GB1451777A - Process for preparation of secondary aliphatic amines - Google Patents
Process for preparation of secondary aliphatic aminesInfo
- Publication number
- GB1451777A GB1451777A GB5289273A GB5289273A GB1451777A GB 1451777 A GB1451777 A GB 1451777A GB 5289273 A GB5289273 A GB 5289273A GB 5289273 A GB5289273 A GB 5289273A GB 1451777 A GB1451777 A GB 1451777A
- Authority
- GB
- United Kingdom
- Prior art keywords
- hydrogen
- reaction
- alcohol
- gas
- ammonia
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title abstract 4
- 150000005619 secondary aliphatic amines Chemical class 0.000 title abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 6
- 239000007789 gas Substances 0.000 abstract 6
- 239000001257 hydrogen Substances 0.000 abstract 5
- 229910052739 hydrogen Inorganic materials 0.000 abstract 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 4
- 238000006243 chemical reaction Methods 0.000 abstract 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 3
- 229910021529 ammonia Inorganic materials 0.000 abstract 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 229910017052 cobalt Inorganic materials 0.000 abstract 2
- 239000010941 cobalt Substances 0.000 abstract 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 abstract 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 abstract 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 abstract 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 229910052788 barium Inorganic materials 0.000 abstract 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 abstract 1
- 239000010949 copper Substances 0.000 abstract 1
- 238000006356 dehydrogenation reaction Methods 0.000 abstract 1
- 150000002431 hydrogen Chemical class 0.000 abstract 1
- 239000011261 inert gas Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 150000003335 secondary amines Chemical class 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
- B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00027—Process aspects
- B01J2219/00029—Batch processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00105—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling
- B01J2219/00108—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling involving reactant vapours
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2255701A DE2255701C3 (de) | 1972-11-14 | 1972-11-14 | Verfahren zur Herstellung sekundärer aliphatischer Amine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1451777A true GB1451777A (en) | 1976-10-06 |
Family
ID=5861667
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB5289273A Expired GB1451777A (en) | 1972-11-14 | 1973-11-14 | Process for preparation of secondary aliphatic amines |
Country Status (22)
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4207263A (en) * | 1976-10-09 | 1980-06-10 | Basf Aktiengesellschaft | Manufacture of secondary amines by alkylating ammonia with alcohols |
| US4234727A (en) * | 1978-09-01 | 1980-11-18 | Basf Aktiengesellschaft | Preparation of amines |
| EP1101526A3 (en) * | 1999-11-17 | 2001-10-10 | Praxair Technology, Inc. | Batch reactor with on-demand supply of reactive gas |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2645712C2 (de) * | 1976-10-09 | 1983-08-04 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von sekundären Aminen durch Umsetzung von Ammoniak mit primären oder sekundären ein- oder mehrwertigen Alkoholen |
| DE3246978A1 (de) * | 1982-12-18 | 1984-06-20 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von aminen |
| DE19935448B4 (de) * | 1999-07-28 | 2013-08-22 | Oxea Gmbh | Verfahren zur Herstellung sekundärer aliphatischer Amine aus Aldehyden mittlerer Kettenlänge |
| JP6780664B2 (ja) | 2017-12-05 | 2020-11-04 | 日本軽金属株式会社 | 一体型円形防爆弁成形用の電池蓋用アルミニウム合金板およびその製造方法 |
-
1972
- 1972-11-14 DE DE2255701A patent/DE2255701C3/de not_active Expired
-
1973
- 1973-11-08 ES ES420361A patent/ES420361A1/es not_active Expired
- 1973-11-09 DD DD174560A patent/DD108970A5/xx unknown
- 1973-11-09 NL NLAANVRAGE7315381,A patent/NL177109C/xx not_active IP Right Cessation
- 1973-11-09 CH CH1574173A patent/CH590201A5/xx not_active IP Right Cessation
- 1973-11-12 FI FI3477/73A patent/FI61684C/fi active
- 1973-11-12 IT IT31209/73A patent/IT999342B/it active
- 1973-11-12 AR AR250951A patent/AR196568A1/es active
- 1973-11-12 AT AT949073A patent/AT332363B/de not_active IP Right Cessation
- 1973-11-13 CA CA185,586A patent/CA1000742A/en not_active Expired
- 1973-11-13 BR BR8900/73A patent/BR7308900D0/pt unknown
- 1973-11-13 ZA ZA738685A patent/ZA738685B/xx unknown
- 1973-11-13 DK DK613073A patent/DK143333C/da not_active IP Right Cessation
- 1973-11-13 AU AU62420/73A patent/AU6242073A/en not_active Expired
- 1973-11-13 SU SU1971536A patent/SU550975A3/ru active
- 1973-11-13 JP JP48126860A patent/JPS5817739B2/ja not_active Expired
- 1973-11-13 SE SE7315345A patent/SE402761C/xx unknown
- 1973-11-14 YU YU02944/73A patent/YU294473A/xx unknown
- 1973-11-14 FR FR7340416A patent/FR2206311B1/fr not_active Expired
- 1973-11-14 NO NO4376/73A patent/NO138284C/no unknown
- 1973-11-14 BE BE137759A patent/BE807331A/xx not_active IP Right Cessation
- 1973-11-14 GB GB5289273A patent/GB1451777A/en not_active Expired
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4207263A (en) * | 1976-10-09 | 1980-06-10 | Basf Aktiengesellschaft | Manufacture of secondary amines by alkylating ammonia with alcohols |
| US4234727A (en) * | 1978-09-01 | 1980-11-18 | Basf Aktiengesellschaft | Preparation of amines |
| EP1101526A3 (en) * | 1999-11-17 | 2001-10-10 | Praxair Technology, Inc. | Batch reactor with on-demand supply of reactive gas |
Also Published As
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PE20 | Patent expired after termination of 20 years |
Effective date: 19931113 |