GB1403329A - Vapour-phase alkylation in presence of crystalline alumino silicate catalyst - Google Patents
Vapour-phase alkylation in presence of crystalline alumino silicate catalystInfo
- Publication number
- GB1403329A GB1403329A GB1226073A GB1226073A GB1403329A GB 1403329 A GB1403329 A GB 1403329A GB 1226073 A GB1226073 A GB 1226073A GB 1226073 A GB1226073 A GB 1226073A GB 1403329 A GB1403329 A GB 1403329A
- Authority
- GB
- United Kingdom
- Prior art keywords
- benzene
- toluene
- methanol
- alkylating agent
- vapour
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 title abstract 3
- 230000029936 alkylation Effects 0.000 title abstract 2
- 238000005804 alkylation reaction Methods 0.000 title abstract 2
- 239000003054 catalyst Substances 0.000 title abstract 2
- 229910000323 aluminium silicate Inorganic materials 0.000 title 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 9
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 9
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 6
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 3
- 229940100198 alkylating agent Drugs 0.000 abstract 3
- 239000002168 alkylating agent Substances 0.000 abstract 3
- 229910021536 Zeolite Inorganic materials 0.000 abstract 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 abstract 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 abstract 2
- 239000010457 zeolite Substances 0.000 abstract 2
- -1 C5E Aromatic hydrocarbons Chemical class 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 abstract 1
- 239000005977 Ethylene Substances 0.000 abstract 1
- 238000002441 X-ray diffraction Methods 0.000 abstract 1
- 150000001336 alkenes Chemical class 0.000 abstract 1
- 230000002152 alkylating effect Effects 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 239000011230 binding agent Substances 0.000 abstract 1
- FVKGRHSPCZORQC-UHFFFAOYSA-N formaldehyde;toluene Chemical compound O=C.CC1=CC=CC=C1 FVKGRHSPCZORQC-UHFFFAOYSA-N 0.000 abstract 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
- C07C2/86—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon
- C07C2/862—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon the non-hydrocarbon contains only oxygen as hetero-atoms
- C07C2/867—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon the non-hydrocarbon contains only oxygen as hetero-atoms the non-hydrocarbon is an aldehyde or a ketone
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/34—Regenerating or reactivating
- B01J20/3408—Regenerating or reactivating of aluminosilicate molecular sieves
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/08—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the faujasite type, e.g. type X or Y
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
- C07C2/54—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition of unsaturated hydrocarbons to saturated hydrocarbons or to hydrocarbons containing a six-membered aromatic ring with no unsaturation outside the aromatic ring
- C07C2/64—Addition to a carbon atom of a six-membered aromatic ring
- C07C2/66—Catalytic processes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
- C07C2/86—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon
- C07C2/862—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon the non-hydrocarbon contains only oxygen as hetero-atoms
- C07C2/864—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon the non-hydrocarbon contains only oxygen as hetero-atoms the non-hydrocarbon is an alcohol
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
- B01J2229/10—After treatment, characterised by the effect to be obtained
- B01J2229/26—After treatment, characterised by the effect to be obtained to stabilize the total catalyst structure
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
- B01J2229/30—After treatment, characterised by the means used
- B01J2229/42—Addition of matrix or binder particles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2521/00—Catalysts comprising the elements, oxides or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium or hafnium
- C07C2521/02—Boron or aluminium; Oxides or hydroxides thereof
- C07C2521/04—Alumina
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2529/00—Catalysts comprising molecular sieves
- C07C2529/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites, pillared clays
- C07C2529/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- C07C2529/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2529/00—Catalysts comprising molecular sieves
- C07C2529/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites, pillared clays
- C07C2529/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- C07C2529/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups C07C2529/08 - C07C2529/65
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Analytical Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US24836572A | 1972-04-28 | 1972-04-28 | |
| US25277672A | 1972-05-12 | 1972-05-12 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1403329A true GB1403329A (en) | 1975-08-28 |
Family
ID=26939306
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1226073A Expired GB1403329A (en) | 1972-04-28 | 1973-03-14 | Vapour-phase alkylation in presence of crystalline alumino silicate catalyst |
Country Status (7)
| Country | Link |
|---|---|
| JP (1) | JPS5644050B2 (enrdf_load_stackoverflow) |
| CA (1) | CA1000745A (enrdf_load_stackoverflow) |
| DE (1) | DE2321399C2 (enrdf_load_stackoverflow) |
| FR (1) | FR2181940B1 (enrdf_load_stackoverflow) |
| GB (1) | GB1403329A (enrdf_load_stackoverflow) |
| IT (1) | IT982848B (enrdf_load_stackoverflow) |
| NL (1) | NL7305993A (enrdf_load_stackoverflow) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0005315A3 (en) * | 1978-05-08 | 1979-11-28 | Imperial Chemical Industries Limited | Process for the alkylation of aromatic hydrocarbons |
| EP0029652A1 (en) * | 1979-11-20 | 1981-06-03 | Mobil Oil Corporation | Preparation of 2-phenylalkanes |
| WO1997003933A1 (en) * | 1995-07-19 | 1997-02-06 | Amoco Corporation | Conversion of aromatics and olefins |
| WO2019190774A1 (en) * | 2018-03-30 | 2019-10-03 | Exxonmobil Chemical Patents Inc. | Process for co-production of mixed xylenes and high octane c9+ aromatics |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3751504A (en) * | 1972-05-12 | 1973-08-07 | Mobil Oil Corp | Vapor-phase alkylation in presence of crystalline aluminosilicate catalyst with separate transalkylation |
| NZ178543A (en) * | 1974-09-23 | 1978-04-03 | Mobil Oil Corp | Conversion catalyst, crystalline alumin osilicate zeolite containing phosphorus |
| US4016218A (en) * | 1975-05-29 | 1977-04-05 | Mobil Oil Corporation | Alkylation in presence of thermally modified crystalline aluminosilicate catalyst |
| NZ183608A (en) * | 1976-03-31 | 1978-12-18 | Mobil Oil Corp | Aluminosilicate zeolite catalyst for selectine production of para-diakyl substituted benzenes |
| DE2622318C2 (de) * | 1976-05-19 | 1986-01-02 | Mobil Oil Corp., New York, N.Y. | Verfahren zur Alkylierung oder Transalkylierung von aromatischen Kohlenwasserstoffen |
| US4107224A (en) * | 1977-02-11 | 1978-08-15 | Mobil Oil Corporation | Manufacture of ethyl benzene |
| US4393262A (en) * | 1978-12-14 | 1983-07-12 | Mobil Oil Corporation | Production of isopropylbenzene |
| CA1135286A (en) * | 1978-12-14 | 1982-11-09 | Mobil Oil Corporation | Alkylation of aromatic hydrocarbons |
| US4329533A (en) * | 1980-05-05 | 1982-05-11 | Mobil Oil Corporation | Shape selective reactions with zeolite catalysts modified with group IA metals |
| JPS5939836A (ja) * | 1982-08-27 | 1984-03-05 | Toyo Soda Mfg Co Ltd | １，２，４，５−テトラアルキルベンゼンの製造方法 |
| JPS59128210A (ja) * | 1982-12-30 | 1984-07-24 | Asahi Chem Ind Co Ltd | 結晶性アルミノシリケ−ト、その製造方法及びそのアルミノシリケ−トから成るモノアルキルベンゼンのアルキル化用触媒 |
| US6670517B1 (en) * | 2000-08-24 | 2003-12-30 | Exxon Mobil Chemical Patents Inc. | Process for alkylating aromatics |
| IT1392325B1 (it) * | 2008-09-11 | 2012-02-28 | Polimeri Europa Spa | Processo per l'alchilazione di benzene con isopropanolo o miscele di isopropanolo e propilene |
| WO2017104325A1 (ja) | 2015-12-15 | 2017-06-22 | コニカミノルタ株式会社 | 有機エレクトロルミネッセンス素子、有機エレクトロルミネッセンス素子の製造方法、表示装置、照明装置及び有機エレクトロルミネッセンス素子材料 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2351897A (en) * | 1944-06-20 | Typewriter-calculating machine | ||
| US2904607A (en) * | 1957-01-29 | 1959-09-15 | Exxon Research Engineering Co | Alkylation of aromatics |
| GB1161974A (en) * | 1967-04-14 | 1969-08-20 | Mobil Oil Corp | Synthetic Crystalline Aluminosilicate and method of preparing the same |
| US3631120A (en) * | 1969-06-13 | 1971-12-28 | Exxon Research Engineering Co | Alkylation of aromatic hydrocarbons |
-
1973
- 1973-03-14 GB GB1226073A patent/GB1403329A/en not_active Expired
- 1973-03-26 JP JP3364473A patent/JPS5644050B2/ja not_active Expired
- 1973-04-20 FR FR7314504A patent/FR2181940B1/fr not_active Expired
- 1973-04-26 CA CA169,623A patent/CA1000745A/en not_active Expired
- 1973-04-27 NL NL7305993A patent/NL7305993A/xx active Search and Examination
- 1973-04-27 DE DE2321399A patent/DE2321399C2/de not_active Expired
- 1973-04-27 IT IT23539/73A patent/IT982848B/it active
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0005315A3 (en) * | 1978-05-08 | 1979-11-28 | Imperial Chemical Industries Limited | Process for the alkylation of aromatic hydrocarbons |
| EP0029652A1 (en) * | 1979-11-20 | 1981-06-03 | Mobil Oil Corporation | Preparation of 2-phenylalkanes |
| US4301317A (en) | 1979-11-20 | 1981-11-17 | Mobil Oil Corporation | Preparation of 2-phenylalkanes |
| WO1997003933A1 (en) * | 1995-07-19 | 1997-02-06 | Amoco Corporation | Conversion of aromatics and olefins |
| NL1003627C2 (nl) * | 1995-07-19 | 1997-03-21 | Amoco Corp | Conversie van aromaten en olefinen. |
| US5792894A (en) * | 1995-07-19 | 1998-08-11 | Amoco Corporation | Conversion of aromatic and olefins |
| WO2019190774A1 (en) * | 2018-03-30 | 2019-10-03 | Exxonmobil Chemical Patents Inc. | Process for co-production of mixed xylenes and high octane c9+ aromatics |
| CN111954652A (zh) * | 2018-03-30 | 2020-11-17 | 埃克森美孚化学专利公司 | 混合二甲苯和高辛烷值c9+芳族化合物的共同制备方法 |
| US11053176B2 (en) | 2018-03-30 | 2021-07-06 | Exxonmobil Chemical Patents Inc. | Process for co-production of mixed xylenes and high octane C9+ aromatics |
| CN111954652B (zh) * | 2018-03-30 | 2022-11-08 | 埃克森美孚化学专利公司 | 混合二甲苯和高辛烷值c9+芳族化合物的共同制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| IT982848B (it) | 1974-10-21 |
| DE2321399A1 (de) | 1973-11-15 |
| DE2321399C2 (de) | 1982-09-16 |
| FR2181940B1 (enrdf_load_stackoverflow) | 1977-02-04 |
| CA1000745A (en) | 1976-11-30 |
| JPS4920124A (enrdf_load_stackoverflow) | 1974-02-22 |
| JPS5644050B2 (enrdf_load_stackoverflow) | 1981-10-16 |
| FR2181940A1 (enrdf_load_stackoverflow) | 1973-12-07 |
| NL7305993A (enrdf_load_stackoverflow) | 1973-10-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PE20 | Patent expired after termination of 20 years |
Effective date: 19930313 |