GB656303A - Improvements in or relating to the production of dialkoxythiophosphoryl chlorides - Google Patents

Improvements in or relating to the production of dialkoxythiophosphoryl chlorides

Info

Publication number
GB656303A
GB656303A GB2907848A GB2907848A GB656303A GB 656303 A GB656303 A GB 656303A GB 2907848 A GB2907848 A GB 2907848A GB 2907848 A GB2907848 A GB 2907848A GB 656303 A GB656303 A GB 656303A
Authority
GB
United Kingdom
Prior art keywords
dialkoxythiophosphoryl
chlorides
sulphuryl chloride
production
salts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2907848A
Inventor
Richard Frank Ashbolt
Harold Coates
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Solvay Solutions UK Ltd
Original Assignee
Albright and Wilson Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Albright and Wilson Ltd filed Critical Albright and Wilson Ltd
Priority to GB2907848A priority Critical patent/GB656303A/en
Publication of GB656303A publication Critical patent/GB656303A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/06Phosphorus compounds without P—C bonds
    • C07F9/16Esters of thiophosphoric acids or thiophosphorous acids
    • C07F9/165Esters of thiophosphoric acids
    • C07F9/20Esters of thiophosphoric acids containing P-halide groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)

Abstract

Dialkoxythiophosphoryl chlorides are prepared by reacting bis-(dialkoxythiophosphoryl)-disulphides with sulphuryl chloride. The starting materials can be made by the action of a halogen or sulphuryl chloride on 0.0-dialkyl-dithiophosphoric acids or their salts, or alternatively the dialkoxy-thiophosphoryl chlorides can be obtained directly from the acids or their salts by treatment with more than one molecular proportion of sulphuryl chloride. The reaction is preferably carried out in an inert solvent, e.g. carbon tetrachloride, not above room temperature and preferably around 0 DEG C. The alkoxy group preferably contains not more than 3 carbon atoms, and examples are given of the production of the dimethoxy-, diethoxy-and di-isopropoxycompounds. Specification 646,188 is referred to, as well as U.S.A. Specification 2,060,815.
GB2907848A 1948-11-09 1948-11-09 Improvements in or relating to the production of dialkoxythiophosphoryl chlorides Expired GB656303A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB2907848A GB656303A (en) 1948-11-09 1948-11-09 Improvements in or relating to the production of dialkoxythiophosphoryl chlorides

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB2907848A GB656303A (en) 1948-11-09 1948-11-09 Improvements in or relating to the production of dialkoxythiophosphoryl chlorides

Publications (1)

Publication Number Publication Date
GB656303A true GB656303A (en) 1951-08-22

Family

ID=10285802

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2907848A Expired GB656303A (en) 1948-11-09 1948-11-09 Improvements in or relating to the production of dialkoxythiophosphoryl chlorides

Country Status (1)

Country Link
GB (1) GB656303A (en)

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