ES8104136A1 - Procedimiento y dispositivo para la regeneracion de acido sulfurico impurificado - Google Patents
Procedimiento y dispositivo para la regeneracion de acido sulfurico impurificadoInfo
- Publication number
- ES8104136A1 ES8104136A1 ES492361A ES492361A ES8104136A1 ES 8104136 A1 ES8104136 A1 ES 8104136A1 ES 492361 A ES492361 A ES 492361A ES 492361 A ES492361 A ES 492361A ES 8104136 A1 ES8104136 A1 ES 8104136A1
- Authority
- ES
- Spain
- Prior art keywords
- acid
- weight
- under
- concentrated
- pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/88—Concentration of sulfuric acid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/0094—Evaporating with forced circulation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/02—Evaporators with heating coils
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/26—Multiple-effect evaporating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/30—Accessories for evaporators ; Constructional details thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/90—Separation; Purification
- C01B17/905—Removal of organic impurities
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PROCEDIMIENTO Y DISPOSITIVO PARA LA REGENERACION DEL ACIDO SULFURICO. CONSISTE EN CONCENTRAR PRIMERAMENTE EL ACIDO EN UNA UNIDAD DE CONCENTRACION PREVIA DE DOS ETAPAS CALENTADA INDIRECTAMENTE, OBTENIENDOSE UNA CONCENTRACION DE SALIDA. A CONTINUACION, EL ACIDO SE CONDUCE A UNA UNIDAD DE ALTA CONCENTRACION, DONDE SE SOMETE A UNA TEMPERATURA COMPRENDIDA ENTRE 160 Y 250 GRADOS Y A UNA PRESION COMPRENDIDA ENTRE 30 Y 100 TORR, OBTENIENDOSE UNA CONCENTRACION DE UN 90 A UN 98,3 POR 100 EN PESO DE H2SO4. POR ULTIMO, EL ACIDO SE PASA A UNA ETAPA DE PURIFICACION, DONDE A PRESION ATMOSFERICA O MAS REDUCIDA Y A UNA TEMPERATURA COMPRENDIDA ENTRE 220 Y 350 GRADOS, EL ACIDO SE PURIFICA. EL DISPOSITIVO SE CARACTERIZA PORQUE EN LA PRIMERA ETAPA DE CONCENTRACION PREVIA LLEVA UN INTERCAMBIADOR DE CALOR, FORMADO POR UN HAZ DE TUBOS DE TANTALO, CONECTADO CON UN DEPOSITO DE VAPOR DE SALIDA, EN LA SEGUNDA ETAPA DE CONCENTRACION PREVIA LLEVA UN INTERCAMBIADOR DE CALOR, FORMADO POR TUBOS DE ACERO REVESTIDOS DE ESMALTE, CONECTADO CON UN DEPOSITO DE VAPOR DE SALIDA; EN LA ETAPA DE CONCENTRACION LLEVA UN INTERCAMBIADOR DE CALOR; Y EN LA ETAPA DE PURIFICACION LLEVA UN TUBO DE CRISTAL DE CUARZO CALENTADO POR RADIACION, UN DISPOSITIVO DE CALENTAMIENTO PARA CALENTAR EL ACIDO, UNA ZONA DE REACCION Y UNA ZONA DE REACCION ULTERIOR. R
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH551379A CH641126A5 (en) | 1979-06-13 | 1979-06-13 | Process and system for regenerating sulphuric acid |
DE19803018665 DE3018665A1 (de) | 1979-06-13 | 1980-05-16 | Verfahren und vorrichtung zum regenerieren von schwefelsaeure |
Publications (2)
Publication Number | Publication Date |
---|---|
ES492361A0 ES492361A0 (es) | 1981-04-16 |
ES8104136A1 true ES8104136A1 (es) | 1981-04-16 |
Family
ID=25697891
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES492361A Expired ES8104136A1 (es) | 1979-06-13 | 1980-06-12 | Procedimiento y dispositivo para la regeneracion de acido sulfurico impurificado |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP0022181B1 (es) |
CA (1) | CA1152285A (es) |
ES (1) | ES8104136A1 (es) |
FI (1) | FI67355C (es) |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3409717C2 (de) * | 1984-03-16 | 1994-03-31 | Bayer Ag | Verfahren zur Herstellung von Nitrobenzol |
DE3409719A1 (de) * | 1984-03-16 | 1985-09-19 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von dinitrotoluol |
DE3718675A1 (de) | 1987-06-04 | 1988-12-15 | Bayer Ag | Verfahren zum eindampfen von schwefelsaeure |
DE3935892C2 (de) * | 1989-10-27 | 1994-08-25 | Metallgesellschaft Ag | Verfahren und Vorrichtung zum Konzentrieren einer Schwefelsäure und Wasser enthaltenden Flüssigkeit |
DE3938915C1 (es) * | 1989-11-24 | 1991-05-08 | Bayer Ag, 5090 Leverkusen, De | |
DE4029737C1 (es) * | 1990-09-20 | 1991-12-05 | Metallgesellschaft Ag, 6000 Frankfurt, De | |
CH682398A5 (de) * | 1991-09-13 | 1993-09-15 | Escher Wyss Ag | Verfahren zur Energieeinsparung bei der Herstellung von Titandioxid. |
DE4213324A1 (de) * | 1992-04-23 | 1993-10-28 | Bayer Ag | Verfahren zum Konzentrieren und Reinigen von Schwefelsäure |
DE4230099C2 (de) * | 1992-09-09 | 1998-09-24 | Bayer Ag | Verfahren zum Regenerieren gebrauchter Schwefelsäure |
DE4403841C2 (de) * | 1994-02-08 | 1997-12-04 | Bayer Ag | Verfahren zum Eindampfen von Gebrauchtschwefelsäure |
DE19642328A1 (de) * | 1996-10-14 | 1998-04-16 | Bayer Ag | Verfahren zur Aufkonzentrierung von gebrauchten Schwefelsäuren |
DE19920695A1 (de) * | 1999-05-05 | 2000-11-16 | Metallgesellschaft Ag | Verfahren zur Aufkonzentrierung von Dünnsäure |
WO2008003297A2 (de) * | 2006-07-03 | 2008-01-10 | Lailach Guenter | Verfahren und anlage zum konzentrieren metallsulfathaltiger schwefelsäure |
EP2272796B1 (en) * | 2009-07-07 | 2020-08-05 | Haldor Topsøe A/S | Process for production of concentrated sulphuric acid from off-gas |
DE102020131827A1 (de) | 2020-12-01 | 2022-06-02 | Andreas Wilk | Vorrichtung und Verfahren zur Aufkonzentrierung korrosiver Flüssigkeiten |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1074019B (de) * | 1960-01-28 | Carl Buschm^ Hamburg Bergedorf Willy | Verfahren zur Reinigung und Konzentration von Ab fallschwefelsaure | |
FR1241856A (fr) * | 1959-08-13 | 1960-09-23 | Kestner App Evaporateurs | Procédé de concentration d'acide sulfurique à haute teneur |
DE2242055C3 (de) * | 1972-08-26 | 1979-05-31 | Industrie Chemie Thoma Gmbh, 6000 Frankfurt | Verfahren zur Konzentration und Reinigung von durch organische Substanzen verunreinigter Schwefelsäure |
-
1980
- 1980-06-09 EP EP19800103187 patent/EP0022181B1/de not_active Expired
- 1980-06-11 FI FI801880A patent/FI67355C/fi not_active IP Right Cessation
- 1980-06-11 CA CA000353787A patent/CA1152285A/en not_active Expired
- 1980-06-12 ES ES492361A patent/ES8104136A1/es not_active Expired
Also Published As
Publication number | Publication date |
---|---|
ES492361A0 (es) | 1981-04-16 |
CA1152285A (en) | 1983-08-23 |
EP0022181B1 (de) | 1983-10-12 |
EP0022181A2 (de) | 1981-01-14 |
FI801880A (fi) | 1980-12-14 |
EP0022181A3 (en) | 1981-08-26 |
FI67355C (fi) | 1985-03-11 |
FI67355B (fi) | 1984-11-30 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
ES8104136A1 (es) | Procedimiento y dispositivo para la regeneracion de acido sulfurico impurificado | |
JPS56104732A (en) | Preparation of silica glass | |
DE3061197D1 (en) | A method for the preparation of silica aerogel and its use | |
MX9802344A (es) | Metodo y aparato para producir bioxido de titanio. | |
GB816047A (en) | Process for refining crude silicon | |
ES8106762A1 (es) | Procedimiento para el tratamiento termico en horno de meta- les | |
GB1141260A (en) | A method and apparatus for the purification of hydrofluoric acid | |
ES8105304A1 (es) | Procedimiento para la obtencion de acido cianurico puro | |
DE3360724D1 (en) | Process for removing heavy metal ions and arsenic from wet-process phosphoric acid | |
HU9203611D0 (en) | Method for impregnating or simultaneous impregnating and drying of wood | |
NO840454L (no) | Fremgangsmaate og apparat for fremstilling av ammoniumnitrat | |
ES8104137A1 (es) | Procedimiento y dispositivo para la regeneracion de acido sulfurico impurificado | |
JPS56102519A (en) | Cold rolling method for stainless steel of high strength | |
ES423260A1 (es) | Un procedimiento para separar el fluor de las soluciones deacido fosforico. | |
Yanyuk | A Production Process for Rapid High Temperature Carburisation in High Voltage Electric Fields | |
DE3577979D1 (de) | Verfahren zum tempern von elastomeren und plastomeren gegenstaenden durch gleichzeitige behandlung mit waerme und vakuum in abwesenheit von sauerstoff und die so erhaltenen gegenstaende. | |
LAZAR et al. | CHEMICAL METHOD FOR THE PURIFICATION OF NATURAL GRAPHITE. | |
JPS54144764A (en) | Method of treating borofluoride in waste water | |
JPS5562809A (en) | Purifying method of sodium aluminate solution | |
JPS575323A (en) | Heat treating method for semiconductor wafer | |
JPS57210840A (en) | Manufacture for hollow rubber product stuck to a solid member | |
JPS5588830A (en) | Regenerating method of absorbing solution for acidic gas | |
IN170882B (es) | ||
JPS53139222A (en) | Heavy water reactor pressure pipe rolled joint method | |
Skryabina et al. | Certain Characteristics of Synergistic Microplasticity Effects Observed During the Electrolytic Hydrogenation of Iron |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
FD1A | Patent lapsed |
Effective date: 19970519 |