ES2539368T3 - Procedimiento y dispositivo para la desgasificación de azufre líquido - Google Patents
Procedimiento y dispositivo para la desgasificación de azufre líquido Download PDFInfo
- Publication number
- ES2539368T3 ES2539368T3 ES11290609.4T ES11290609T ES2539368T3 ES 2539368 T3 ES2539368 T3 ES 2539368T3 ES 11290609 T ES11290609 T ES 11290609T ES 2539368 T3 ES2539368 T3 ES 2539368T3
- Authority
- ES
- Spain
- Prior art keywords
- sulfur
- zone
- gas
- chamber
- liquid sulfur
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 229910052717 sulfur Inorganic materials 0.000 title claims abstract description 208
- 239000011593 sulfur Substances 0.000 title claims abstract description 208
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title claims abstract description 206
- 239000007788 liquid Substances 0.000 title claims abstract description 113
- 238000007872 degassing Methods 0.000 title claims abstract description 60
- 238000000034 method Methods 0.000 title claims abstract description 56
- 239000007789 gas Substances 0.000 claims abstract description 152
- 238000000926 separation method Methods 0.000 claims abstract description 22
- 239000011261 inert gas Substances 0.000 claims abstract description 13
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000001301 oxygen Substances 0.000 claims abstract description 10
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 10
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims description 84
- 238000005507 spraying Methods 0.000 claims description 35
- 230000008569 process Effects 0.000 claims description 30
- 238000002347 injection Methods 0.000 claims description 15
- 239000007924 injection Substances 0.000 claims description 15
- 238000005192 partition Methods 0.000 claims description 14
- 239000007921 spray Substances 0.000 claims description 8
- 238000006424 Flood reaction Methods 0.000 claims description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 90
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 74
- 239000012071 phase Substances 0.000 description 27
- 230000005587 bubbling Effects 0.000 description 16
- 239000001257 hydrogen Substances 0.000 description 16
- 229910052739 hydrogen Inorganic materials 0.000 description 16
- 229920001021 polysulfide Polymers 0.000 description 16
- 150000008117 polysulfides Polymers 0.000 description 16
- 239000005077 polysulfide Substances 0.000 description 15
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 13
- 238000006243 chemical reaction Methods 0.000 description 12
- 239000007791 liquid phase Substances 0.000 description 11
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 description 10
- 230000032258 transport Effects 0.000 description 10
- 238000007254 oxidation reaction Methods 0.000 description 9
- 238000010408 sweeping Methods 0.000 description 9
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 8
- 230000015572 biosynthetic process Effects 0.000 description 8
- 239000003054 catalyst Substances 0.000 description 8
- 239000000126 substance Substances 0.000 description 8
- 239000002253 acid Substances 0.000 description 7
- 238000000354 decomposition reaction Methods 0.000 description 7
- 238000009434 installation Methods 0.000 description 7
- 230000001105 regulatory effect Effects 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 239000002912 waste gas Substances 0.000 description 6
- 238000001816 cooling Methods 0.000 description 5
- 238000009792 diffusion process Methods 0.000 description 5
- 238000000605 extraction Methods 0.000 description 5
- 230000002349 favourable effect Effects 0.000 description 5
- 230000003647 oxidation Effects 0.000 description 5
- 238000005086 pumping Methods 0.000 description 5
- 150000003464 sulfur compounds Chemical class 0.000 description 5
- 229910021529 ammonia Inorganic materials 0.000 description 4
- 238000002485 combustion reaction Methods 0.000 description 4
- 238000010924 continuous production Methods 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 238000010348 incorporation Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 238000005260 corrosion Methods 0.000 description 3
- 230000007797 corrosion Effects 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 150000003463 sulfur Chemical class 0.000 description 3
- 230000007704 transition Effects 0.000 description 3
- 229910001868 water Inorganic materials 0.000 description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical class [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 description 2
- SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 230000033228 biological regulation Effects 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 239000008246 gaseous mixture Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- -1 heterocyclic nitrogen compounds Chemical class 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 230000000149 penetrating effect Effects 0.000 description 2
- 231100000614 poison Toxicity 0.000 description 2
- 230000007096 poisonous effect Effects 0.000 description 2
- 238000009625 Frasch process Methods 0.000 description 1
- GVGLGOZIDCSQPN-PVHGPHFFSA-N Heroin Chemical compound O([C@H]1[C@H](C=C[C@H]23)OC(C)=O)C4=C5[C@@]12CCN(C)[C@@H]3CC5=CC=C4OC(C)=O GVGLGOZIDCSQPN-PVHGPHFFSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 230000035508 accumulation Effects 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000006477 desulfuration reaction Methods 0.000 description 1
- 230000023556 desulfurization Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 229940083124 ganglion-blocking antiadrenergic secondary and tertiary amines Drugs 0.000 description 1
- 239000007792 gaseous phase Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000003999 initiator Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229910017464 nitrogen compound Inorganic materials 0.000 description 1
- 230000002085 persistent effect Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 239000003380 propellant Substances 0.000 description 1
- 125000002943 quinolinyl group Chemical group N1=C(C=CC2=CC=CC=C12)* 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 239000011949 solid catalyst Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0042—Degasification of liquids modifying the liquid flow
- B01D19/0047—Atomizing, spraying, trickling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0005—Degasification of liquids with one or more auxiliary substances
- B01D19/001—Degasification of liquids with one or more auxiliary substances by bubbling steam through the liquid
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/02—Preparation of sulfur; Purification
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/02—Preparation of sulfur; Purification
- C01B17/0232—Purification, e.g. degassing
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Degasification And Air Bubble Elimination (AREA)
- Gas Separation By Absorption (AREA)
- Treating Waste Gases (AREA)
- Physical Water Treatments (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Filling Or Discharging Of Gas Storage Vessels (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP11290609.4A EP2607304B1 (de) | 2011-12-23 | 2011-12-23 | Verfahren und Vorrichtung zur Entgasung von flüssigem Schwefel |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2539368T3 true ES2539368T3 (es) | 2015-06-30 |
Family
ID=47137716
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES11290609.4T Active ES2539368T3 (es) | 2011-12-23 | 2011-12-23 | Procedimiento y dispositivo para la desgasificación de azufre líquido |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US10131542B2 (cg-RX-API-DMAC7.html) |
| EP (1) | EP2607304B1 (cg-RX-API-DMAC7.html) |
| CN (1) | CN104114481B (cg-RX-API-DMAC7.html) |
| DE (1) | DE102012005450B4 (cg-RX-API-DMAC7.html) |
| ES (1) | ES2539368T3 (cg-RX-API-DMAC7.html) |
| IN (1) | IN2014MN00924A (cg-RX-API-DMAC7.html) |
| PL (1) | PL2607304T3 (cg-RX-API-DMAC7.html) |
| RU (1) | RU2629077C2 (cg-RX-API-DMAC7.html) |
| WO (1) | WO2013091972A1 (cg-RX-API-DMAC7.html) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102017001093A1 (de) | 2016-04-07 | 2017-10-26 | Entex Rust & Mitschke Gmbh | Entgasen bei der Extrusion von Kunststoffen mit Filterscheiben aus Sintermetall |
| DE102015001167A1 (de) | 2015-02-02 | 2016-08-04 | Entex Rust & Mitschke Gmbh | Entgasen bei der Extrusion von Kunststoffen |
| CN108367207B (zh) | 2015-10-05 | 2021-08-24 | 氟石科技公司 | 用于硫的脱气的系统和方法 |
| DE102017004563A1 (de) | 2017-03-05 | 2018-09-06 | Entex Rust & Mitschke Gmbh | Entgasen beim Extrudieren von Polymeren |
| CN107083316A (zh) * | 2017-05-22 | 2017-08-22 | 浙江农林大学 | 一种去除葡萄酒中二氧化硫的装置及其使用方法 |
| DE102018001412A1 (de) | 2017-12-11 | 2019-06-13 | Entex Rust & Mitschke Gmbh | Entgasen beim Extrudieren von Stoffen, vorzugsweise von Kunststoffen |
| DE102018206313A1 (de) * | 2018-04-24 | 2019-10-24 | Krones Ag | Entgasungsanlage und Verfahren zum Durchführen eines Entgasungsprozesses einer Flüssigkeit und Getränkebehandlungsmaschine |
| US10836637B2 (en) * | 2018-07-31 | 2020-11-17 | Controls Southeast, Inc. | Contactor apparatus and method of use |
| CN111474291B (zh) * | 2019-01-23 | 2022-08-30 | 中国石油天然气股份有限公司 | 一种液体硫磺中总硫化氢含量的催化剂化学测定方法 |
| US11713246B2 (en) | 2019-03-15 | 2023-08-01 | Fluor Technologies Corporation | Liquid sulfur degassing |
| CN111420430B (zh) * | 2020-04-10 | 2024-12-10 | 上海蓝滨石化设备有限责任公司 | 一种液硫脱气装置及其组成的橇装集成设备 |
| CN115724407B (zh) * | 2021-08-31 | 2024-07-16 | 中国石油化工股份有限公司 | 一种液硫脱气装置及方法 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL173735C (nl) * | 1972-05-24 | 1988-06-16 | Shell Int Research | Werkwijze voor het verwijderen van waterstofsulfide uit gesmolten zwavel. |
| US4131437A (en) * | 1975-12-19 | 1978-12-26 | Exxon Research & Engineering Co. | Process for the continuous multistage degasification of liquid sulfur |
| DE2842141A1 (de) | 1978-09-28 | 1980-04-10 | Union Rheinische Braunkohlen | Verfahren zur entfernung von schwefelwasserstoff aus fluessigem schwefel |
| DE3417230A1 (de) | 1984-05-10 | 1985-11-14 | Metallgesellschaft Ag, 6000 Frankfurt | Verfahren und vorrichtung zum entgasen von schwefelwasserstoffhaltigem fluessigem schwefel |
| FR2601350B1 (fr) | 1986-07-10 | 1988-09-30 | Elf Aquitaine | Procede pour l'elimination rapide de l'hydrogene sulfure contenu dans le soufre liquide et systeme catalytique utilisable pour sa mise en oeuvre |
| JPS63222005A (ja) * | 1987-03-09 | 1988-09-14 | Jgc Corp | 粗製液体硫黄の精製方法 |
| DE4331126A1 (de) | 1993-09-14 | 1995-03-16 | Ruhr Oel Gmbh | Verfahren zur Entfernung von Schwefelwasserstoff aus flüssigem Schwefel |
| CA2160412A1 (en) * | 1994-10-13 | 1996-04-14 | Adolf Frederik Scheybeler | Method and apparatus for degassing sulphur |
| NL1003085C2 (nl) * | 1995-09-15 | 1997-03-20 | Stork Comprimo Bv | Werkwijze en inrichting voor het ontgassen van zwavel. |
| US5632967A (en) * | 1995-09-19 | 1997-05-27 | Goar, Allison & Associates, Inc. | Process for the high pressure degassing of hydrogen sulfide from liquid sulfur |
| US6676918B2 (en) | 2002-06-14 | 2004-01-13 | Exxonmobil Research And Engineering Company | Hydrogen sulfide removal from liquid sulfur |
| US7081233B2 (en) * | 2004-05-18 | 2006-07-25 | Dynamax Engineering Ltd. | Method and apparatus for degassing liquid sulfur |
| RU2353576C2 (ru) * | 2006-12-04 | 2009-04-27 | Антон Александрович Пшегорский | Способ дегазации жидкой серы |
| US7927577B2 (en) | 2009-01-12 | 2011-04-19 | Worleyparsons Group, Inc. | Sulfur collection systems and processes with integrated degassing |
| US8084013B2 (en) * | 2009-07-22 | 2011-12-27 | Kps Technology & Engineering Llc | Method and apparatus for degasification of claus-derived sulfur |
| US8663596B2 (en) * | 2010-01-25 | 2014-03-04 | Fluor Enterprises, Inc. | Reactor, a structure packing, and a method for improving oxidation of hydrogen sulfide or polysulfides in liquid sulfur |
-
2011
- 2011-12-23 PL PL11290609T patent/PL2607304T3/pl unknown
- 2011-12-23 ES ES11290609.4T patent/ES2539368T3/es active Active
- 2011-12-23 EP EP11290609.4A patent/EP2607304B1/de not_active Not-in-force
-
2012
- 2012-03-20 DE DE102012005450A patent/DE102012005450B4/de not_active Expired - Fee Related
- 2012-11-05 US US14/368,180 patent/US10131542B2/en not_active Expired - Fee Related
- 2012-11-05 IN IN924MUN2014 patent/IN2014MN00924A/en unknown
- 2012-11-05 CN CN201280062999.1A patent/CN104114481B/zh not_active Expired - Fee Related
- 2012-11-05 RU RU2014130137A patent/RU2629077C2/ru active
- 2012-11-05 WO PCT/EP2012/071808 patent/WO2013091972A1/de not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| WO2013091972A1 (de) | 2013-06-27 |
| DE102012005450B4 (de) | 2013-07-04 |
| US20140366731A1 (en) | 2014-12-18 |
| IN2014MN00924A (cg-RX-API-DMAC7.html) | 2015-04-17 |
| RU2014130137A (ru) | 2016-02-20 |
| CN104114481A (zh) | 2014-10-22 |
| RU2629077C2 (ru) | 2017-08-24 |
| PL2607304T3 (pl) | 2015-08-31 |
| EP2607304A1 (de) | 2013-06-26 |
| EP2607304B1 (de) | 2015-03-25 |
| CN104114481B (zh) | 2017-02-22 |
| DE102012005450A1 (de) | 2013-06-27 |
| US10131542B2 (en) | 2018-11-20 |
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