GB1507126A - Method and apparatus for indicating embrittlement due to hydrogen permeation during surface treatment processes - Google Patents
Method and apparatus for indicating embrittlement due to hydrogen permeation during surface treatment processesInfo
- Publication number
- GB1507126A GB1507126A GB15021/76A GB1502176A GB1507126A GB 1507126 A GB1507126 A GB 1507126A GB 15021/76 A GB15021/76 A GB 15021/76A GB 1502176 A GB1502176 A GB 1502176A GB 1507126 A GB1507126 A GB 1507126A
- Authority
- GB
- United Kingdom
- Prior art keywords
- membrane electrode
- electrode
- plating
- probe
- embrittlement
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
- G01N27/416—Systems
- G01N27/49—Systems involving the determination of the current at a single specific value, or small range of values, of applied voltage for producing selective measurement of one or more particular ionic species
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Molecular Biology (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Electroplating Methods And Accessories (AREA)
- Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
Abstract
1507126 Metal embrittlement determination ISRAEL AIRCRAFT INDUSTRIES Ltd 13 April 1976 [24 April 1975] 15021/76 Heading G1N An indication of embrittlement of a metal part due to hydrogen permeation during etching or plating is provided by immersing a probe comprising a plurality of electrodes one being a membrane electrode and of the same metal as the part and an electrolyte into the bath during treatment applying a voltage between the electrodes sufficient to oxidize hydrogen diffusing out of the membrane electrode and measuring the probe current. Preferably a counter electrode and optionally a reference electrode are placed in the electrolyte. The inner face of the membrane electrode is maintained positive with respect to the counter electrode and the outer face of the membrane electrode is, in a plating bath, made negative relative to the plating anodes. As shown, the probe comprises insulating plastics (e.g. PTFE) chamber 2 containing 0À2 N NaOH. Membrane electrode 14 is fixed to chamber 2 by nut 16 and has a palladium inner layer connected to lead 19. A platinum foil counter electrode 20 and saturated calomel reference electrode 24 are connected to leads 20, 26 respectively. The sensor is connected to a potentiostat Which maintains the membrane electrode at a positive potential corresponding to a hydrogen partial pressure of 10<SP>-7</SP> - 10<SP>-14</SP> torr.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IL47163A IL47163A (en) | 1975-04-24 | 1975-04-24 | Method and apparatus for indicating embrittlement due to hydrogen permeation during surface treatment processes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1507126A true GB1507126A (en) | 1978-04-12 |
Family
ID=11048199
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB15021/76A Expired GB1507126A (en) | 1975-04-24 | 1976-04-13 | Method and apparatus for indicating embrittlement due to hydrogen permeation during surface treatment processes |
Country Status (5)
| Country | Link |
|---|---|
| DE (1) | DE2617041A1 (en) |
| FR (1) | FR2308930A1 (en) |
| GB (1) | GB1507126A (en) |
| IL (1) | IL47163A (en) |
| IT (1) | IT1063245B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0936465A2 (en) * | 1998-02-10 | 1999-08-18 | Thyssen Krupp Stahl AG | Method and measuring device for testing the reaction of metal samples to hydrogen |
| GB2490395A (en) * | 2011-04-29 | 2012-10-31 | Inst Chemii Fizycznej Polskiej Akademii Nauk | Probe for determining rate of hydrogen permeation |
| CN104330312A (en) * | 2014-11-20 | 2015-02-04 | 西安摩尔石油工程实验室有限公司 | Detection testing device for hydrogen embrittlement resistance of materials |
-
1975
- 1975-04-24 IL IL47163A patent/IL47163A/en unknown
-
1976
- 1976-04-13 GB GB15021/76A patent/GB1507126A/en not_active Expired
- 1976-04-17 DE DE19762617041 patent/DE2617041A1/en not_active Withdrawn
- 1976-04-22 IT IT22567/76A patent/IT1063245B/en active
- 1976-04-22 FR FR7611863A patent/FR2308930A1/en active Granted
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0936465A2 (en) * | 1998-02-10 | 1999-08-18 | Thyssen Krupp Stahl AG | Method and measuring device for testing the reaction of metal samples to hydrogen |
| EP0936465A3 (en) * | 1998-02-10 | 2002-05-02 | ThyssenKrupp Stahl AG | Method and measuring device for testing the reaction of metal samples to hydrogen |
| DE19805194C2 (en) * | 1998-02-10 | 2003-03-06 | Thyssenkrupp Stahl Ag | Test procedure for the hydrogen behavior of metal samples as well as measuring equipment for the implementation of the procedure |
| GB2490395A (en) * | 2011-04-29 | 2012-10-31 | Inst Chemii Fizycznej Polskiej Akademii Nauk | Probe for determining rate of hydrogen permeation |
| CN104330312A (en) * | 2014-11-20 | 2015-02-04 | 西安摩尔石油工程实验室有限公司 | Detection testing device for hydrogen embrittlement resistance of materials |
Also Published As
| Publication number | Publication date |
|---|---|
| IL47163A0 (en) | 1975-08-31 |
| IL47163A (en) | 1977-04-29 |
| FR2308930B3 (en) | 1979-01-12 |
| IT1063245B (en) | 1985-02-11 |
| FR2308930A1 (en) | 1976-11-19 |
| DE2617041A1 (en) | 1976-11-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |