GB288884A - 1-amino-2, 4-dichloro-anthraquinone and a process of making the same from m-dichloro-benzene and phthalic anhydride together with the intermediate products of such process - Google Patents
1-amino-2, 4-dichloro-anthraquinone and a process of making the same from m-dichloro-benzene and phthalic anhydride together with the intermediate products of such processInfo
- Publication number
- GB288884A GB288884A GB2150127A GB2150127A GB288884A GB 288884 A GB288884 A GB 288884A GB 2150127 A GB2150127 A GB 2150127A GB 2150127 A GB2150127 A GB 2150127A GB 288884 A GB288884 A GB 288884A
- Authority
- GB
- United Kingdom
- Prior art keywords
- dichlor
- acid
- amino
- dichloro
- phthalic anhydride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
- C09B1/16—Amino-anthraquinones
- C09B1/18—Preparation by synthesis of the nucleus
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
288,884. Gubelmann, I., Weiland, H. J., and Stallmann, O. Aug. 15, 1927. 2<1> : 4<1>-Dichlor-2-benzoylbenzoic acid; 2<1> : 4<1>- dichlor-5<1>-nitro-2-benzoylbenzoic acid; 2<1> : 4<1>-dichlor-5<1>-amino-2-benzoyl benzoic acid.-m-Dichlorbenzene is condensed with phthalic anhydride, the resulting 2<1> : 4<1>-dichlor-2-benzoylbenzoic acid is nitrated and then reduced and the 2<1> : 4<1> - dichlor - 5<1> - amino-2-benzoylbenzoic acid finally treated with a dehydrating agent in order to close the ring and produce 1-amino-2: 4-diclloranthraquinone. For the condensation of the m-dichlorbenzene and phthalic anhydride aluminium or ferric chloride may be used. The reduction of the 2<1> : 4<1>-dichlor-5<1>-nitro-2-benzoylbenzoic acid is preferably effected with iron and acetic acid but iron and hydrochloric acid, electrclytic hydrogen, or hydrogen and a catalyst may be employed. For the final ring closure sulphuric acid is used.
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2150127A GB288884A (en) | 1927-08-15 | 1927-08-15 | 1-amino-2, 4-dichloro-anthraquinone and a process of making the same from m-dichloro-benzene and phthalic anhydride together with the intermediate products of such process |
DEN27961D DE565041C (en) | 1927-08-15 | 1927-10-20 | Process for the preparation of 1-amino-2, 4-dichloroanthraquinone |
FR642931D FR642931A (en) | 1927-08-15 | 1927-10-24 | 1-amino-2, 4-dichloro-anthraquinone, process for its manufacture starting from meta-dichloro-benzene and phthalic anhydride and intermediate products of this process |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2150127A GB288884A (en) | 1927-08-15 | 1927-08-15 | 1-amino-2, 4-dichloro-anthraquinone and a process of making the same from m-dichloro-benzene and phthalic anhydride together with the intermediate products of such process |
Publications (1)
Publication Number | Publication Date |
---|---|
GB288884A true GB288884A (en) | 1928-04-19 |
Family
ID=10163993
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2150127A Expired GB288884A (en) | 1927-08-15 | 1927-08-15 | 1-amino-2, 4-dichloro-anthraquinone and a process of making the same from m-dichloro-benzene and phthalic anhydride together with the intermediate products of such process |
Country Status (3)
Country | Link |
---|---|
DE (1) | DE565041C (en) |
FR (1) | FR642931A (en) |
GB (1) | GB288884A (en) |
-
1927
- 1927-08-15 GB GB2150127A patent/GB288884A/en not_active Expired
- 1927-10-20 DE DEN27961D patent/DE565041C/en not_active Expired
- 1927-10-24 FR FR642931D patent/FR642931A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
FR642931A (en) | 1928-09-06 |
DE565041C (en) | 1932-11-25 |
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