FR2877146B1 - Materiau nanostructure, procede pour sa preparation. - Google Patents

Materiau nanostructure, procede pour sa preparation.

Info

Publication number
FR2877146B1
FR2877146B1 FR0411243A FR0411243A FR2877146B1 FR 2877146 B1 FR2877146 B1 FR 2877146B1 FR 0411243 A FR0411243 A FR 0411243A FR 0411243 A FR0411243 A FR 0411243A FR 2877146 B1 FR2877146 B1 FR 2877146B1
Authority
FR
France
Prior art keywords
carbon
precursor
stage
ratio
gel
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR0411243A
Other languages
English (en)
French (fr)
Other versions
FR2877146A1 (fr
Inventor
Joel Gaubicher
Dominique Guyomard
Matthieu Dubarry
Philippe Moreau
Marc Deschamps
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Centre National de la Recherche Scientifique CNRS
Blue Solutions SA
Original Assignee
Centre National de la Recherche Scientifique CNRS
Batscap SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR0411243A priority Critical patent/FR2877146B1/fr
Application filed by Centre National de la Recherche Scientifique CNRS, Batscap SA filed Critical Centre National de la Recherche Scientifique CNRS
Priority to CNB2005800362694A priority patent/CN100550481C/zh
Priority to DE602005006437T priority patent/DE602005006437T2/de
Priority to US11/665,921 priority patent/US7744835B2/en
Priority to KR1020077011606A priority patent/KR101276570B1/ko
Priority to JP2007537327A priority patent/JP4979585B2/ja
Priority to AT05809230T priority patent/ATE393966T1/de
Priority to ES05809230T priority patent/ES2304732T3/es
Priority to PCT/FR2005/002581 priority patent/WO2006045923A2/fr
Priority to CA2584231A priority patent/CA2584231C/fr
Priority to EP05809230A priority patent/EP1831945B1/fr
Publication of FR2877146A1 publication Critical patent/FR2877146A1/fr
Application granted granted Critical
Publication of FR2877146B1 publication Critical patent/FR2877146B1/fr
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/62Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/621Binders
    • H01M4/622Binders being polymers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82BNANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/20Vanadium, niobium or tantalum
    • B01J23/22Vanadium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82BNANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B1/00Nanostructures formed by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/13Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/133Electrodes based on carbonaceous material, e.g. graphite-intercalation compounds or CFx
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/62Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/624Electric conductive fillers
    • H01M4/625Carbon or graphite
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00Manufacture or treatment of nanostructures
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • H01M10/0525Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/056Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0561Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of inorganic materials only
    • H01M10/0562Solid materials
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/056Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0564Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
    • H01M10/0565Polymeric materials, e.g. gel-type or solid-type
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M2004/026Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028Positive electrodes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00Nanotechnology
    • Y10S977/70Nanostructure
    • Y10S977/773Nanoparticle, i.e. structure having three dimensions of 100 nm or less
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00Nanotechnology
    • Y10S977/70Nanostructure
    • Y10S977/811Of specified metal oxide composition, e.g. conducting or semiconducting compositions such as ITO, ZnOx
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913Rod, strand, filament or fiber
    • Y10T428/2918Rod, strand, filament or fiber including free carbon or carbide or therewith [not as steel]
    • Y10T428/292In coating or impregnation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982Particulate matter [e.g., sphere, flake, etc.]
    • Y10T428/2991Coated
    • Y10T428/2993Silicic or refractory material containing [e.g., tungsten oxide, glass, cement, etc.]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Nanotechnology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Secondary Cells (AREA)
  • Inorganic Fibers (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
FR0411243A 2004-10-22 2004-10-22 Materiau nanostructure, procede pour sa preparation. Expired - Fee Related FR2877146B1 (fr)

Priority Applications (11)

Application Number Priority Date Filing Date Title
FR0411243A FR2877146B1 (fr) 2004-10-22 2004-10-22 Materiau nanostructure, procede pour sa preparation.
PCT/FR2005/002581 WO2006045923A2 (fr) 2004-10-22 2005-10-18 Materiau nanostructure, procede pour sa preparation
US11/665,921 US7744835B2 (en) 2004-10-22 2005-10-18 Nanostructure material, method for the preparation thereof
KR1020077011606A KR101276570B1 (ko) 2004-10-22 2005-10-18 나노구조 물질 및 그 제조 방법
JP2007537327A JP4979585B2 (ja) 2004-10-22 2005-10-18 ナノ構造材料およびその製造方法
AT05809230T ATE393966T1 (de) 2004-10-22 2005-10-18 Nanostrukturmaterial und verfahren zu seiner herstellung
CNB2005800362694A CN100550481C (zh) 2004-10-22 2005-10-18 纳米结构材料及其制备方法
DE602005006437T DE602005006437T2 (de) 2004-10-22 2005-10-18 Nanostrukturmaterial und verfahren zu seiner herstellung
CA2584231A CA2584231C (fr) 2004-10-22 2005-10-18 Preparation avec gel et profilage thermique d'un materiau carbone nanostructure a conduction electronique
EP05809230A EP1831945B1 (fr) 2004-10-22 2005-10-18 Materiau nanostructure, procede pour sa preparation
ES05809230T ES2304732T3 (es) 2004-10-22 2005-10-18 Material nanoestructurado, metodo para su preparacion.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR0411243A FR2877146B1 (fr) 2004-10-22 2004-10-22 Materiau nanostructure, procede pour sa preparation.

Publications (2)

Publication Number Publication Date
FR2877146A1 FR2877146A1 (fr) 2006-04-28
FR2877146B1 true FR2877146B1 (fr) 2007-01-19

Family

ID=34950918

Family Applications (1)

Application Number Title Priority Date Filing Date
FR0411243A Expired - Fee Related FR2877146B1 (fr) 2004-10-22 2004-10-22 Materiau nanostructure, procede pour sa preparation.

Country Status (11)

Country Link
US (1) US7744835B2 (enExample)
EP (1) EP1831945B1 (enExample)
JP (1) JP4979585B2 (enExample)
KR (1) KR101276570B1 (enExample)
CN (1) CN100550481C (enExample)
AT (1) ATE393966T1 (enExample)
CA (1) CA2584231C (enExample)
DE (1) DE602005006437T2 (enExample)
ES (1) ES2304732T3 (enExample)
FR (1) FR2877146B1 (enExample)
WO (1) WO2006045923A2 (enExample)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2876997B1 (fr) 2004-10-22 2007-01-19 Batscap Sa Oxyde de lithium et de vanadium, procede pour sa preparation
JP5409601B2 (ja) * 2007-04-16 2014-02-05 ビーエーエスエフ ソシエタス・ヨーロピア リチウム含有率の高い金属酸化物の製造方法
JP4561839B2 (ja) * 2008-01-23 2010-10-13 ソニー株式会社 非水電解質電池および非水電解質電池用電極ならびにそれらの製造方法
US8784764B2 (en) * 2008-12-15 2014-07-22 Corning Incorporated Methods for forming activated carbon material for high energy density ultracapacitors
US9337509B2 (en) 2011-06-02 2016-05-10 Toyota Jidosha Kabushiki Kaisha Solid electrolyte material, solid state battery, and method for producing solid electrolyte material
WO2013173927A1 (en) * 2012-05-25 2013-11-28 Bathium Canada Inc. Electrode material for lithium electrochemical cells
WO2014004875A2 (en) * 2012-06-29 2014-01-03 University Of New Hampshire Treatment of anodized aluminum components
US9997778B2 (en) * 2012-11-05 2018-06-12 University Of Washington Through Its Center For Commercialization Polycrystalline vanadium oxide nanosheets
CN103165875B (zh) * 2013-03-13 2015-05-27 武汉理工大学 锂离子预嵌入型五氧化二钒纳米带及其制备方法和应用
CN103811740B (zh) * 2014-02-18 2015-09-23 中南大学 一种核壳结构LixV2O5/LiV3O8嵌锂材料及其制备方法
CN112520787A (zh) * 2020-12-11 2021-03-19 广东石油化工学院 一种β相偏钒酸钠的溶液制备方法及其在锂离子电池的应用
KR102837986B1 (ko) * 2023-03-20 2025-07-24 광주과학기술원 리튬이차전지용 양극재 및 이의 제조방법

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0679487B2 (ja) * 1988-05-25 1994-10-05 株式会社ユアサコーポレーション 非水電解質二次電池
JPH03225774A (ja) * 1990-01-30 1991-10-04 Bridgestone Corp 非水電解質二次電池
US5326545A (en) * 1993-03-30 1994-07-05 Valence Technology, Inc. Method of making lithium battery electrode compositions
US5334334A (en) * 1993-03-30 1994-08-02 Valence Technology, Inc. Method of preparing lithium battery electrode compositions
US5512214A (en) * 1993-03-30 1996-04-30 Koksbang; Rene Lithium battery electrode compositions
JP4686871B2 (ja) 2001-02-28 2011-05-25 株式会社豊田中央研究所 リチウム二次電池
FR2831715B1 (fr) * 2001-10-25 2004-03-19 Centre Nat Rech Scient Oxyde de lithium et de vanadium, son utilisation comme matiere active d'electrode
FR2876998B1 (fr) 2004-10-22 2007-01-19 Batscap Sa Procede de preparation de gamma-liv205

Also Published As

Publication number Publication date
ES2304732T3 (es) 2008-10-16
JP2008516886A (ja) 2008-05-22
WO2006045923A2 (fr) 2006-05-04
EP1831945A2 (fr) 2007-09-12
CA2584231C (fr) 2013-08-27
EP1831945B1 (fr) 2008-04-30
CN101065866A (zh) 2007-10-31
DE602005006437D1 (de) 2008-06-12
FR2877146A1 (fr) 2006-04-28
KR101276570B1 (ko) 2013-06-18
US20090263724A1 (en) 2009-10-22
DE602005006437T2 (de) 2009-06-18
WO2006045923A3 (fr) 2006-11-30
ATE393966T1 (de) 2008-05-15
US7744835B2 (en) 2010-06-29
CA2584231A1 (fr) 2006-05-04
KR20070108357A (ko) 2007-11-09
JP4979585B2 (ja) 2012-07-18
CN100550481C (zh) 2009-10-14

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