFAOYSA-N 0.000 abstract 1
- ILLWCRYDUSMPDX-UHFFFAOYSA-N N(C(=O)C)C1=CC(=C(C=C1)[As]=O)C(=O)O.[Na] Chemical compound N(C(=O)C)C1=CC(=C(C=C1)[As]=O)C(=O)O.[Na] ILLWCRYDUSMPDX-UHFFFAOYSA-N 0.000 abstract 1
- 125000002252 acyl group Chemical group 0.000 abstract 1
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 125000003236 benzoyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C(*)=O 0.000 abstract 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 abstract 1
- 229940093920 gynecological arsenic compound Drugs 0.000 abstract 1
- 230000003993 interaction Effects 0.000 abstract 1
- BQVCCPGCDUSGOE-UHFFFAOYSA-N phenylarsine oxide Chemical compound O=[As]C1=CC=CC=C1 BQVCCPGCDUSGOE-UHFFFAOYSA-N 0.000 abstract 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical group OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 abstract 1
- IWHZTRZVCDBWTL-UHFFFAOYSA-N trihydroxy(phenyl)-lambda5-arsane Chemical compound C1(=CC=CC=C1)[AsH](O)(O)O IWHZTRZVCDBWTL-UHFFFAOYSA-N 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/66—Arsenic compounds
- C07F9/70—Organo-arsenic compounds
- C07F9/74—Aromatic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
547,409. Organo-arsenic compounds. MAY & BAKER, Ltd., and PHILLIPS, M. A. Jan. 24, 1941, No. 970. [Class 2 (iii)] 4 - Acylamino - 2 - hydroxyphenylarsenoxides are prepared by reacting in aqueous solution a neutral soluble salt of a phenylarsenoxide or phenylarsenious acid containing a nuclear carboxylic or sulphonic acid group with a neutral soluble salt of an arylthioarsinite of the formula wherein X represents an aromatic or aliphatic residue. Examples describe the production of 4-acetamino-2-hydroxyphenylarsenoxide hemihydrate by interaction in water of (1) sodium di - (carboxymethyl) - 4 - acetamino - 2 - hydroxyphenylthioarsinite and sodium pbenzarsenious acid ; (2) sodium di- (o-carboxyphenyl)- 4-acetamino-2-hydroxyphenylthioar - sinite and sodium 4-acetamino-2-carboxy - phenylarsenoxide ; (3) sodium di- (3-carboxy - 4-methoxyphenyl) - 4 - acetamino - 2 - hydroxyphenylthioarsinite and sodium p-benzarsenious acid. The thioarsinites may be prepared by the process of Specification 331,869, [Class 2 (iii). Reference is also made to the benzoyl group as an acyl component.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB97041A GB547409A (en) | 1941-01-24 | 1941-01-24 | Process for the preparation of 4-acetamido-2-hydroxyphenylarsenoxide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB97041A GB547409A (en) | 1941-01-24 | 1941-01-24 | Process for the preparation of 4-acetamido-2-hydroxyphenylarsenoxide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB547409A true GB547409A (en) | 1942-08-26 |
Family
ID=9713722
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB97041A Expired GB547409A (en) | 1941-01-24 | 1941-01-24 | Process for the preparation of 4-acetamido-2-hydroxyphenylarsenoxide |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB547409A (en) |
-
1941
- 1941-01-24 GB GB97041A patent/GB547409A/en not_active Expired
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