FI964483A - Förfarande och anordning för utföring av kemiska reaktionen medelst mikrostrukturblandning - Google Patents

Förfarande och anordning för utföring av kemiska reaktionen medelst mikrostrukturblandning Download PDF

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Publication number
FI964483A
FI964483A FI964483A FI964483A FI964483A FI 964483 A FI964483 A FI 964483A FI 964483 A FI964483 A FI 964483A FI 964483 A FI964483 A FI 964483A FI 964483 A FI964483 A FI 964483A
Authority
FI
Finland
Prior art keywords
mixing
reaction chamber
chemical reactions
fluid filaments
free
Prior art date
Application number
FI964483A
Other languages
English (en)
Finnish (fi)
Other versions
FI964483A0 (sv
Inventor
Klaus Schubert
Wilhelm Bier
Gerd Linder
Dieter Seidel
Thomas Menzel
Bernd Koglin
Hans-Joerg Preisigke
Original Assignee
Bayer Ag
Karlsruhe Forschzent
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE4416343A external-priority patent/DE4416343C2/de
Priority claimed from DE4433439A external-priority patent/DE4433439A1/de
Application filed by Bayer Ag, Karlsruhe Forschzent filed Critical Bayer Ag
Publication of FI964483A0 publication Critical patent/FI964483A0/sv
Publication of FI964483A publication Critical patent/FI964483A/sv

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30Injector mixers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093Microreactors, e.g. miniaturised or microfabricated reactors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/20Jet mixers, i.e. mixers using high-speed fluid streams
    • B01F25/23Mixing by intersecting jets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40Static mixers
    • B01F25/42Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/43Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
    • B01F25/432Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction with means for dividing the material flow into separate sub-flows and for repositioning and recombining these sub-flows; Cross-mixing, e.g. conducting the outer layer of the material nearer to the axis of the tube or vice-versa
    • B01F25/4323Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction with means for dividing the material flow into separate sub-flows and for repositioning and recombining these sub-flows; Cross-mixing, e.g. conducting the outer layer of the material nearer to the axis of the tube or vice-versa using elements provided with a plurality of channels or using a plurality of tubes which can either be placed between common spaces or collectors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/30Micromixers
    • B01F33/301Micromixers using specific means for arranging the streams to be mixed, e.g. channel geometries or dispositions
    • B01F33/3012Interdigital streams, e.g. lamellae
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/30Micromixers
    • B01F33/301Micromixers using specific means for arranging the streams to be mixed, e.g. channel geometries or dispositions
    • B01F33/3017Mixing chamber
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/30Micromixers
    • B01F33/3039Micromixers with mixing achieved by diffusion between layers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/30Micromixers
    • B01F33/3045Micromixers using turbulence on microscale
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2415Tubular reactors
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D9/00Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D9/0031Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits for one heat-exchange medium being formed by paired plates touching each other
    • F28D9/0037Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits for one heat-exchange medium being formed by paired plates touching each other the conduits for the other heat-exchange medium also being formed by paired plates touching each other
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F3/00Plate-like or laminated elements; Assemblies of plate-like or laminated elements
    • F28F3/02Elements or assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with recesses, with corrugations
    • F28F3/04Elements or assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with recesses, with corrugations the means being integral with the element
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00121Controlling the temperature by direct heating or cooling
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00159Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00783Laminate assemblies, i.e. the reactor comprising a stack of plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00889Mixing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00993Design aspects
    • B01J2219/00995Mathematical modeling
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F2260/00Heat exchangers or heat exchange elements having special size, e.g. microstructures
    • F28F2260/02Heat exchangers or heat exchange elements having special size, e.g. microstructures having microchannels

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Dispersion Chemistry (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Accessories For Mixers (AREA)
FI964483A 1994-05-09 1996-11-07 Förfarande och anordning för utföring av kemiska reaktionen medelst mikrostrukturblandning FI964483A (sv)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE4416343A DE4416343C2 (de) 1994-05-09 1994-05-09 Statischer Mikro-Vermischer
DE4433439A DE4433439A1 (de) 1994-09-20 1994-09-20 Verfahren zur Durchführung chemischer Reaktionen mittels Mikrostruktur-Mischung
PCT/EP1995/001701 WO1995030476A1 (de) 1994-05-09 1995-05-05 Verfahren und vorrichtung zur durchführung chemischer reaktionen mittels mikrostruktur-mischung

Publications (2)

Publication Number Publication Date
FI964483A0 FI964483A0 (sv) 1996-11-07
FI964483A true FI964483A (sv) 1996-11-08

Family

ID=25936446

Family Applications (1)

Application Number Title Priority Date Filing Date
FI964483A FI964483A (sv) 1994-05-09 1996-11-07 Förfarande och anordning för utföring av kemiska reaktionen medelst mikrostrukturblandning

Country Status (10)

Country Link
EP (1) EP0758918B1 (sv)
JP (1) JP3633624B2 (sv)
KR (1) KR100372853B1 (sv)
AT (1) ATE170773T1 (sv)
CA (1) CA2189783A1 (sv)
DE (1) DE59503529D1 (sv)
DK (1) DK0758918T3 (sv)
ES (1) ES2120204T3 (sv)
FI (1) FI964483A (sv)
WO (1) WO1995030476A1 (sv)

Families Citing this family (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19540292C1 (de) * 1995-10-28 1997-01-30 Karlsruhe Forschzent Statischer Mikrovermischer
DE19541266A1 (de) * 1995-11-06 1997-05-07 Bayer Ag Verfahren und Vorrichtung zur Durchführung chemischer Reaktionen mittels eines Mikrostruktur-Lamellenmischers
DE19541265A1 (de) * 1995-11-06 1997-05-07 Bayer Ag Verfahren zur Herstellung von Dispersionen und zur Durchführung chemischer Reaktionen mit disperser Phase
DE19604289C2 (de) * 1996-02-07 1998-04-23 Danfoss As Mikromischer
DE19703779C2 (de) 1997-02-01 2003-06-05 Karlsruhe Forschzent Verfahren und Vorrichtung zur Herstellung eines dispersen Gemisches
DE19741645A1 (de) * 1997-09-22 1999-03-25 Bayer Ag Verfahren und Vorrichtung zur Oxidation organischer Verbindungen in flüssiger Phase unter Verwendung peroxidischer Oxidationsmittel
DE19748481C2 (de) * 1997-11-03 2003-09-25 Inst Mikrotechnik Mainz Gmbh Statischer Mikrovermischer
DE19800529A1 (de) * 1998-01-09 1999-07-15 Bayer Ag Verfahren zur Phosgenierung von Aminen in der Gasphase unter Einsatz von Mikrostrukturmischern
DE19917156B4 (de) * 1999-04-16 2006-01-19 INSTITUT FüR MIKROTECHNIK MAINZ GMBH Verfahren zur Herstellung einer Wasser-in-Dieselöl-Emulsion als Kraftstoff sowie dessen Verwendungen
DE19917148C2 (de) * 1999-04-16 2002-01-10 Inst Mikrotechnik Mainz Gmbh Verfahren und Mikrovermischer zur Herstellung einer Dispersion
DE19961257C2 (de) * 1999-12-18 2002-12-19 Inst Mikrotechnik Mainz Gmbh Mikrovermischer
DE10031381A1 (de) * 2000-06-28 2002-01-10 Merck Patent Gmbh Verfahren zur Kupplung von organischen Verbindungen
DE10055758A1 (de) * 2000-11-07 2002-05-16 Siemens Axiva Gmbh & Co Kg Verfahren zur Herstellung von Aldolen unter Verwendung eines mikrostrukturierten Reaktionssystems
DE10108485A1 (de) * 2001-02-22 2002-09-05 Bayer Ag Verbessertes Verfahren zur Herstellung von Polyetherpolyolen
DE10108484A1 (de) * 2001-02-22 2002-09-05 Bayer Ag Verbessertes Verfahren zur Herstelung von Polyetherpolyolen
DE10123093A1 (de) * 2001-05-07 2002-11-21 Inst Mikrotechnik Mainz Gmbh Verfahren und statischer Mikrovermischer zum Mischen mindestens zweier Fluide
DE10148615B4 (de) * 2001-09-26 2005-03-31 INSTITUT FüR MIKROTECHNIK MAINZ GMBH Verfahren und Vorrichtung zur Durchführung chemischer Prozesse
JP2003294596A (ja) * 2002-03-29 2003-10-15 Asahi Kasei Corp 混合機構
JP4585800B2 (ja) * 2003-09-29 2010-11-24 株式会社日立ハイテクノロジーズ 混合器及び液体分析装置
US7147364B2 (en) * 2003-09-29 2006-12-12 Hitachi High-Technologies Corporation Mixer and liquid analyzer provided with same
JP4485178B2 (ja) * 2003-12-01 2010-06-16 新日鐵化学株式会社 ビスフェノール類の製造方法
JP4547606B2 (ja) * 2004-03-17 2010-09-22 富士フイルム株式会社 マイクロリアクターの複合反応方法及びマイクロリアクター
JP5159018B2 (ja) * 2004-09-06 2013-03-06 洋太郎 畑村 混合装置
DE102004062074A1 (de) * 2004-12-23 2006-07-06 Forschungszentrum Karlsruhe Gmbh Statischer Mikrovermischer
US7938947B2 (en) 2005-02-21 2011-05-10 National University Corporation Okayama University Flow control device, microreactor and use thereof
DE102005025248B4 (de) * 2005-06-02 2009-07-30 Forschungszentrum Karlsruhe Gmbh Fluidführungssystem
JP4899681B2 (ja) 2006-07-18 2012-03-21 富士ゼロックス株式会社 マイクロ流路デバイス
JP5151204B2 (ja) 2007-03-27 2013-02-27 富士ゼロックス株式会社 マイクロ流路デバイス及びマイクロ流路デバイスの製造方法
JP5119848B2 (ja) 2007-10-12 2013-01-16 富士ゼロックス株式会社 マイクロリアクタ装置
JP4946778B2 (ja) * 2007-10-17 2012-06-06 株式会社日立プラントテクノロジー マイクロリアクタ
JP2010115624A (ja) 2008-11-14 2010-05-27 Fuji Xerox Co Ltd マイクロ流路デバイス、分離装置、並びに、分離方法
JP5003702B2 (ja) 2009-03-16 2012-08-15 富士ゼロックス株式会社 マイクロ流体素子及びマイクロ流体制御方法
EP2586521A4 (en) 2010-06-28 2016-03-02 Dainippon Ink & Chemicals MICRO MIXER
CN110508195A (zh) * 2019-09-03 2019-11-29 扬州大学 一种微通道混合流体单元、装置及系统
JP7391804B2 (ja) 2020-09-15 2023-12-05 株式会社東芝 流体制御器、及び、流体混合器

Family Cites Families (2)

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Publication number Priority date Publication date Assignee Title
US4313680A (en) * 1979-11-05 1982-02-02 Chevron Research Company Reactor for fast reactions
SE432059B (sv) * 1980-04-11 1984-03-19 Munters Ab Carl Blandningsanordning for blandning av strommande medier innefattande minst tva system av atskilda genomstromningskanaler

Also Published As

Publication number Publication date
KR970702748A (ko) 1997-06-10
EP0758918A1 (de) 1997-02-26
DE59503529D1 (de) 1998-10-15
CA2189783A1 (en) 1995-11-16
KR100372853B1 (ko) 2003-05-09
FI964483A0 (sv) 1996-11-07
ES2120204T3 (es) 1998-10-16
WO1995030476A1 (de) 1995-11-16
EP0758918B1 (de) 1998-09-09
DK0758918T3 (da) 1999-06-07
JP3633624B2 (ja) 2005-03-30
JPH09512742A (ja) 1997-12-22
ATE170773T1 (de) 1998-09-15

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