FR3007753A1 - Procede de preparation de particules de bicarbonate de metal alcalin - Google Patents

Procede de preparation de particules de bicarbonate de metal alcalin Download PDF

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Publication number
FR3007753A1
FR3007753A1 FR1356160A FR1356160A FR3007753A1 FR 3007753 A1 FR3007753 A1 FR 3007753A1 FR 1356160 A FR1356160 A FR 1356160A FR 1356160 A FR1356160 A FR 1356160A FR 3007753 A1 FR3007753 A1 FR 3007753A1
Authority
FR
France
Prior art keywords
alkali metal
sodium
solution
additive
metal bicarbonate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
FR1356160A
Other languages
English (en)
French (fr)
Inventor
David Jean Lucien Savary
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Solvay SA
Original Assignee
Solvay SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Solvay SA filed Critical Solvay SA
Priority to FR1356160A priority Critical patent/FR3007753A1/fr
Priority to MX2015017859A priority patent/MX2015017859A/es
Priority to CA2916157A priority patent/CA2916157A1/en
Priority to US14/900,514 priority patent/US10308517B2/en
Priority to BR112015032278A priority patent/BR112015032278A2/pt
Priority to RU2016102166A priority patent/RU2016102166A/ru
Priority to EP14735513.5A priority patent/EP3013749B1/fr
Priority to CN201480047401.0A priority patent/CN105492391B/zh
Priority to PCT/EP2014/063555 priority patent/WO2014207120A2/fr
Priority to CN201480047406.3A priority patent/CN105492392B/zh
Priority to CN201480047400.6A priority patent/CN105492390B/zh
Priority to EP14735515.0A priority patent/EP3013750A2/fr
Priority to PL14735513T priority patent/PL3013749T3/pl
Priority to AU2014301127A priority patent/AU2014301127B2/en
Priority to JP2016522504A priority patent/JP6630270B2/ja
Priority to PCT/EP2014/063559 priority patent/WO2014207124A2/fr
Priority to US14/900,524 priority patent/US9815708B2/en
Priority to PL14758095T priority patent/PL3013751T3/pl
Priority to CN201810548049.9A priority patent/CN109553117A/zh
Priority to EP14758095.5A priority patent/EP3013751B1/fr
Priority to PCT/EP2014/063558 priority patent/WO2014207123A2/fr
Priority to US14/900,533 priority patent/US9873615B2/en
Publication of FR3007753A1 publication Critical patent/FR3007753A1/fr
Priority to US16/423,709 priority patent/US20190276326A1/en
Priority to JP2019126800A priority patent/JP2019206474A/ja
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00—Carbonates of sodium, potassium or alkali metals in general
    • C01D7/38—Preparation in the form of granules, pieces or other shaped products
    • C01D7/40—Influencing the crystallisation process
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00—Carbonates of sodium, potassium or alkali metals in general
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00—Carbonates of sodium, potassium or alkali metals in general
    • C01D7/10—Preparation of bicarbonates from carbonates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00—Carbonates of sodium, potassium or alkali metals in general
    • C01D7/22—Purification
    • C01D7/24—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/02—Particle morphology depicted by an image obtained by optical microscopy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/10—Solid density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Medicinal Preparation (AREA)
  • Detergent Compositions (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Cosmetics (AREA)
FR1356160A 2013-06-26 2013-06-26 Procede de preparation de particules de bicarbonate de metal alcalin Pending FR3007753A1 (fr)

Priority Applications (24)

Application Number Priority Date Filing Date Title
FR1356160A FR3007753A1 (fr) 2013-06-26 2013-06-26 Procede de preparation de particules de bicarbonate de metal alcalin
EP14735515.0A EP3013750A2 (fr) 2013-06-26 2014-06-26 Procede de preparation de particules de bicarbonate de metal alcalin
AU2014301127A AU2014301127B2 (en) 2013-06-26 2014-06-26 Method for preparing alkali metal bicarbonate particles
US14/900,514 US10308517B2 (en) 2013-06-26 2014-06-26 Method for preparing alkali metal bicarbonate particles
BR112015032278A BR112015032278A2 (pt) 2013-06-26 2014-06-26 método para preparar partículas de bicarbonato de metal alcalino, e, partículas de bicarbonato de metal alcalino
RU2016102166A RU2016102166A (ru) 2013-06-26 2014-06-26 Способ получения частиц бикарбоната щелочного металла
EP14735513.5A EP3013749B1 (fr) 2013-06-26 2014-06-26 Procédé de préparation de particules de bicarbonate de métal alcalin
CN201480047401.0A CN105492391B (zh) 2013-06-26 2014-06-26 用于制备碱金属碳酸氢盐颗粒的方法
PCT/EP2014/063555 WO2014207120A2 (fr) 2013-06-26 2014-06-26 Procédé de préparation de particules de bicarbonate de métal alcalin
CN201480047406.3A CN105492392B (zh) 2013-06-26 2014-06-26 用于制备碱金属碳酸氢盐颗粒的方法
CN201480047400.6A CN105492390B (zh) 2013-06-26 2014-06-26 用于制备碱金属碳酸氢盐颗粒的方法
MX2015017859A MX2015017859A (es) 2013-06-26 2014-06-26 Metodo para preparar particulas de bicarbonato de metal alcalino.
PL14735513T PL3013749T3 (pl) 2013-06-26 2014-06-26 Sposób przygotowywania cząstek wodorowęglanu metalu alkalicznego
PCT/EP2014/063559 WO2014207124A2 (fr) 2013-06-26 2014-06-26 Procédé de préparation de particules de bicarbonate de métal alcalin
JP2016522504A JP6630270B2 (ja) 2013-06-26 2014-06-26 アルカリ金属重炭酸塩粒子の製造方法
PCT/EP2014/063558 WO2014207123A2 (fr) 2013-06-26 2014-06-26 Procede de preparation de particules de bicarbonate de metal alcalin
US14/900,524 US9815708B2 (en) 2013-06-26 2014-06-26 Method for preparing particles of alkali metal bicarbonate
PL14758095T PL3013751T3 (pl) 2013-06-26 2014-06-26 Sposób wytwarzania cząstek wodorowęglanu metalu alkalicznego
CN201810548049.9A CN109553117A (zh) 2013-06-26 2014-06-26 用于制备碱金属碳酸氢盐颗粒的方法
EP14758095.5A EP3013751B1 (fr) 2013-06-26 2014-06-26 Procédé de préparation de particules de bicarbonate de métal alcalin
CA2916157A CA2916157A1 (en) 2013-06-26 2014-06-26 Method for preparing alkali metal bicarbonate particles
US14/900,533 US9873615B2 (en) 2013-06-26 2014-06-26 Method for preparing particles of alkali metal bicarbonate
US16/423,709 US20190276326A1 (en) 2013-06-26 2019-05-28 Method for preparing alkali metal bicarbonate particles
JP2019126800A JP2019206474A (ja) 2013-06-26 2019-07-08 アルカリ金属重炭酸塩粒子の製造方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1356160A FR3007753A1 (fr) 2013-06-26 2013-06-26 Procede de preparation de particules de bicarbonate de metal alcalin

Publications (1)

Publication Number Publication Date
FR3007753A1 true FR3007753A1 (fr) 2015-01-02

Family

ID=50023636

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1356160A Pending FR3007753A1 (fr) 2013-06-26 2013-06-26 Procede de preparation de particules de bicarbonate de metal alcalin

Country Status (12)

Country Link
US (4) US9815708B2 (enExample)
EP (3) EP3013750A2 (enExample)
JP (2) JP6630270B2 (enExample)
CN (4) CN105492390B (enExample)
AU (1) AU2014301127B2 (enExample)
BR (1) BR112015032278A2 (enExample)
CA (1) CA2916157A1 (enExample)
FR (1) FR3007753A1 (enExample)
MX (1) MX2015017859A (enExample)
PL (2) PL3013751T3 (enExample)
RU (1) RU2016102166A (enExample)
WO (3) WO2014207120A2 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013092754A1 (en) 2011-12-23 2013-06-27 Solvay Sa Process for the joint production of sodium carbonate and sodium bicarbonate
FR3007753A1 (fr) 2013-06-26 2015-01-02 Solvay Procede de preparation de particules de bicarbonate de metal alcalin
US10766782B2 (en) 2015-09-23 2020-09-08 Solvay Sa Production of crystalline sodium bicarbonate
US10392257B2 (en) 2015-09-23 2019-08-27 Solvay Sa Method for enhancing sodium bicarbonate flowability
KR20190111060A (ko) 2017-01-24 2019-10-01 이 아이 듀폰 디 네모아 앤드 캄파니 다당류를 이용한 침전된 탄산칼슘의 제조 방법
KR102022939B1 (ko) * 2018-01-30 2019-09-19 가톨릭대학교 산학협력단 수산화나트륨이 용해된 알코올-물 혼합 수용액의 탄산화를 통한 중탄산나트륨 제조방법
JP7448926B1 (ja) 2023-05-31 2024-03-13 株式会社徳岡テクノ 二酸化炭素吸着方法、二酸化炭素処理装置、及び、二酸化炭素吸着システム

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2954282A (en) * 1954-12-13 1960-09-27 Fmc Corp Method of crystallizing
US3072466A (en) * 1960-08-12 1963-01-08 Fmc Corp Method of crystallizing sodium bicarbonate
US3725014A (en) * 1971-04-21 1973-04-03 Allied Chem Sodium carbonate crystallization process with foam prevention

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL70417C (enExample) 1950-04-24
US2954262A (en) 1957-06-26 1960-09-27 Bendix Corp Anti-skid device
US3111379A (en) * 1961-04-12 1963-11-19 Fmc Corp Manufacture of potassium bicarbonate
US3347623A (en) * 1966-11-03 1967-10-17 Kali Chemie Ag Preparation of potassium bicarbonate
JPS4817160B1 (enExample) * 1970-01-14 1973-05-26
US3653847A (en) * 1970-09-14 1972-04-04 American Potash & Chem Corp Inhibition of sodium bicarbonate crystallization during crystallization of other materials using polyphosphates
US3855397A (en) 1973-04-12 1974-12-17 Allied Chem Method of producing sodium carbonate and bicarbonate spherules from brine
US3852427A (en) 1973-04-12 1974-12-03 Allied Chem Sodium bicarbonate spherulites from sodium d esquicarbonate
US3981686A (en) * 1974-10-24 1976-09-21 Intermountain Research And Development Corporation Clarifier process for producing sodium carbonate
DE2940614C2 (de) * 1979-10-06 1982-09-16 Chemische Werke Hüls AG, 4370 Marl Verfahren zur Herstellung von Natriumhydrogencarbonat und Chlorwasserstoff
US4478599A (en) * 1982-05-25 1984-10-23 Kerr-Mcgee Chemical Corporation Method of continuously controlling crystal fines formation
FR2646154B1 (fr) * 1989-04-24 1991-06-28 Solvay Bicarbonate de sodium et procede pour la cristallisation de bicarbonate de sodium
JPH0397617A (ja) 1989-06-29 1991-04-23 Tosoh Corp 重炭酸ナトリウムの製造方法
US6042622A (en) * 1996-07-31 2000-03-28 Basf Corporation Process for crystallization of alkali metal bicarbonate salts
US6270740B2 (en) 1997-03-20 2001-08-07 General Chemical Corporation Method of producing modified sodium carbonate crystals for the production of sodium bicarbonate
CA2284967A1 (en) * 1998-10-13 2000-04-13 Aristos Capital Corporation Method of formulating alkali earth salts
JP4817160B2 (ja) 2001-03-07 2011-11-16 日立バルブ株式会社 空気調和システム及び電動操作機
US6667021B2 (en) * 2001-09-12 2003-12-23 General Chemical Corporation Method for producing enhanced sodium carbonate crystals for making sodium bicarbonate
CN100348489C (zh) * 2003-04-24 2007-11-14 狮王株式会社 表面处理水溶性无机化合物颗粒及其制造方法、以及粒状洗涤剂组合物
KR101102273B1 (ko) * 2003-04-24 2012-01-03 라이온 가부시키가이샤 표면처리 수용성 무기 화합물 입자 및 그 제조방법, 및입상 세제 조성물
CN1780671A (zh) 2003-04-29 2006-05-31 阿克佐诺贝尔股份有限公司 涉及使用反溶剂结晶的方法
US20060150892A1 (en) 2003-04-29 2006-07-13 Akzo Nobel N.V. Processes Involving the Use of Antisolvent Crystallisation
EP1997780A1 (en) 2006-03-15 2008-12-03 Asahi Glass Company, Limited High-purity sodium hydrogen carbonate crystal grain and process for producing the same
EP2399866A1 (en) * 2010-06-22 2011-12-28 Solvay SA Process for the joint production of sodium carbonate and sodium bicarbonate
EP2607312A1 (en) * 2011-12-21 2013-06-26 Solvay Sa Process for preparing sodium bicarbonate particles
WO2013092754A1 (en) 2011-12-23 2013-06-27 Solvay Sa Process for the joint production of sodium carbonate and sodium bicarbonate
GB201202797D0 (en) 2012-02-20 2012-04-04 Eminate Ltd Sodium bicarbonate product
CN102940307B (zh) * 2012-11-19 2016-06-08 湖南中烟工业有限责任公司 一种用于口含型烟草制品的缓释碱性微胶囊及其制备方法和应用
FR3007753A1 (fr) 2013-06-26 2015-01-02 Solvay Procede de preparation de particules de bicarbonate de metal alcalin

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2954282A (en) * 1954-12-13 1960-09-27 Fmc Corp Method of crystallizing
US3072466A (en) * 1960-08-12 1963-01-08 Fmc Corp Method of crystallizing sodium bicarbonate
US3725014A (en) * 1971-04-21 1973-04-03 Allied Chem Sodium carbonate crystallization process with foam prevention

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
CHEMICAL ABSTRACTS, CHEMICAL ABSTRACTS SERVICE (C A S), US, 21 October 1991 (1991-10-21), XP000318285, ISSN: 0009-2258 *
MARTINEZ-CRUZ N ET AL: "Effect of molecular weight of polystyrensulfonic acid sodium salt polymers on the precipitation kinetics of sodium bicarbonate", JOURNAL OF CRYSTAL GROWTH, ELSEVIER, AMSTERDAM, NL, vol. 270, no. 3-4, 1 October 2004 (2004-10-01), pages 573 - 581, XP004565858, ISSN: 0022-0248, DOI: 10.1016/J.JCRYSGRO.2004.06.024 *

Also Published As

Publication number Publication date
US20190276326A1 (en) 2019-09-12
WO2014207120A2 (fr) 2014-12-31
JP2016523803A (ja) 2016-08-12
WO2014207124A2 (fr) 2014-12-31
US9873615B2 (en) 2018-01-23
BR112015032278A2 (pt) 2017-07-25
WO2014207123A3 (fr) 2015-03-05
CN105492391A (zh) 2016-04-13
RU2016102166A (ru) 2017-07-31
WO2014207124A3 (fr) 2015-03-12
PL3013751T3 (pl) 2020-07-27
AU2014301127A1 (en) 2016-01-28
WO2014207120A3 (fr) 2015-03-05
CN105492391B (zh) 2018-03-09
JP2019206474A (ja) 2019-12-05
WO2014207123A2 (fr) 2014-12-31
JP6630270B2 (ja) 2020-01-15
CN105492390A (zh) 2016-04-13
CN105492392A (zh) 2016-04-13
US20160145115A1 (en) 2016-05-26
EP3013751B1 (fr) 2020-01-08
US20160130153A1 (en) 2016-05-12
CN109553117A (zh) 2019-04-02
EP3013749A2 (fr) 2016-05-04
CN105492392B (zh) 2018-06-26
PL3013749T3 (pl) 2020-07-13
CA2916157A1 (en) 2014-12-31
EP3013749B1 (fr) 2020-02-12
EP3013751A2 (fr) 2016-05-04
US20160368779A1 (en) 2016-12-22
US9815708B2 (en) 2017-11-14
US10308517B2 (en) 2019-06-04
CN105492390B (zh) 2018-03-09
MX2015017859A (es) 2016-08-03
AU2014301127B2 (en) 2018-04-26
EP3013750A2 (fr) 2016-05-04

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