FR3061350B1 - Procede de fabrication d'une structure d'un supercondensateur et structure issue dudit procede - Google Patents

Procede de fabrication d'une structure d'un supercondensateur et structure issue dudit procede Download PDF

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Publication number
FR3061350B1
FR3061350B1 FR1663259A FR1663259A FR3061350B1 FR 3061350 B1 FR3061350 B1 FR 3061350B1 FR 1663259 A FR1663259 A FR 1663259A FR 1663259 A FR1663259 A FR 1663259A FR 3061350 B1 FR3061350 B1 FR 3061350B1
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France
Prior art keywords
nitrogen
doped
manufacturing
graphene
oxidized
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Active
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FR1663259A
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English (en)
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FR3061350A1 (fr
Inventor
Philippe Stevens
Gwenaelle Toussaint
Aurelien-Louis Habrioux
Clement-Aime Comminges
Ismael Abidat
Teko-Wilhelmin Napporn
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Electricite de France SA
Centre National de la Recherche Scientifique CNRS
Universite de Poitiers
Original Assignee
Electricite de France SA
Centre National de la Recherche Scientifique CNRS
Universite de Poitiers
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Application filed by Electricite de France SA, Centre National de la Recherche Scientifique CNRS, Universite de Poitiers filed Critical Electricite de France SA
Priority to FR1663259A priority Critical patent/FR3061350B1/fr
Priority to PCT/EP2017/083958 priority patent/WO2018115208A1/fr
Publication of FR3061350A1 publication Critical patent/FR3061350A1/fr
Application granted granted Critical
Publication of FR3061350B1 publication Critical patent/FR3061350B1/fr
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Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01GCAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
    • H01G11/00Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/22Electrodes
    • H01G11/26Electrodes characterised by their structure, e.g. multi-layered, porosity or surface features
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • C01B32/182Graphene
    • C01B32/184Preparation
    • C01B32/19Preparation by exfoliation
    • C01B32/192Preparation by exfoliation starting from graphitic oxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • C01B32/182Graphene
    • C01B32/194After-treatment
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • C01B32/182Graphene
    • C01B32/198Graphene oxide
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01GCAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
    • H01G11/00Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/22Electrodes
    • H01G11/30Electrodes characterised by their material
    • H01G11/32Carbon-based
    • H01G11/36Nanostructures, e.g. nanofibres, nanotubes or fullerenes
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01GCAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
    • H01G11/00Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/84Processes for the manufacture of hybrid or EDL capacitors, or components thereof
    • H01G11/86Processes for the manufacture of hybrid or EDL capacitors, or components thereof specially adapted for electrodes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/13Energy storage using capacitors

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Power Engineering (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Electric Double-Layer Capacitors Or The Like (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

L'invention se rapporte à un procédé de fabrication d'une structure (30) destinée à former une interface (44) entre une électrode (41, 42) et un électrolyte (43) d'un supercondensateur (40), comprenant au moins un feuillet de graphène oxydé dopé à l'azote et des groupements (31) à base de phosphore et d'oxygène. D'abord, une suspension aqueuse (1) d'un oxyde de graphène est préparée dans de l'eau, à laquelle un composé à base d'azote (2) est ajouté. La suspension aqueuse est chauffée, puis filtrée afin d'obtenir un composé solide (20) comprenant du graphène oxydé dopé à l'azote. Une suspension acide (3) comprenant le composé solide et un acide phosphorique (4) est ensuite préparée, puis chauffée et filtrée afin d'obtenir une structure comprenant au moins un feuillet de graphène oxydé dopé à l'azote et comprenant des groupements à base de phosphore et d'oxygène.
FR1663259A 2016-12-22 2016-12-22 Procede de fabrication d'une structure d'un supercondensateur et structure issue dudit procede Active FR3061350B1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
FR1663259A FR3061350B1 (fr) 2016-12-22 2016-12-22 Procede de fabrication d'une structure d'un supercondensateur et structure issue dudit procede
PCT/EP2017/083958 WO2018115208A1 (fr) 2016-12-22 2017-12-20 Procédé de dopage de graphène oxydé par l'azote et le phosphore pour l'obtention d'un matériau d'électrode de supercondensateur

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1663259 2016-12-22
FR1663259A FR3061350B1 (fr) 2016-12-22 2016-12-22 Procede de fabrication d'une structure d'un supercondensateur et structure issue dudit procede

Publications (2)

Publication Number Publication Date
FR3061350A1 FR3061350A1 (fr) 2018-06-29
FR3061350B1 true FR3061350B1 (fr) 2019-05-31

Family

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FR1663259A Active FR3061350B1 (fr) 2016-12-22 2016-12-22 Procede de fabrication d'une structure d'un supercondensateur et structure issue dudit procede

Country Status (2)

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FR (1) FR3061350B1 (fr)
WO (1) WO2018115208A1 (fr)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109612177B (zh) * 2018-12-25 2020-02-21 吉林大学 一种二维限域冰及其制备方法
CN111362251B (zh) * 2020-03-20 2021-08-03 山东大学 一种高磷-氮共掺杂三维多孔碳块及其制备方法和应用
CN111733472B (zh) * 2020-06-01 2023-04-04 中科悦达(上海)材料科技有限公司 石墨烯与黑色素组成的复合材料及其制备方法和用途
CN112079351A (zh) * 2020-09-01 2020-12-15 深圳市超导新材料有限公司 一种含氮少层石墨烯的制备方法
CN113213468B (zh) * 2021-05-31 2022-12-23 杭州高烯科技有限公司 一步法制备均匀尺寸氧化石墨烯的设备
CN113582165A (zh) * 2021-07-21 2021-11-02 上海纳米技术及应用国家工程研究中心有限公司 一种磷原子掺杂石墨烯的纳米复合材料的制备方法
WO2023202734A1 (fr) * 2022-04-21 2023-10-26 Univerzita Palackeho V Olomouci Acide graphénique dopé à l'azote, son procédé de préparation et son utilisation
CN115410838B (zh) * 2022-09-09 2023-11-24 三峡大学 磷、碳共修饰钴基氧化物的制备方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103723716B (zh) * 2013-12-23 2016-06-08 北京化工大学 氮掺杂碳包覆氧化石墨烯二维多孔复合材料及其制备方法
CN105621393A (zh) * 2014-11-28 2016-06-01 中国科学院大连化学物理研究所 一种官能化石墨烯材料及其制备和应用
KR101760321B1 (ko) * 2014-12-29 2017-07-21 성균관대학교산학협력단 이온성 액체를 이용한 도핑된 환원된 그래핀 옥사이드의 제조방법 및 이에 의해 제조되는 도핑된 환원된 그래핀 옥사이드
CN104817063B (zh) * 2015-05-07 2016-08-17 常州大学 一种二维氮磷掺杂石墨烯的制备方法

Also Published As

Publication number Publication date
WO2018115208A1 (fr) 2018-06-28
FR3061350A1 (fr) 2018-06-29

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