FR2388029A1 - Preparations tinctoriales aqueuses - Google Patents

Preparations tinctoriales aqueuses

Info

Publication number
FR2388029A1
FR2388029A1 FR7811422A FR7811422A FR2388029A1 FR 2388029 A1 FR2388029 A1 FR 2388029A1 FR 7811422 A FR7811422 A FR 7811422A FR 7811422 A FR7811422 A FR 7811422A FR 2388029 A1 FR2388029 A1 FR 2388029A1
Authority
FR
France
Prior art keywords
aqueous
preparations
aqueous dye
tinctorial
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7811422A
Other languages
English (en)
Other versions
FR2388029B1 (fr
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Novartis AG
Original Assignee
Ciba Geigy AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ciba Geigy AG filed Critical Ciba Geigy AG
Publication of FR2388029A1 publication Critical patent/FR2388029A1/fr
Application granted granted Critical
Publication of FR2388029B1 publication Critical patent/FR2388029B1/fr
Granted legal-status Critical Current

Links

Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642—Compounds containing nitrogen
    • D06P1/645—Aliphatic, araliphatic or cycloaliphatic compounds containing amino groups
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
    • C09B67/0084—Dispersions of dyes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
    • D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • D06P1/525—Polymers of unsaturated carboxylic acids or functional derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642—Compounds containing nitrogen
    • D06P1/647—Nitrogen-containing carboxylic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/653—Nitrogen-free carboxylic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/667—Organo-phosphorus compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/34—Material containing ester groups
    • D06P3/52—Polyesters
    • D06P3/54—Polyesters using dispersed dyestuffs
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/58—Material containing hydroxyl groups
    • D06P3/60—Natural or regenerated cellulose
    • D06P3/6033—Natural or regenerated cellulose using dispersed dyes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/82—Textiles which contain different kinds of fibres
    • D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
    • D06P3/8223—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups
    • D06P3/8228—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using one kind of dye
    • D06P3/8233—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using one kind of dye using dispersed dyes

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Abstract

Préparation tinctoriale aqueuse contenant au moins un colorant insoluble dans l'eau, un agent de dispersion et au moins un autre additif. Les nouvelles préparations tinctoriales aqueuses contiennent au moins un produit de polymérisation soluble dans l'eau contenant des groupes carboxyliques. Application des préparations tinctoriales aqueuses à la teinture de matières textiles.
FR7811422A 1977-04-19 1978-04-18 Preparations tinctoriales aqueuses Granted FR2388029A1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH480877A CH627490A5 (de) 1977-04-19 1977-04-19 Waessrige farbstoffpraeparate.

Publications (2)

Publication Number Publication Date
FR2388029A1 true FR2388029A1 (fr) 1978-11-17
FR2388029B1 FR2388029B1 (fr) 1981-11-20

Family

ID=4282899

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7811422A Granted FR2388029A1 (fr) 1977-04-19 1978-04-18 Preparations tinctoriales aqueuses

Country Status (9)

Country Link
US (1) US4297100A (fr)
JP (1) JPS53130727A (fr)
BR (1) BR7802408A (fr)
CH (1) CH627490A5 (fr)
CS (1) CS196427B2 (fr)
DE (1) DE2816539C2 (fr)
FR (1) FR2388029A1 (fr)
GB (1) GB1603215A (fr)
IN (1) IN148690B (fr)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0014503A1 (fr) * 1979-02-02 1980-08-20 Rohner AG Pratteln Procédé de préparation de compositions solides dispersables en milieu aqueux de substances actives étant peu solubles à insolubles dans l'eau, fortement concentrées, finement dispersées, contenant peu ou pas d'agent dispersant
FR2497245A1 (fr) * 1980-12-30 1982-07-02 Protex Manuf Prod Chimiq Procede de teinture sur fibres cellulosiques et/ou synthetiques
EP0056991A2 (fr) * 1981-01-26 1982-08-04 Ciba-Geigy Ag Préparations tinctoriales liquides
EP0097291A1 (fr) * 1982-06-23 1984-01-04 Bayer Ag Préparations de colorants
EP0124866A1 (fr) * 1983-05-04 1984-11-14 Ciba-Geigy Ag Granules de colorant dispersables dans l'eau froide
EP0225287A1 (fr) * 1985-11-25 1987-06-10 Ciba-Geigy Ag Préparations stables au stockage de corps solides peu solubles ou insolubles dans l'eau
EP0738766A1 (fr) * 1995-04-20 1996-10-23 Clariant Finance (BVI) Limited Suspensions liquides stables de colorants au soufre et méthode pour les analyser
EP0824155A1 (fr) * 1996-08-15 1998-02-18 Clariant Finance (BVI) Limited Solutions aqueuses concentrées de sels de sodium d'acides polycarboxyliques, leur préparation et leur utilisation

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3151451A1 (de) * 1981-12-24 1983-07-07 Hoechst Ag, 6230 Frankfurt "hilfsmittel und verfahren zum klotzfaerben und bedrucken synthetischer fasermaterialien"
US4514186A (en) * 1982-04-11 1985-04-30 Ciba Geigy Corporation Aqueous formulations of water-insoluble or sparingly water-soluble dyes and hypophosphite/unsaturated acid teldmer
DE3227915A1 (de) * 1982-07-27 1984-02-02 Basf Ag, 6700 Ludwigshafen Waessrige konzentrierte loesungen von mischungen aus organischen komplexbildnern und dispergiermitteln auf basis von polymeren aliphatischen carbonsaeuren
US4595394A (en) * 1983-04-08 1986-06-17 Kao Corporation Agent for improving processability of cellulose fibers: acid polymer salts for improved scouring
LU84875A1 (fr) * 1983-06-27 1985-03-29 Oreal Compositions tinctoriales pour fibres keratiniques a base de colorants directs et de gomme de xanthane
US4648883A (en) * 1984-07-25 1987-03-10 Ciba-Geigy Corporation Process for the preparation of storage stable aqueous formulations of anionic dyes: amon exchange resin treatment
JPS61204276A (ja) * 1985-03-07 1986-09-10 Nippon Kayaku Co Ltd 反応性染料の安定な液状組成物
JPS61266683A (ja) * 1985-05-17 1986-11-26 花王株式会社 セルロ−ス系繊維用染色助剤
US4629470A (en) * 1985-10-18 1986-12-16 The United States Of America As Represented By The Secretary Of Agriculture Process for dyeing smooth-dry cellulosic fabric
JPH01192885A (ja) * 1988-01-22 1989-08-02 Kao Corp ポリエステル繊維の高温染色法
DE4024422A1 (de) * 1990-08-01 1992-02-06 Basf Ag Dispergiermittel fuer farbmittelzubereitungen
US5851236A (en) * 1996-08-15 1998-12-22 Clariant Finance (Bvi) Limited Aqueous, concentrated polycarboxylic acid sodium salt solutions, their production and use
TW515859B (en) 1997-12-17 2003-01-01 Ciba Sc Holding Ag Process for ink-jet printing textile fibre materials
US20040139566A1 (en) * 2003-01-03 2004-07-22 Szymanski Matthew A. Method for forming colored cellulosic materials
US8268338B2 (en) 2007-07-09 2012-09-18 Eastern Michigan University Bactericidal silver surfactant delivery into coating and polymer compositions
DE102008041338A1 (de) * 2008-08-19 2010-02-25 Evonik Röhm Gmbh Einfärbeprozess für Poly(meth)acrylate mit Flüssigfarben auf Wasserbasis und Flüssigfarben auf Wasserbasis
JP2014208928A (ja) * 2013-03-27 2014-11-06 ブラザー工業株式会社 抜染剤、収容容器、インクジェット記録装置、抜染方法、画像形成方法、抜染剤の安定化剤、及び抜染剤の安定化方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE634844A (fr) *
FR2049897A5 (fr) * 1969-06-12 1971-03-26 Ciba Geigy
US3940247A (en) * 1973-12-03 1976-02-24 Gaf Corporation Dye migration control with amine salt of poly(vinyl methyl ether/maleic acid)

Family Cites Families (30)

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US3223471A (en) * 1965-12-14 Process fgr dyeing textile materials
DE623404C (fr) * 1930-05-26
US2063987A (en) * 1931-09-18 1936-12-15 Dreyfus Henry Amino carboxylic acid condensation products and process of making them
US2146755A (en) * 1936-08-25 1939-02-14 Eastman Kodak Co Dye compositions
US2647094A (en) * 1950-08-19 1953-07-28 Monsanto Chemicals Pigment pastes comprising a pigment and a salt of a copolymer of styrene and a maleic half-ester
BE577868A (fr) * 1958-04-18
GB871193A (en) * 1959-04-01 1961-06-21 Ici Ltd Improved colouration process for textile materials
US3086831A (en) * 1959-07-01 1963-04-23 American Cyanamid Co Compositions of a pyrazolone azo dye with polyvinylpyrrolidone
US3139321A (en) * 1961-05-03 1964-06-30 Du Pont Vat dye-quaternary ammonium polyacrylate ester composition and continuous pad dyeingtherewith
US3467485A (en) * 1962-05-03 1969-09-16 Geigy Ag J R Process for the dyeing of polyamide fibers
NL6503790A (fr) * 1964-03-25 1965-09-27
US3484180A (en) * 1965-04-14 1969-12-16 American Aniline Prod Vat dye dispersions
US3545995A (en) * 1966-08-01 1970-12-08 Kao Corp Method of dispersing fine powders
AT289709B (de) * 1967-12-22 1971-05-10 Basf Ag Verfahren zur Verringerung der Schmutzadsorption an bindemittelhaltigen Pigmentfärbungen und -drucken auf Fasermaterialien
US3912677A (en) * 1970-05-14 1975-10-14 Ici Australia Ltd Compounds
BR7203579D0 (pt) 1971-06-02 1973-06-21 Gould Inc Estrutura catalitica capaz de catalisar a reducao de no
US3765832A (en) * 1972-04-14 1973-10-16 Gen Mills Chem Inc Dye solutions thickened with borax crosslinked polygalactomannan carboxy-, hydroxy- or carbanylalkyl ethers
JPS5023850B2 (fr) 1972-07-31 1975-08-11
DE2249443C2 (de) * 1972-10-09 1984-11-15 Cassella Ag, 6000 Frankfurt Wasserlösliche, Sulfonsäuregruppen enthaltende Copolymerisate und ihre Verwendung als Textilhilfsmittel
FR2227385B1 (fr) * 1973-04-27 1977-11-04 Ugine Kuhlmann
US3954609A (en) * 1973-05-29 1976-05-04 English Clays Lovering Pochin & Company Limited Particulate solid materials
US3861869A (en) * 1973-05-29 1975-01-21 Wolfgang Schwindt Printing textiles with acrylic acid copolymer paste
US3957427A (en) * 1973-12-03 1976-05-18 Gaf Corporation Control of dye migration by treating textile with aqueous dye bath containing an amide derivative of polyvinyl methyl ether/maleic anhydride
JPS5638711B2 (fr) 1974-01-09 1981-09-08
US3945843A (en) * 1974-07-22 1976-03-23 Nalco Chemical Company Acrylic acid copolymer as pigment dispersant
DE2444823C3 (de) * 1974-09-19 1982-05-19 Basf Ag, 6700 Ludwigshafen Verfahren zum Färben von Cellulosefasern
US4197087A (en) * 1975-12-29 1980-04-08 Daido-Maruta Finishing Co. Ltd. Liquid type dye preparations
US4095942A (en) * 1976-03-08 1978-06-20 Ciba-Geigy Corporation Printing of hydrophobic textiles without afterwash and product thereof
JPH03190274A (ja) * 1989-12-20 1991-08-20 Sanyo Electric Co Ltd ヘテロ接合バイポーラトランジスタ
JPH1038575A (ja) * 1996-07-29 1998-02-13 Hitachi Cable Ltd 方位検出装置の高域ノイズ除去方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE634844A (fr) *
FR2049897A5 (fr) * 1969-06-12 1971-03-26 Ciba Geigy
US3940247A (en) * 1973-12-03 1976-02-24 Gaf Corporation Dye migration control with amine salt of poly(vinyl methyl ether/maleic acid)

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
EXBK/78 *

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0014503A1 (fr) * 1979-02-02 1980-08-20 Rohner AG Pratteln Procédé de préparation de compositions solides dispersables en milieu aqueux de substances actives étant peu solubles à insolubles dans l'eau, fortement concentrées, finement dispersées, contenant peu ou pas d'agent dispersant
FR2497245A1 (fr) * 1980-12-30 1982-07-02 Protex Manuf Prod Chimiq Procede de teinture sur fibres cellulosiques et/ou synthetiques
EP0056991A2 (fr) * 1981-01-26 1982-08-04 Ciba-Geigy Ag Préparations tinctoriales liquides
EP0056991A3 (en) * 1981-01-26 1982-11-24 Ciba-Geigy Ag Liquid dyestuff preparations
EP0097291A1 (fr) * 1982-06-23 1984-01-04 Bayer Ag Préparations de colorants
EP0124866A1 (fr) * 1983-05-04 1984-11-14 Ciba-Geigy Ag Granules de colorant dispersables dans l'eau froide
EP0225287A1 (fr) * 1985-11-25 1987-06-10 Ciba-Geigy Ag Préparations stables au stockage de corps solides peu solubles ou insolubles dans l'eau
EP0738766A1 (fr) * 1995-04-20 1996-10-23 Clariant Finance (BVI) Limited Suspensions liquides stables de colorants au soufre et méthode pour les analyser
EP0824155A1 (fr) * 1996-08-15 1998-02-18 Clariant Finance (BVI) Limited Solutions aqueuses concentrées de sels de sodium d'acides polycarboxyliques, leur préparation et leur utilisation

Also Published As

Publication number Publication date
JPS53130727A (en) 1978-11-15
FR2388029B1 (fr) 1981-11-20
US4297100A (en) 1981-10-27
DE2816539A1 (de) 1978-10-26
JPS6327383B2 (fr) 1988-06-02
BR7802408A (pt) 1978-12-19
CH627490A5 (de) 1982-01-15
GB1603215A (en) 1981-11-18
IN148690B (fr) 1981-05-09
DE2816539C2 (de) 1989-02-02
CS196427B2 (en) 1980-03-31

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