GB1011240A - Manufacture of 6-halomethyl-2:4-diamino-s-triazines - Google Patents
Manufacture of 6-halomethyl-2:4-diamino-s-triazinesInfo
- Publication number
- GB1011240A GB1011240A GB48927/62A GB4892762A GB1011240A GB 1011240 A GB1011240 A GB 1011240A GB 48927/62 A GB48927/62 A GB 48927/62A GB 4892762 A GB4892762 A GB 4892762A GB 1011240 A GB1011240 A GB 1011240A
- Authority
- GB
- United Kingdom
- Prior art keywords
- diamino
- halomethyl
- triazines
- manufacture
- produced
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 6
- 239000004342 Benzoyl peroxide Substances 0.000 abstract 2
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 abstract 2
- 235000019400 benzoyl peroxide Nutrition 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 230000026030 halogenation Effects 0.000 abstract 2
- 238000005658 halogenation reaction Methods 0.000 abstract 2
- JYEUMXHLPRZUAT-UHFFFAOYSA-N 1,2,3-triazine Chemical compound C1=CN=NN=C1 JYEUMXHLPRZUAT-UHFFFAOYSA-N 0.000 abstract 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- -1 benzoyl peroxide Chemical class 0.000 abstract 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 1
- 229910052794 bromium Inorganic materials 0.000 abstract 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 230000002140 halogenating effect Effects 0.000 abstract 1
- 239000002917 insecticide Substances 0.000 abstract 1
- 150000001451 organic peroxides Chemical class 0.000 abstract 1
- 239000012429 reaction media Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/48—Two nitrogen atoms
- C07D251/50—Two nitrogen atoms with a halogen atom attached to the third ring carbon atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/6515—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having three nitrogen atoms as the only ring hetero atoms
- C07F9/6521—Six-membered rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
6 - Halomethyl - 2 : 4 - diamino - S - triazines, are produced by halogenating, which excludes fluorinating, preferably above 100 DEG C., preferably in the presence of a halogenation catalyst and in particular an organic peroxide, e.g. benzoyl peroxide, 6-methyl-2 : 4-diamino triazine in a acid medium, preferably one in which the parent triazine is soluble, e.g. a carboxylic acid, and in particular acetic acid. The products may be converted to insecticides as in Specification 899,701 (see Group IV (b)). In the example, 6-bromomethyl compound is produced using acetic acid as reaction medium, benzoyl peroxide as catalyst and bromine as halogenation agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB48927/62A GB1011240A (en) | 1962-12-28 | 1962-12-28 | Manufacture of 6-halomethyl-2:4-diamino-s-triazines |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB48927/62A GB1011240A (en) | 1962-12-28 | 1962-12-28 | Manufacture of 6-halomethyl-2:4-diamino-s-triazines |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1011240A true GB1011240A (en) | 1965-11-24 |
Family
ID=10450466
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB48927/62A Expired GB1011240A (en) | 1962-12-28 | 1962-12-28 | Manufacture of 6-halomethyl-2:4-diamino-s-triazines |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB1011240A (en) |
-
1962
- 1962-12-28 GB GB48927/62A patent/GB1011240A/en not_active Expired
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