GB645832A - Improvements in and relating to the separation of niobium from tantalum - Google Patents
Improvements in and relating to the separation of niobium from tantalumInfo
- Publication number
- GB645832A GB645832A GB463547A GB463547A GB645832A GB 645832 A GB645832 A GB 645832A GB 463547 A GB463547 A GB 463547A GB 463547 A GB463547 A GB 463547A GB 645832 A GB645832 A GB 645832A
- Authority
- GB
- United Kingdom
- Prior art keywords
- niobium
- tantalum
- nitriding
- nitrogen
- relating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/20—Obtaining niobium, tantalum or vanadium
- C22B34/24—Obtaining niobium or tantalum
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
Material containing the pentoxides of niobium and tantalum is treated with a nitriding agent, thereby selectively nitriding the niobium, and the product is treated with chlorine, bromine or iodine or a dissociation compound thereof, converting the niobium nitride into a volatile halide which distils and is condensed, the tantalum remaining as oxide. The nitriding may be effected with ammonia at 500-900 DEG C. or with a nitrogen-hydrogen mixture at 900 DEG C. Overheating in the chlorination stage should be avoided by diluting the halogen with an inert gas such as nitrogen.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB463547A GB645832A (en) | 1947-02-18 | 1947-02-18 | Improvements in and relating to the separation of niobium from tantalum |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB463547A GB645832A (en) | 1947-02-18 | 1947-02-18 | Improvements in and relating to the separation of niobium from tantalum |
Publications (1)
Publication Number | Publication Date |
---|---|
GB645832A true GB645832A (en) | 1950-11-08 |
Family
ID=9780877
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB463547A Expired GB645832A (en) | 1947-02-18 | 1947-02-18 | Improvements in and relating to the separation of niobium from tantalum |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB645832A (en) |
-
1947
- 1947-02-18 GB GB463547A patent/GB645832A/en not_active Expired
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