FI94764B - Karboximetylsulfoetylcellulosa och förfarande för dess framställning - Google Patents

Karboximetylsulfoetylcellulosa och förfarande för dess framställning Download PDF

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Publication number
FI94764B
FI94764B FI885692A FI885692A FI94764B FI 94764 B FI94764 B FI 94764B FI 885692 A FI885692 A FI 885692A FI 885692 A FI885692 A FI 885692A FI 94764 B FI94764 B FI 94764B
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FI
Finland
Prior art keywords
cmsec
carboxymethylsulfoethylcellulose
added
substitution
cellulose
Prior art date
Application number
FI885692A
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English (en)
Finnish (fi)
Other versions
FI94764C (sv
FI885692A (sv
FI885692A0 (sv
Inventor
Klaus Szablikowski
Klaus Balser
Dieter Herzog
Original Assignee
Wolff Walsrode Ag
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Publication of FI885692A0 publication Critical patent/FI885692A0/sv
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/60—Compositions for stimulating production by acting on the underground formation
    • C09K8/84—Compositions based on water or polar solvents
    • C09K8/86—Compositions based on water or polar solvents containing organic compounds
    • C09K8/88—Compositions based on water or polar solvents containing organic compounds macromolecular compounds
    • C09K8/90—Compositions based on water or polar solvents containing organic compounds macromolecular compounds of natural origin, e.g. polysaccharides, cellulose
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/731—Cellulose; Quaternized cellulose derivatives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B11/00—Preparation of cellulose ethers
    • C08B11/193—Mixed ethers, i.e. ethers with two or more different etherifying groups
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00—Materials not provided for elsewhere

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Animal Behavior & Ethology (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Biochemistry (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Dermatology (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)

Claims (4)

1. Karboximetylsulfoetylcellulosa (CMSEC), k d n -netecknad därav, att dess 1. substitutionsgrad dr 0,1 - 1 och substitutionsgrad är 0,3 ~ 1,2 och substi- tutionsgraderna följer den följande ekvationen; 0,5 £ DSsulfoetyl + D®karboximetyl ^ 10 2. viskositet 1 2-prosentig lösning dr 5 - 60 000 mPa · s (mätt vld en skdrnlngshastlghet av 2,5 s'1 vld en temperatur av 20 eC) och 3. transmlttans i 2-prosentig vattenlösning dr 15 > 95 % (det använda ljusets väglängd λ * 550 nm, kyvettens optiska längd 10 mm), och att den kan framstäilas genom företring av cellulosan i en alkalisk lösning med minst en en sul£oalkylgrupp av-givande förening SA och minst en en karboximetylgrupp av- 20 givande förening CM, varvid a) cellulosan suspenderas tili en sekunddr eller tertidr alkohol, b) suspensionen sammanfogas med föreningen SA och/eller CM, varvid ett pH-vdrde 0-9 erh&lls, 25 c) pH justeras ddrefter tili ett alkaliskt omr&de i 13 - 14 genom tillsdttning av en bas, d) företringen utförs vid en temperatur av 55 -100 eC och e) tillsdtts eventuellt ddrefter föreningen CM 30 och/eller SA vid en temperatur av 15 - 100 °C och ett pH : av 10 - 14, varvid CMSEC bildas.
2. Karboximetylsulfoetylcellulosa enligt patentkrav 1, kdnnetecknad därav, att endast föreningen SA tillsdtts i reaktionssteg b) och endast föreningen CM i 35 reaktionssteg e). ♦ 17 94764
3. Karboxlmetylsulfoetylcellulosa enligt patervtkrav 1, kännetecknad därav, att endast föreningen CM tlllsätts i reaktionssteg b) och endast föreningen SA 1 reaktlonssteg e). 5
4. Förfarande för framställning av en karboxlmetyl sulfoetylcellulosa CMSEC enligt patentkrav 1 genom föret-rlng av karboxlmetylcellulosa CMC 1 en alkallsk lösnlng med minst en en sulfoalkylgrupp avglvande förenlng SA, könnetecknat därav, att 10 a) CMC suspenderas tili en sekundär eller tertlär alkohol, b) suspenslonen sanunanfogas med föreningen SA, var-vld ett pH-värde 0-9 erhälls, c) pH justeras därefter tili ett alkaliskt omrdde 15 13 - 14 genom tillsättning av en bas, d) företrlngen utförs vld en temperatur av 55 -100 eC, varvid CMSEC blldas. * II
FI885692A 1987-12-11 1988-12-08 Karboximetylsulfoetylcellulosa och förfarande för dess framställning FI94764C (sv)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19873742106 DE3742106A1 (de) 1987-12-11 1987-12-11 Carboxymethylsulfoethylcellulose und verfahren zu ihrer herstellung
DE3742106 1987-12-11

Publications (4)

Publication Number Publication Date
FI885692A0 FI885692A0 (sv) 1988-12-08
FI885692A FI885692A (sv) 1989-06-12
FI94764B true FI94764B (sv) 1995-07-14
FI94764C FI94764C (sv) 1995-10-25

Family

ID=6342422

Family Applications (1)

Application Number Title Priority Date Filing Date
FI885692A FI94764C (sv) 1987-12-11 1988-12-08 Karboximetylsulfoetylcellulosa och förfarande för dess framställning

Country Status (4)

Country Link
US (1) US5001232A (sv)
EP (1) EP0319865B1 (sv)
DE (2) DE3742106A1 (sv)
FI (1) FI94764C (sv)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4024968A1 (de) * 1990-08-07 1992-07-09 Wolff Walsrode Ag Dihydroxypropylsulfoethylcellulosen, ihre herstellung und verwendung
DE4113892A1 (de) * 1991-04-27 1992-10-29 Wolff Walsrode Ag Wasserloesliche sulfoethylcelluloseether mit sehr guter loesungsqualitaet und verfahren zu ihrer herstellung
US5247072A (en) * 1991-10-25 1993-09-21 Kimberly-Clark Corporation Carboxyalkyl polysaccharides having improved absorbent properties and process for the preparation thereof
DE4203530A1 (de) * 1992-02-07 1993-08-12 Wolff Walsrode Ag Verwendung von wasserloeslichen sulfoalkylderivaten der cellulose in gips- und zementhaltigen massen
US5550189A (en) * 1992-04-17 1996-08-27 Kimberly-Clark Corporation Modified polysaccharides having improved absorbent properties and process for the preparation thereof
DE4241286A1 (de) * 1992-12-08 1994-06-09 Wolff Walsrode Ag Hochsubstituierte Carboxymethyl-sulfoethylcelluloseether, Verfahren zu deren Herstellung und Verwendung in Textildruckfarbpasten
DE4241289A1 (de) * 1992-12-08 1994-06-09 Wolff Walsrode Ag Hochsubstituierte Carboxymethyl-sulfoethylcelluloseether (CMSEC), Verfahren zu deren Herstellung und Verwendung im Textildruck
DE60119083D1 (de) * 2001-05-23 2006-06-01 Linificio E Canapificio Naz S Leinenfasern, die O-alkylierte Celluloseether enthalten, und Verfahren zu deren Herstellung
US20060142560A1 (en) * 2004-12-29 2006-06-29 Glasser Wolfgang G Sulfoalkylated cellulose
US20060142484A1 (en) * 2004-12-29 2006-06-29 Glasser Wolfgang G Sulfoalkylated cellulose polymer network
CN100365209C (zh) * 2005-12-30 2008-01-30 湖北达雅化工技术发展有限公司 一种涂布纸涂料保水剂及其制备方法
CN103788214B (zh) * 2014-01-17 2015-12-30 甘肃高歌伟业新材料科技有限公司 以秸秆为原料制备耐电解质印花糊料的方法
CN111789301A (zh) * 2020-07-11 2020-10-20 罗金火 多层式导流多孔体

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB659506A (en) * 1949-03-28 1951-10-24 Dow Chemical Co Improved method of making methyl carboxyalkyl ethers of cellulose
US2811519A (en) * 1954-02-05 1957-10-29 Eastman Kodak Co Mixed cellulose ethers and their preparation
US3357971A (en) * 1964-07-06 1967-12-12 Hercules Inc Mixed cellulose ethers
SU794098A1 (ru) * 1979-03-14 1981-01-07 Всесоюзный Научно-Исследовательскийи Экспериментальный Институт По Переработкехимических Волокон Композици дл печати текстильногоМАТЕРиАлА из АцЕТАТНыХ, ВиСКОзНыХ,НАТуРАльНыХ или СиНТЕТичЕСКиХпОлиАМидНыХ ВОлОКОН
DE3417952A1 (de) * 1984-05-15 1985-11-21 Hoechst Ag, 6230 Frankfurt Verfahren zur herstellung von wasserloeslichen cellulosemischethern
JPS63182301A (ja) * 1987-01-22 1988-07-27 Dai Ichi Kogyo Seiyaku Co Ltd 新規なセルロ−スエ−テルナトリウム塩及びその製造方法

Also Published As

Publication number Publication date
EP0319865B1 (de) 1994-06-22
EP0319865A3 (en) 1990-07-25
EP0319865A2 (de) 1989-06-14
FI94764C (sv) 1995-10-25
US5001232A (en) 1991-03-19
DE3742106A1 (de) 1989-06-22
FI885692A (sv) 1989-06-12
DE3850363D1 (de) 1994-07-28
FI885692A0 (sv) 1988-12-08

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Owner name: WOLFF WALSRODE AG