GB656303A - Improvements in or relating to the production of dialkoxythiophosphoryl chlorides - Google Patents
Improvements in or relating to the production of dialkoxythiophosphoryl chloridesInfo
- Publication number
- GB656303A GB656303A GB2907848A GB2907848A GB656303A GB 656303 A GB656303 A GB 656303A GB 2907848 A GB2907848 A GB 2907848A GB 2907848 A GB2907848 A GB 2907848A GB 656303 A GB656303 A GB 656303A
- Authority
- GB
- United Kingdom
- Prior art keywords
- dialkoxythiophosphoryl
- chlorides
- sulphuryl chloride
- production
- salts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000001805 chlorine compounds Chemical class 0.000 title abstract 2
- YBBRCQOCSYXUOC-UHFFFAOYSA-N sulfuryl dichloride Chemical compound ClS(Cl)(=O)=O YBBRCQOCSYXUOC-UHFFFAOYSA-N 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 2
- 150000007513 acids Chemical class 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 abstract 2
- 125000003545 alkoxy group Chemical group 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 125000001891 dimethoxy group Chemical group [H]C([H])([H])O* 0.000 abstract 1
- 229910052736 halogen Inorganic materials 0.000 abstract 1
- 150000002367 halogens Chemical class 0.000 abstract 1
- 239000012442 inert solvent Substances 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
- C07F9/165—Esters of thiophosphoric acids
- C07F9/20—Esters of thiophosphoric acids containing P-halide groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
Abstract
Dialkoxythiophosphoryl chlorides are prepared by reacting bis-(dialkoxythiophosphoryl)-disulphides with sulphuryl chloride. The starting materials can be made by the action of a halogen or sulphuryl chloride on 0.0-dialkyl-dithiophosphoric acids or their salts, or alternatively the dialkoxy-thiophosphoryl chlorides can be obtained directly from the acids or their salts by treatment with more than one molecular proportion of sulphuryl chloride. The reaction is preferably carried out in an inert solvent, e.g. carbon tetrachloride, not above room temperature and preferably around 0 DEG C. The alkoxy group preferably contains not more than 3 carbon atoms, and examples are given of the production of the dimethoxy-, diethoxy-and di-isopropoxycompounds. Specification 646,188 is referred to, as well as U.S.A. Specification 2,060,815.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2907848A GB656303A (en) | 1948-11-09 | 1948-11-09 | Improvements in or relating to the production of dialkoxythiophosphoryl chlorides |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2907848A GB656303A (en) | 1948-11-09 | 1948-11-09 | Improvements in or relating to the production of dialkoxythiophosphoryl chlorides |
Publications (1)
Publication Number | Publication Date |
---|---|
GB656303A true GB656303A (en) | 1951-08-22 |
Family
ID=10285802
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2907848A Expired GB656303A (en) | 1948-11-09 | 1948-11-09 | Improvements in or relating to the production of dialkoxythiophosphoryl chlorides |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB656303A (en) |
-
1948
- 1948-11-09 GB GB2907848A patent/GB656303A/en not_active Expired
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