GB1197544A - Process for the Preparation of Triglycidyl Isocyanurate - Google Patents
Process for the Preparation of Triglycidyl IsocyanurateInfo
- Publication number
- GB1197544A GB1197544A GB28007/68A GB2800768A GB1197544A GB 1197544 A GB1197544 A GB 1197544A GB 28007/68 A GB28007/68 A GB 28007/68A GB 2800768 A GB2800768 A GB 2800768A GB 1197544 A GB1197544 A GB 1197544A
- Authority
- GB
- United Kingdom
- Prior art keywords
- epichlorohydrin
- reaction
- isocyanurate
- chloro
- catalyst
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- OUPZKGBUJRBPGC-UHFFFAOYSA-N 1,3,5-tris(oxiran-2-ylmethyl)-1,3,5-triazinane-2,4,6-trione Chemical compound O=C1N(CC2OC2)C(=O)N(CC2OC2)C(=O)N1CC1CO1 OUPZKGBUJRBPGC-UHFFFAOYSA-N 0.000 title abstract 6
- 238000002360 preparation method Methods 0.000 title abstract 2
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 abstract 9
- 238000006243 chemical reaction Methods 0.000 abstract 6
- 239000003054 catalyst Substances 0.000 abstract 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 abstract 4
- 239000011541 reaction mixture Substances 0.000 abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 4
- -1 3-chloro-2-hydroxypropyl groups Chemical group 0.000 abstract 3
- 229910000039 hydrogen halide Inorganic materials 0.000 abstract 3
- 239000012433 hydrogen halide Substances 0.000 abstract 3
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 abstract 3
- DEWLEGDTCGBNGU-UHFFFAOYSA-N 1,3-dichloropropan-2-ol Chemical compound ClCC(O)CCl DEWLEGDTCGBNGU-UHFFFAOYSA-N 0.000 abstract 2
- 235000011187 glycerol Nutrition 0.000 abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 1
- 239000000654 additive Substances 0.000 abstract 1
- 230000000996 additive effect Effects 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 abstract 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 1
- 239000002585 base Substances 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 238000009833 condensation Methods 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 abstract 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 abstract 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract 1
- 125000001453 quaternary ammonium group Chemical group 0.000 abstract 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 abstract 1
- 150000003512 tertiary amines Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/30—Only oxygen atoms
- C07D251/34—Cyanuric or isocyanuric esters
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Epoxy Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH837167A CH488727A (de) | 1967-06-13 | 1967-06-13 | Verfahren zur Herstellung von Triglycidyl-isocyanurat |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1197544A true GB1197544A (en) | 1970-07-08 |
Family
ID=4339284
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB28007/68A Expired GB1197544A (en) | 1967-06-13 | 1968-06-12 | Process for the Preparation of Triglycidyl Isocyanurate |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US3547918A (enExample) |
| AT (1) | AT278833B (enExample) |
| BE (1) | BE716464A (enExample) |
| CH (1) | CH488727A (enExample) |
| DE (1) | DE1770510C3 (enExample) |
| ES (1) | ES354972A1 (enExample) |
| FR (1) | FR1570826A (enExample) |
| GB (1) | GB1197544A (enExample) |
| NL (1) | NL6808252A (enExample) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2413722C3 (de) * | 1974-03-21 | 1982-04-08 | Bayer Ag, 5090 Leverkusen | Neue 1-(4-Phenoxy-phenyl)-1,3,5-triazin-Derivate, ein Verfahren zu ihrer Herstellung sowie ihre Anwendung als Arzneimittel |
| GB8429686D0 (en) * | 1984-11-23 | 1985-01-03 | Int Paint Plc | Dispersants |
| JPS62187463A (ja) * | 1986-02-13 | 1987-08-15 | Nissan Chem Ind Ltd | トリグリシジルイソシアヌレ−トの固化方法 |
| TWI225059B (en) * | 1998-04-20 | 2004-12-11 | Nissan Chemical Ind Ltd | beta-form tris-(2,3-epoxypropyl)-isocyanurate crystals and process for their production |
| TW550263B (en) * | 1998-09-01 | 2003-09-01 | Nissan Chemical Ind Ltd | Method for reducing an organic solvent remaining in tris-(2,3-epoxypropyl)-isocyanurate crystals |
| CN102964341B (zh) * | 2012-11-28 | 2016-02-24 | 黄山锦峰实业有限公司 | 异氰尿酸三缩水甘油酯的生产系统 |
| CN104327058B (zh) * | 2014-08-07 | 2017-08-25 | 黄山锦峰实业有限公司 | 异氰尿酸三缩水甘油酯的制备方法 |
| CN113307802B (zh) * | 2021-06-10 | 2023-10-27 | 黄山友谊南海新材料有限公司 | 一种高纯度异氰脲酸三缩水甘油酯的加工方法 |
| CN113244854B (zh) * | 2021-06-10 | 2024-10-29 | 黄山友谊南海新材料有限公司 | 一种高纯度tgic加工系统 |
| CN115445657B (zh) * | 2022-10-08 | 2023-08-15 | 安徽泓泽新材料科技有限公司 | 一种用于呔哔克合成的催化剂及其制备方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2809942A (en) * | 1955-10-21 | 1957-10-15 | Devoe & Raynolds Co | Process for making polyglycidyl cyanurates |
| NL302361A (enExample) * | 1963-01-31 | |||
| DE1211650B (de) * | 1964-07-16 | 1966-03-03 | Henkel & Cie Gmbh | Verfahren zur Herstellung von kristallisiertem Triglycidylisocyanurat |
-
1967
- 1967-06-13 CH CH837167A patent/CH488727A/de not_active IP Right Cessation
-
1968
- 1968-05-28 DE DE1770510A patent/DE1770510C3/de not_active Expired
- 1968-06-11 US US735996A patent/US3547918A/en not_active Expired - Lifetime
- 1968-06-11 FR FR1570826D patent/FR1570826A/fr not_active Expired
- 1968-06-12 GB GB28007/68A patent/GB1197544A/en not_active Expired
- 1968-06-12 AT AT562068A patent/AT278833B/de not_active IP Right Cessation
- 1968-06-12 ES ES0354972A patent/ES354972A1/es not_active Expired
- 1968-06-12 NL NL6808252A patent/NL6808252A/xx unknown
- 1968-06-12 BE BE716464D patent/BE716464A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| FR1570826A (enExample) | 1969-06-13 |
| DE1770510B2 (de) | 1975-06-12 |
| AT278833B (de) | 1970-02-10 |
| DE1770510A1 (de) | 1971-10-28 |
| BE716464A (enExample) | 1968-12-12 |
| CH488727A (de) | 1970-04-15 |
| US3547918A (en) | 1970-12-15 |
| ES354972A1 (es) | 1969-11-16 |
| DE1770510C3 (de) | 1980-11-06 |
| NL6808252A (enExample) | 1968-12-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PE20 | Patent expired after termination of 20 years |