AU2014301127B2 - Method for preparing alkali metal bicarbonate particles - Google Patents

Method for preparing alkali metal bicarbonate particles Download PDF

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Publication number
AU2014301127B2
AU2014301127B2 AU2014301127A AU2014301127A AU2014301127B2 AU 2014301127 B2 AU2014301127 B2 AU 2014301127B2 AU 2014301127 A AU2014301127 A AU 2014301127A AU 2014301127 A AU2014301127 A AU 2014301127A AU 2014301127 B2 AU2014301127 B2 AU 2014301127B2
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AU
Australia
Prior art keywords
additive
alkali metal
solution
crystallization
bicarbonate particles
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
AU2014301127A
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English (en)
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AU2014301127A1 (en
Inventor
David Jean Lucien SAVARY
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Solvay SA
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Solvay SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Solvay SA filed Critical Solvay SA
Publication of AU2014301127A1 publication Critical patent/AU2014301127A1/en
Application granted granted Critical
Publication of AU2014301127B2 publication Critical patent/AU2014301127B2/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00—Carbonates of sodium, potassium or alkali metals in general
    • C01D7/38—Preparation in the form of granules, pieces or other shaped products
    • C01D7/40—Influencing the crystallisation process
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00—Carbonates of sodium, potassium or alkali metals in general
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00—Carbonates of sodium, potassium or alkali metals in general
    • C01D7/10—Preparation of bicarbonates from carbonates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00—Carbonates of sodium, potassium or alkali metals in general
    • C01D7/22—Purification
    • C01D7/24—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/02—Particle morphology depicted by an image obtained by optical microscopy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/10—Solid density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Medicinal Preparation (AREA)
  • Detergent Compositions (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Cosmetics (AREA)
AU2014301127A 2013-06-26 2014-06-26 Method for preparing alkali metal bicarbonate particles Expired - Fee Related AU2014301127B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1356160A FR3007753A1 (fr) 2013-06-26 2013-06-26 Procede de preparation de particules de bicarbonate de metal alcalin
FR1356160 2013-06-26
PCT/EP2014/063555 WO2014207120A2 (fr) 2013-06-26 2014-06-26 Procédé de préparation de particules de bicarbonate de métal alcalin

Publications (2)

Publication Number Publication Date
AU2014301127A1 AU2014301127A1 (en) 2016-01-28
AU2014301127B2 true AU2014301127B2 (en) 2018-04-26

Family

ID=50023636

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2014301127A Expired - Fee Related AU2014301127B2 (en) 2013-06-26 2014-06-26 Method for preparing alkali metal bicarbonate particles

Country Status (12)

Country Link
US (4) US9815708B2 (enExample)
EP (3) EP3013750A2 (enExample)
JP (2) JP6630270B2 (enExample)
CN (4) CN105492390B (enExample)
AU (1) AU2014301127B2 (enExample)
BR (1) BR112015032278A2 (enExample)
CA (1) CA2916157A1 (enExample)
FR (1) FR3007753A1 (enExample)
MX (1) MX2015017859A (enExample)
PL (2) PL3013751T3 (enExample)
RU (1) RU2016102166A (enExample)
WO (3) WO2014207120A2 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013092754A1 (en) 2011-12-23 2013-06-27 Solvay Sa Process for the joint production of sodium carbonate and sodium bicarbonate
FR3007753A1 (fr) 2013-06-26 2015-01-02 Solvay Procede de preparation de particules de bicarbonate de metal alcalin
US10766782B2 (en) 2015-09-23 2020-09-08 Solvay Sa Production of crystalline sodium bicarbonate
US10392257B2 (en) 2015-09-23 2019-08-27 Solvay Sa Method for enhancing sodium bicarbonate flowability
KR20190111060A (ko) 2017-01-24 2019-10-01 이 아이 듀폰 디 네모아 앤드 캄파니 다당류를 이용한 침전된 탄산칼슘의 제조 방법
KR102022939B1 (ko) * 2018-01-30 2019-09-19 가톨릭대학교 산학협력단 수산화나트륨이 용해된 알코올-물 혼합 수용액의 탄산화를 통한 중탄산나트륨 제조방법
JP7448926B1 (ja) 2023-05-31 2024-03-13 株式会社徳岡テクノ 二酸化炭素吸着方法、二酸化炭素処理装置、及び、二酸化炭素吸着システム

Citations (4)

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US2642342A (en) * 1950-04-24 1953-06-16 Werkspoor Nv Method of crystallizing sodium carbonate
US3072466A (en) * 1960-08-12 1963-01-08 Fmc Corp Method of crystallizing sodium bicarbonate
US3725014A (en) * 1971-04-21 1973-04-03 Allied Chem Sodium carbonate crystallization process with foam prevention
US3981686A (en) * 1974-10-24 1976-09-21 Intermountain Research And Development Corporation Clarifier process for producing sodium carbonate

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US2954282A (en) * 1954-12-13 1960-09-27 Fmc Corp Method of crystallizing
US2954262A (en) 1957-06-26 1960-09-27 Bendix Corp Anti-skid device
US3111379A (en) * 1961-04-12 1963-11-19 Fmc Corp Manufacture of potassium bicarbonate
US3347623A (en) * 1966-11-03 1967-10-17 Kali Chemie Ag Preparation of potassium bicarbonate
JPS4817160B1 (enExample) * 1970-01-14 1973-05-26
US3653847A (en) * 1970-09-14 1972-04-04 American Potash & Chem Corp Inhibition of sodium bicarbonate crystallization during crystallization of other materials using polyphosphates
US3855397A (en) 1973-04-12 1974-12-17 Allied Chem Method of producing sodium carbonate and bicarbonate spherules from brine
US3852427A (en) 1973-04-12 1974-12-03 Allied Chem Sodium bicarbonate spherulites from sodium d esquicarbonate
DE2940614C2 (de) * 1979-10-06 1982-09-16 Chemische Werke Hüls AG, 4370 Marl Verfahren zur Herstellung von Natriumhydrogencarbonat und Chlorwasserstoff
US4478599A (en) * 1982-05-25 1984-10-23 Kerr-Mcgee Chemical Corporation Method of continuously controlling crystal fines formation
FR2646154B1 (fr) * 1989-04-24 1991-06-28 Solvay Bicarbonate de sodium et procede pour la cristallisation de bicarbonate de sodium
JPH0397617A (ja) 1989-06-29 1991-04-23 Tosoh Corp 重炭酸ナトリウムの製造方法
US6042622A (en) * 1996-07-31 2000-03-28 Basf Corporation Process for crystallization of alkali metal bicarbonate salts
US6270740B2 (en) 1997-03-20 2001-08-07 General Chemical Corporation Method of producing modified sodium carbonate crystals for the production of sodium bicarbonate
CA2284967A1 (en) * 1998-10-13 2000-04-13 Aristos Capital Corporation Method of formulating alkali earth salts
JP4817160B2 (ja) 2001-03-07 2011-11-16 日立バルブ株式会社 空気調和システム及び電動操作機
US6667021B2 (en) * 2001-09-12 2003-12-23 General Chemical Corporation Method for producing enhanced sodium carbonate crystals for making sodium bicarbonate
CN100348489C (zh) * 2003-04-24 2007-11-14 狮王株式会社 表面处理水溶性无机化合物颗粒及其制造方法、以及粒状洗涤剂组合物
KR101102273B1 (ko) * 2003-04-24 2012-01-03 라이온 가부시키가이샤 표면처리 수용성 무기 화합물 입자 및 그 제조방법, 및입상 세제 조성물
CN1780671A (zh) 2003-04-29 2006-05-31 阿克佐诺贝尔股份有限公司 涉及使用反溶剂结晶的方法
US20060150892A1 (en) 2003-04-29 2006-07-13 Akzo Nobel N.V. Processes Involving the Use of Antisolvent Crystallisation
EP1997780A1 (en) 2006-03-15 2008-12-03 Asahi Glass Company, Limited High-purity sodium hydrogen carbonate crystal grain and process for producing the same
EP2399866A1 (en) * 2010-06-22 2011-12-28 Solvay SA Process for the joint production of sodium carbonate and sodium bicarbonate
EP2607312A1 (en) * 2011-12-21 2013-06-26 Solvay Sa Process for preparing sodium bicarbonate particles
WO2013092754A1 (en) 2011-12-23 2013-06-27 Solvay Sa Process for the joint production of sodium carbonate and sodium bicarbonate
GB201202797D0 (en) 2012-02-20 2012-04-04 Eminate Ltd Sodium bicarbonate product
CN102940307B (zh) * 2012-11-19 2016-06-08 湖南中烟工业有限责任公司 一种用于口含型烟草制品的缓释碱性微胶囊及其制备方法和应用
FR3007753A1 (fr) 2013-06-26 2015-01-02 Solvay Procede de preparation de particules de bicarbonate de metal alcalin

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2642342A (en) * 1950-04-24 1953-06-16 Werkspoor Nv Method of crystallizing sodium carbonate
US3072466A (en) * 1960-08-12 1963-01-08 Fmc Corp Method of crystallizing sodium bicarbonate
US3725014A (en) * 1971-04-21 1973-04-03 Allied Chem Sodium carbonate crystallization process with foam prevention
US3981686A (en) * 1974-10-24 1976-09-21 Intermountain Research And Development Corporation Clarifier process for producing sodium carbonate

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
MARTINEZ-CRUZ N ET AL, JOURNAL OF CRYSTAL GROWTH, (20041001), vol. 270, no. 3-4, pages 573 - 581 *

Also Published As

Publication number Publication date
US20190276326A1 (en) 2019-09-12
WO2014207120A2 (fr) 2014-12-31
JP2016523803A (ja) 2016-08-12
WO2014207124A2 (fr) 2014-12-31
US9873615B2 (en) 2018-01-23
BR112015032278A2 (pt) 2017-07-25
WO2014207123A3 (fr) 2015-03-05
CN105492391A (zh) 2016-04-13
RU2016102166A (ru) 2017-07-31
WO2014207124A3 (fr) 2015-03-12
PL3013751T3 (pl) 2020-07-27
AU2014301127A1 (en) 2016-01-28
WO2014207120A3 (fr) 2015-03-05
CN105492391B (zh) 2018-03-09
JP2019206474A (ja) 2019-12-05
WO2014207123A2 (fr) 2014-12-31
JP6630270B2 (ja) 2020-01-15
CN105492390A (zh) 2016-04-13
CN105492392A (zh) 2016-04-13
US20160145115A1 (en) 2016-05-26
FR3007753A1 (fr) 2015-01-02
EP3013751B1 (fr) 2020-01-08
US20160130153A1 (en) 2016-05-12
CN109553117A (zh) 2019-04-02
EP3013749A2 (fr) 2016-05-04
CN105492392B (zh) 2018-06-26
PL3013749T3 (pl) 2020-07-13
CA2916157A1 (en) 2014-12-31
EP3013749B1 (fr) 2020-02-12
EP3013751A2 (fr) 2016-05-04
US20160368779A1 (en) 2016-12-22
US9815708B2 (en) 2017-11-14
US10308517B2 (en) 2019-06-04
CN105492390B (zh) 2018-03-09
MX2015017859A (es) 2016-08-03
EP3013750A2 (fr) 2016-05-04

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MK25 Application lapsed reg. 22.2i(2) - failure to pay acceptance fee