GB1389905A - Production of high purity fission product molybdenum-99 - Google Patents
Production of high purity fission product molybdenum-99Info
- Publication number
- GB1389905A GB1389905A GB3050772A GB3050772A GB1389905A GB 1389905 A GB1389905 A GB 1389905A GB 3050772 A GB3050772 A GB 3050772A GB 3050772 A GB3050772 A GB 3050772A GB 1389905 A GB1389905 A GB 1389905A
- Authority
- GB
- United Kingdom
- Prior art keywords
- solution
- june
- dissolving
- contacting
- precipitate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- ZOKXTWBITQBERF-AKLPVKDBSA-N Molybdenum Mo-99 Chemical compound [99Mo] ZOKXTWBITQBERF-AKLPVKDBSA-N 0.000 title abstract 5
- 230000004992 fission Effects 0.000 title abstract 2
- 229950009740 molybdenum mo-99 Drugs 0.000 title abstract 2
- 239000000243 solution Substances 0.000 abstract 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 abstract 2
- 239000003463 adsorbent Substances 0.000 abstract 2
- 239000012535 impurity Substances 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 150000007522 mineralic acids Chemical class 0.000 abstract 2
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 abstract 2
- WAKHLWOJMHVUJC-SQFISAMPSA-N (2z)-2-hydroxyimino-1,2-diphenylethanol Chemical compound C=1C=CC=CC=1C(=N/O)/C(O)C1=CC=CC=C1 WAKHLWOJMHVUJC-SQFISAMPSA-N 0.000 abstract 1
- 229910018072 Al 2 O 3 Inorganic materials 0.000 abstract 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- GKLVYJBZJHMRIY-OUBTZVSYSA-N Technetium-99 Chemical compound [99Tc] GKLVYJBZJHMRIY-OUBTZVSYSA-N 0.000 abstract 1
- 229910010413 TiO 2 Inorganic materials 0.000 abstract 1
- 229910052770 Uranium Inorganic materials 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 239000012670 alkaline solution Substances 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
- ILRRQNADMUWWFW-UHFFFAOYSA-K aluminium phosphate Chemical compound O1[Al]2OP1(=O)O2 ILRRQNADMUWWFW-UHFFFAOYSA-K 0.000 abstract 1
- 229940001007 aluminium phosphate Drugs 0.000 abstract 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract 1
- 229910000323 aluminium silicate Inorganic materials 0.000 abstract 1
- 235000012211 aluminium silicate Nutrition 0.000 abstract 1
- 239000003610 charcoal Substances 0.000 abstract 1
- 239000003638 chemical reducing agent Substances 0.000 abstract 1
- 238000003745 diagnosis Methods 0.000 abstract 1
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 abstract 1
- 229910001410 inorganic ion Inorganic materials 0.000 abstract 1
- 150000002500 ions Chemical class 0.000 abstract 1
- 230000001678 irradiating effect Effects 0.000 abstract 1
- 229910017604 nitric acid Inorganic materials 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 230000002285 radioactive effect Effects 0.000 abstract 1
- 150000003303 ruthenium Chemical class 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000000741 silica gel Substances 0.000 abstract 1
- 229910002027 silica gel Inorganic materials 0.000 abstract 1
- 229910052709 silver Inorganic materials 0.000 abstract 1
- 239000004332 silver Substances 0.000 abstract 1
- 235000010265 sodium sulphite Nutrition 0.000 abstract 1
- 229910001220 stainless steel Inorganic materials 0.000 abstract 1
- 239000010935 stainless steel Substances 0.000 abstract 1
- 239000001117 sulphuric acid Substances 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
- 229940056501 technetium 99m Drugs 0.000 abstract 1
- JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21G—CONVERSION OF CHEMICAL ELEMENTS; RADIOACTIVE SOURCES
- G21G1/00—Arrangements for converting chemical elements by electromagnetic radiation, corpuscular radiation or particle bombardment, e.g. producing radioactive isotopes
- G21G1/04—Arrangements for converting chemical elements by electromagnetic radiation, corpuscular radiation or particle bombardment, e.g. producing radioactive isotopes outside nuclear reactors or particle accelerators
- G21G1/06—Arrangements for converting chemical elements by electromagnetic radiation, corpuscular radiation or particle bombardment, e.g. producing radioactive isotopes outside nuclear reactors or particle accelerators by neutron irradiation
- G21G1/08—Arrangements for converting chemical elements by electromagnetic radiation, corpuscular radiation or particle bombardment, e.g. producing radioactive isotopes outside nuclear reactors or particle accelerators by neutron irradiation accompanied by nuclear fission
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G39/00—Compounds of molybdenum
- C01G39/003—Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- General Engineering & Computer Science (AREA)
- High Energy & Nuclear Physics (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US00158396A US3799883A (en) | 1971-06-30 | 1971-06-30 | Production of high purity fission product molybdenum-99 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1389905A true GB1389905A (en) | 1975-04-09 |
Family
ID=22567913
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3050772A Expired GB1389905A (en) | 1971-06-30 | 1972-06-29 | Production of high purity fission product molybdenum-99 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US3799883A (enrdf_load_stackoverflow) |
| JP (1) | JPS517800B1 (enrdf_load_stackoverflow) |
| BE (1) | BE785637A (enrdf_load_stackoverflow) |
| CA (1) | CA969373A (enrdf_load_stackoverflow) |
| DE (1) | DE2231976C3 (enrdf_load_stackoverflow) |
| FR (1) | FR2157781B1 (enrdf_load_stackoverflow) |
| GB (1) | GB1389905A (enrdf_load_stackoverflow) |
| IL (1) | IL39793A (enrdf_load_stackoverflow) |
| NL (1) | NL172495C (enrdf_load_stackoverflow) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4659477A (en) * | 1982-08-16 | 1987-04-21 | Pedro B. Macedo | Fixation of anionic materials with a complexing agent |
| RU2145127C1 (ru) * | 1998-02-26 | 2000-01-27 | Российский научный центр "Курчатовский институт" | Способ получения и выделения осколочного молибдена-99 из жидкой гомогенной фазы, содержащей уран |
| RU2489501C1 (ru) * | 2011-12-01 | 2013-08-10 | Общество с ограниченной ответственностью "Прайм-Инвест" | СОСТАВ ЭКСТРАКЦИОННО-ХРОМАТОГРАФИЧЕСКОГО МАТЕРИАЛА ДЛЯ СЕЛЕКТИВНОГО ИЗВЛЕЧЕНИЯ Мo-99 ИЗ ОБЛУЧЕННОГО УРАНОВОГО ТОПЛИВА |
Families Citing this family (44)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4010109A (en) * | 1973-07-02 | 1977-03-01 | Kurt Sauerwein | Device for marking fluent materials |
| GB1531985A (en) * | 1975-03-06 | 1978-11-15 | Radiochemical Centre Ltd | Technetium-99m |
| DE2610948C3 (de) * | 1976-03-16 | 1980-01-10 | Kernforschungszentrum Karlsruhe Gmbh, 7500 Karlsruhe | Verfahren zur Gewinnung von Molybdän -99 aus mit Neutronen bestrahlter, spaltbare Stoffe und Spaltprodukte enthaltender Matrix |
| DE2610947C3 (de) * | 1976-03-16 | 1980-01-10 | Kernforschungszentrum Karlsruhe Gmbh, 7500 Karlsruhe | Verfahren zur Gewinnung von Molybdän-99 aus mit Neutronen bestrahlter, spaltbare Stoffe und Spaltprodukte enthaltender Matrix |
| US4199551A (en) * | 1978-01-13 | 1980-04-22 | Amax Inc. | Recovery of molybdenum and uranium from activated charcoal containing molybdenum and residual uranium |
| JPS5525844U (enrdf_load_stackoverflow) * | 1978-08-10 | 1980-02-19 | ||
| DK151919C (da) * | 1979-06-28 | 1988-08-15 | Radiometer As | Fremgangsmaade, referencevaeske og referencevaeskesystem til samtidig kalibrering og/eller kvalitetskontrol af calciumfoelsomme elektroder og ph-elektroder |
| FR2531060B1 (fr) * | 1982-07-28 | 1986-07-04 | Cogema | Procede de recuperation du molybdene sur charbon actif, a partir d'une solution uranifere acide contenant plus de molybdene que d'uranium |
| JPS59114881U (ja) * | 1983-01-24 | 1984-08-03 | 株式会社貝印刃物開発センター | さやの支持構造 |
| FR2575585B1 (fr) * | 1984-12-28 | 1987-01-30 | Commissariat Energie Atomique | Procede de recuperation de molybdene-99 a partir d'une cible d'alliage d'uranium irradie |
| FR2583403B1 (fr) * | 1985-06-13 | 1988-11-10 | Pechiney Uranium | Procede de separation, par precipitation, du molybdene contenu dans des solutions sulfuriques ou nitriques d'uranium. |
| DE3616391A1 (de) * | 1986-05-15 | 1987-11-19 | Kernforschungsz Karlsruhe | Verfahren zur feinreinigung von spaltmolybdaen |
| US4839133A (en) * | 1987-10-26 | 1989-06-13 | The United States Of America As Represented By The Department Of Energy | Target and method for the production of fission product molybdenum-99 |
| EP0779628A3 (en) * | 1995-12-11 | 1997-07-09 | Institut National des Radioéléments, Nationaal Instituut voor Radio-elementen | Method of stabilizing an aqueous solution of 99Mo molybdate |
| US5802439A (en) * | 1997-02-19 | 1998-09-01 | Lockheed Martin Idaho Technologies Company | Method for the production of 99m Tc compositions from 99 Mo-containing materials |
| US5802438A (en) * | 1997-02-19 | 1998-09-01 | Lockheed Martin Idaho Technologies Company | Method for generating a crystalline 99 MoO3 product and the isolation 99m Tc compositions therefrom |
| IT1316223B1 (it) * | 2000-09-28 | 2003-04-03 | Carlo Rubbia | Metodo e dispositivo per riscaldare gas da uno strato sottile dicombustibile nucleare e propulsore spaziale che utilizza tale metodo. |
| US8666015B2 (en) | 2001-05-08 | 2014-03-04 | The Curators Of The University Of Missouri | Method and apparatus for generating thermal neutrons using an electron accelerator |
| US20060023829A1 (en) * | 2004-08-02 | 2006-02-02 | Battelle Memorial Institute | Medical radioisotopes and methods for producing the same |
| US8497683B2 (en) * | 2006-10-03 | 2013-07-30 | Invensys Systems, Inc. | Spectroscopic sample analyzer and sample handling system |
| RU2313838C1 (ru) * | 2006-12-29 | 2007-12-27 | Институт ядерных исследований РАН ИЯИ РАН | Способ получения радиоолова в состоянии без носителя и мишень для его осуществления (варианты) |
| WO2009100063A2 (en) | 2008-02-05 | 2009-08-13 | The Curators Of The University Of Missouri | Radioisotope production and treatment of solution of target material |
| KR20160072846A (ko) * | 2008-05-02 | 2016-06-23 | 샤인 메디컬 테크놀로지스, 인크. | 의료용 동위원소를 생산하는 디바이스 및 방법 |
| RU2393564C2 (ru) * | 2008-09-12 | 2010-06-27 | Учреждение Российской Академии Наук Институт Ядерных Исследований Ран (Ияи Ран) | Мишень для получения радионуклидов и способ ее изготовления (варианты) |
| US20100169134A1 (en) * | 2008-12-31 | 2010-07-01 | Microsoft Corporation | Fostering enterprise relationships |
| US9691511B1 (en) * | 2009-11-09 | 2017-06-27 | Sandia Corporation | Target-fueled nuclear reactor for medical isotope production |
| US10978214B2 (en) | 2010-01-28 | 2021-04-13 | SHINE Medical Technologies, LLC | Segmented reaction chamber for radioisotope production |
| EP2536664B1 (en) * | 2010-02-19 | 2018-09-26 | Babcock & Wilcox | Method and apparatus for the extraction and processing of molybdenum-99 |
| US9240253B2 (en) * | 2010-04-07 | 2016-01-19 | Ge-Hitachi Nuclear Energy Americas Llc | Column geometry to maximize elution efficiencies for molybdenum-99 |
| EP2398023A1 (en) | 2010-06-21 | 2011-12-21 | The European Union, represented by the European Commission | Production of molybdenum-99 |
| GB201013142D0 (en) | 2010-08-04 | 2010-09-22 | Mallinckrodt Inc | Purification process |
| DE102011002265B4 (de) * | 2011-04-26 | 2012-12-06 | Technische Universität München | Verfahren zur Herstellung von Ausgangsmaterial für einen Technetium-Generator |
| US10734126B2 (en) * | 2011-04-28 | 2020-08-04 | SHINE Medical Technologies, LLC | Methods of separating medical isotopes from uranium solutions |
| GB201112051D0 (en) * | 2011-07-13 | 2011-08-31 | Mallinckrodt Llc | Process |
| JP5888781B2 (ja) * | 2011-11-14 | 2016-03-22 | 国立研究開発法人日本原子力研究開発機構 | 放射性モリブデンの作製方法 |
| KR102172861B1 (ko) | 2012-04-05 | 2020-11-02 | 샤인 메디컬 테크놀로지스, 인크. | 수성 집합체 및 제어 방법 |
| US9330800B2 (en) * | 2012-12-03 | 2016-05-03 | Wisconsin Alumni Research Foundation | Dry phase reactor for generating medical isotopes |
| US9997267B2 (en) | 2013-02-13 | 2018-06-12 | Battelle Memorial Institute | Nuclear reactor target assemblies, nuclear reactor configurations, and methods for producing isotopes, modifying materials within target material, and/or characterizing material within a target material |
| US9793023B2 (en) | 2013-09-26 | 2017-10-17 | Los Alamos National Security, Llc | Recovery of uranium from an irradiated solid target after removal of molybdenum-99 produced from the irradiated target |
| US9842664B2 (en) | 2013-09-26 | 2017-12-12 | Los Alamos National Security, Llc | Recovering and recycling uranium used for production of molybdenum-99 |
| CN109285616B (zh) * | 2018-11-16 | 2020-08-21 | 中国原子能科学研究院 | 从235U裂变产物中提取99Mo的装置及利用该装置提取99Mo的方法 |
| US12040102B2 (en) * | 2020-04-16 | 2024-07-16 | Uchicago Argonne, Llc | Technetium-99M generator for enriched molybdenum |
| US12195825B2 (en) * | 2020-06-30 | 2025-01-14 | Uchicago Argonne, Llc | System and method for producing molybdenum 99 |
| EP3985686B1 (en) | 2020-10-14 | 2022-11-30 | Narodowe Centrum Badan Jadrowych | Method of preparation of the uranium target for the production of molybdenum, molybdenum production process and the uranium target for the production of molybdenum |
-
1971
- 1971-06-30 US US00158396A patent/US3799883A/en not_active Expired - Lifetime
-
1972
- 1972-05-25 CA CA142,933A patent/CA969373A/en not_active Expired
- 1972-06-29 IL IL39793A patent/IL39793A/xx unknown
- 1972-06-29 NL NLAANVRAGE7209050,A patent/NL172495C/xx not_active IP Right Cessation
- 1972-06-29 DE DE2231976A patent/DE2231976C3/de not_active Expired
- 1972-06-29 GB GB3050772A patent/GB1389905A/en not_active Expired
- 1972-06-29 FR FR7223546A patent/FR2157781B1/fr not_active Expired
- 1972-06-29 BE BE785637A patent/BE785637A/xx not_active IP Right Cessation
- 1972-06-29 JP JP47064558A patent/JPS517800B1/ja active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4659477A (en) * | 1982-08-16 | 1987-04-21 | Pedro B. Macedo | Fixation of anionic materials with a complexing agent |
| RU2145127C1 (ru) * | 1998-02-26 | 2000-01-27 | Российский научный центр "Курчатовский институт" | Способ получения и выделения осколочного молибдена-99 из жидкой гомогенной фазы, содержащей уран |
| RU2489501C1 (ru) * | 2011-12-01 | 2013-08-10 | Общество с ограниченной ответственностью "Прайм-Инвест" | СОСТАВ ЭКСТРАКЦИОННО-ХРОМАТОГРАФИЧЕСКОГО МАТЕРИАЛА ДЛЯ СЕЛЕКТИВНОГО ИЗВЛЕЧЕНИЯ Мo-99 ИЗ ОБЛУЧЕННОГО УРАНОВОГО ТОПЛИВА |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2231976A1 (de) | 1973-01-11 |
| IL39793A0 (en) | 1972-09-28 |
| NL7209050A (enrdf_load_stackoverflow) | 1973-01-03 |
| BE785637A (fr) | 1972-12-29 |
| FR2157781A1 (enrdf_load_stackoverflow) | 1973-06-08 |
| CA969373A (en) | 1975-06-17 |
| NL172495C (nl) | 1983-09-01 |
| IL39793A (en) | 1976-01-30 |
| NL172495B (nl) | 1983-04-05 |
| FR2157781B1 (enrdf_load_stackoverflow) | 1976-10-29 |
| JPS517800B1 (enrdf_load_stackoverflow) | 1976-03-11 |
| US3799883A (en) | 1974-03-26 |
| DE2231976B2 (de) | 1979-07-19 |
| DE2231976C3 (de) | 1980-03-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PE20 | Patent expired after termination of 20 years |