GB1016888A - Method of producing nitrile perchlorate - Google Patents
Method of producing nitrile perchlorateInfo
- Publication number
- GB1016888A GB1016888A GB4667262A GB4667262A GB1016888A GB 1016888 A GB1016888 A GB 1016888A GB 4667262 A GB4667262 A GB 4667262A GB 4667262 A GB4667262 A GB 4667262A GB 1016888 A GB1016888 A GB 1016888A
- Authority
- GB
- United Kingdom
- Prior art keywords
- parts
- perchlorate
- litres
- ozone
- nitrile
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/083—Compounds containing nitrogen and non-metals and optionally metals containing one or more halogen atoms
- C01B21/084—Compounds containing nitrogen and non-metals and optionally metals containing one or more halogen atoms containing also one or more oxygen atoms, e.g. nitrosyl halides
- C01B21/0848—Nitrosyl perchlorate
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Nitrile perchlorate, NO2ClO4, is prepared by reacting NO or NO2 (2 parts by volume), chlorine dioxide (2 parts' and ozone (at least 6 parts and preferably at least 12) as ozonized oxygen. The ClO2 and NO or NO2 may be generated chemically or by electrical discharges, e.g. heavy current glow discharges, and are then immediately introduced, at 0.005-0.1 litres/hr., into the bottom of the reaction vessel. Oxygen containing 4-12% ozone is produced in an ozonizer operating at 6-10 kv., and introduced at 8-20 litres/hr. The reaction is carried out at room temperature, and the product forms as a white film in the vessel.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEJ21021A DE1177623B (en) | 1961-12-14 | 1961-12-14 | Process for the production of nitryl perchlorate |
| BE650572A BE650572A (en) | 1961-12-14 | 1964-07-15 | |
| FR981652A FR1400942A (en) | 1961-12-14 | 1964-07-15 | Process for preparing azotyl perchlorate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1016888A true GB1016888A (en) | 1966-01-12 |
Family
ID=27159000
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB4667262A Expired GB1016888A (en) | 1961-12-14 | 1962-12-11 | Method of producing nitrile perchlorate |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE650572A (en) |
| DE (1) | DE1177623B (en) |
| FR (1) | FR1400942A (en) |
| GB (1) | GB1016888A (en) |
-
1961
- 1961-12-14 DE DEJ21021A patent/DE1177623B/en active Pending
-
1962
- 1962-12-11 GB GB4667262A patent/GB1016888A/en not_active Expired
-
1964
- 1964-07-15 FR FR981652A patent/FR1400942A/en not_active Expired
- 1964-07-15 BE BE650572A patent/BE650572A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE1177623B (en) | 1964-09-10 |
| BE650572A (en) | 1964-11-03 |
| FR1400942A (en) | 1965-05-28 |
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