ES8104136A1 - Procedimiento y dispositivo para la regeneracion de acido sulfurico impurificado - Google Patents

Procedimiento y dispositivo para la regeneracion de acido sulfurico impurificado

Info

Publication number
ES8104136A1
ES8104136A1 ES492361A ES492361A ES8104136A1 ES 8104136 A1 ES8104136 A1 ES 8104136A1 ES 492361 A ES492361 A ES 492361A ES 492361 A ES492361 A ES 492361A ES 8104136 A1 ES8104136 A1 ES 8104136A1
Authority
ES
Spain
Prior art keywords
acid
weight
under
concentrated
pressure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES492361A
Other languages
English (en)
Other versions
ES492361A0 (es
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BERTRAMS AG
Bayer AG
Original Assignee
BERTRAMS AG
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from CH551379A external-priority patent/CH641126A5/de
Application filed by BERTRAMS AG, Bayer AG filed Critical BERTRAMS AG
Publication of ES492361A0 publication Critical patent/ES492361A0/es
Publication of ES8104136A1 publication Critical patent/ES8104136A1/es
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/88—Concentration of sulfuric acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/0094—Evaporating with forced circulation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/02—Evaporators with heating coils
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/26—Multiple-effect evaporating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/30—Accessories for evaporators ; Constructional details thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/90—Separation; Purification
    • C01B17/905—Removal of organic impurities

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

PROCEDIMIENTO Y DISPOSITIVO PARA LA REGENERACION DEL ACIDO SULFURICO. CONSISTE EN CONCENTRAR PRIMERAMENTE EL ACIDO EN UNA UNIDAD DE CONCENTRACION PREVIA DE DOS ETAPAS CALENTADA INDIRECTAMENTE, OBTENIENDOSE UNA CONCENTRACION DE SALIDA. A CONTINUACION, EL ACIDO SE CONDUCE A UNA UNIDAD DE ALTA CONCENTRACION, DONDE SE SOMETE A UNA TEMPERATURA COMPRENDIDA ENTRE 160 Y 250 GRADOS Y A UNA PRESION COMPRENDIDA ENTRE 30 Y 100 TORR, OBTENIENDOSE UNA CONCENTRACION DE UN 90 A UN 98,3 POR 100 EN PESO DE H2SO4. POR ULTIMO, EL ACIDO SE PASA A UNA ETAPA DE PURIFICACION, DONDE A PRESION ATMOSFERICA O MAS REDUCIDA Y A UNA TEMPERATURA COMPRENDIDA ENTRE 220 Y 350 GRADOS, EL ACIDO SE PURIFICA. EL DISPOSITIVO SE CARACTERIZA PORQUE EN LA PRIMERA ETAPA DE CONCENTRACION PREVIA LLEVA UN INTERCAMBIADOR DE CALOR, FORMADO POR UN HAZ DE TUBOS DE TANTALO, CONECTADO CON UN DEPOSITO DE VAPOR DE SALIDA, EN LA SEGUNDA ETAPA DE CONCENTRACION PREVIA LLEVA UN INTERCAMBIADOR DE CALOR, FORMADO POR TUBOS DE ACERO REVESTIDOS DE ESMALTE, CONECTADO CON UN DEPOSITO DE VAPOR DE SALIDA; EN LA ETAPA DE CONCENTRACION LLEVA UN INTERCAMBIADOR DE CALOR; Y EN LA ETAPA DE PURIFICACION LLEVA UN TUBO DE CRISTAL DE CUARZO CALENTADO POR RADIACION, UN DISPOSITIVO DE CALENTAMIENTO PARA CALENTAR EL ACIDO, UNA ZONA DE REACCION Y UNA ZONA DE REACCION ULTERIOR. R
ES492361A 1979-06-13 1980-06-12 Procedimiento y dispositivo para la regeneracion de acido sulfurico impurificado Expired ES8104136A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH551379A CH641126A5 (en) 1979-06-13 1979-06-13 Process and system for regenerating sulphuric acid
DE19803018665 DE3018665A1 (de) 1979-06-13 1980-05-16 Verfahren und vorrichtung zum regenerieren von schwefelsaeure

Publications (2)

Publication Number Publication Date
ES492361A0 ES492361A0 (es) 1981-04-16
ES8104136A1 true ES8104136A1 (es) 1981-04-16

Family

ID=25697891

Family Applications (1)

Application Number Title Priority Date Filing Date
ES492361A Expired ES8104136A1 (es) 1979-06-13 1980-06-12 Procedimiento y dispositivo para la regeneracion de acido sulfurico impurificado

Country Status (4)

Country Link
EP (1) EP0022181B1 (es)
CA (1) CA1152285A (es)
ES (1) ES8104136A1 (es)
FI (1) FI67355C (es)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3409717C2 (de) * 1984-03-16 1994-03-31 Bayer Ag Verfahren zur Herstellung von Nitrobenzol
DE3409719A1 (de) * 1984-03-16 1985-09-19 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von dinitrotoluol
DE3718675A1 (de) * 1987-06-04 1988-12-15 Bayer Ag Verfahren zum eindampfen von schwefelsaeure
DE3935892C2 (de) * 1989-10-27 1994-08-25 Metallgesellschaft Ag Verfahren und Vorrichtung zum Konzentrieren einer Schwefelsäure und Wasser enthaltenden Flüssigkeit
DE3938915C1 (es) * 1989-11-24 1991-05-08 Bayer Ag, 5090 Leverkusen, De
DE4029737C1 (es) * 1990-09-20 1991-12-05 Metallgesellschaft Ag, 6000 Frankfurt, De
CH682398A5 (de) * 1991-09-13 1993-09-15 Escher Wyss Ag Verfahren zur Energieeinsparung bei der Herstellung von Titandioxid.
DE4213324A1 (de) * 1992-04-23 1993-10-28 Bayer Ag Verfahren zum Konzentrieren und Reinigen von Schwefelsäure
DE4230099C2 (de) * 1992-09-09 1998-09-24 Bayer Ag Verfahren zum Regenerieren gebrauchter Schwefelsäure
DE4403841C2 (de) * 1994-02-08 1997-12-04 Bayer Ag Verfahren zum Eindampfen von Gebrauchtschwefelsäure
DE19642328A1 (de) * 1996-10-14 1998-04-16 Bayer Ag Verfahren zur Aufkonzentrierung von gebrauchten Schwefelsäuren
DE19920695A1 (de) * 1999-05-05 2000-11-16 Metallgesellschaft Ag Verfahren zur Aufkonzentrierung von Dünnsäure
WO2008003297A2 (de) * 2006-07-03 2008-01-10 Lailach Guenter Verfahren und anlage zum konzentrieren metallsulfathaltiger schwefelsäure
EP2272796B1 (en) * 2009-07-07 2020-08-05 Haldor Topsøe A/S Process for production of concentrated sulphuric acid from off-gas
DE102020131827A1 (de) 2020-12-01 2022-06-02 Andreas Wilk Vorrichtung und Verfahren zur Aufkonzentrierung korrosiver Flüssigkeiten

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1074019B (de) * 1960-01-28 Carl Buschm^ Hamburg Bergedorf Willy Verfahren zur Reinigung und Konzentration von Ab fallschwefelsaure
FR1241856A (fr) * 1959-08-13 1960-09-23 Kestner App Evaporateurs Procédé de concentration d'acide sulfurique à haute teneur
DE2242055C3 (de) * 1972-08-26 1979-05-31 Industrie Chemie Thoma Gmbh, 6000 Frankfurt Verfahren zur Konzentration und Reinigung von durch organische Substanzen verunreinigter Schwefelsäure

Also Published As

Publication number Publication date
FI67355B (fi) 1984-11-30
EP0022181A3 (en) 1981-08-26
FI67355C (fi) 1985-03-11
ES492361A0 (es) 1981-04-16
CA1152285A (en) 1983-08-23
EP0022181B1 (de) 1983-10-12
FI801880A (fi) 1980-12-14
EP0022181A2 (de) 1981-01-14

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Legal Events

Date Code Title Description
FD1A Patent lapsed

Effective date: 19970519