ES2175682T3 - Procedimiento para la obtencion de hexametilendiamina a partir de mezclas, que contienen hexametilendiamina. - Google Patents

Procedimiento para la obtencion de hexametilendiamina a partir de mezclas, que contienen hexametilendiamina.

Info

Publication number
ES2175682T3
ES2175682T3 ES98908025T ES98908025T ES2175682T3 ES 2175682 T3 ES2175682 T3 ES 2175682T3 ES 98908025 T ES98908025 T ES 98908025T ES 98908025 T ES98908025 T ES 98908025T ES 2175682 T3 ES2175682 T3 ES 2175682T3
Authority
ES
Spain
Prior art keywords
mixture
hexametilendiamine
procedure
submitted
distillation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES98908025T
Other languages
English (en)
Inventor
Peter Bassler
Rolf Fischer
Hermann Luyken
Alwin Rehfinger
Guido Voit
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=7819564&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES2175682(T3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2175682T3 publication Critical patent/ES2175682T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82—Purification; Separation; Stabilisation; Use of additives
    • C07C209/84—Purification
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/20—Power plant

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyamides (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

LA INVENCION SE REFIERE A UN PROCEDIMIENTO PARA OBTENER HEXAMETIL - DIAMINA (I) A PARTIR DE MEZCLA (II) QUE CONTIENE (I) HEXAMETIL - DIAMINA, (III) HEXAMETILENIMINA, (IV) UN COMPUESTO SELECCIONADO ENTRE EL GRUPO FORMADO POR LA 2 - AMINOMETIL CICLOPENTILAMINA Y EL 1,2 - DIAMINOCICLOHEXANO, (V) UNA IMINA, Y (VI) ADIPONITRILO Y NITRILO DEL ACIDO 6 - AMINOCAPROICO. SEGUN DICHO PROCEDIMIENTO, (A) UNA MEZCLA (II) SE SOMETE A DESTILACION, PRODUCIENDO (A1) UNA FRACCION CON BAJO PUNTO DE EBULLICION QUE CONTIENE BASICAMENTE (III), (A2) UNA FRACCION CON PUNTO MEDIO DE EBULLICION (VII) QUE CONTIENE (I), (IV) Y (V), Y (A3) UNA FRACCION CON ELEVADO PUNTO DE EBULLICION QUE CONTIENE (V) Y (VI); (B) UNA MEZCLA (VII) SE SOMETE A DESTILACION, PRODUCIENDO (B1) UN PRODUCTO SITUADO EN LA PARTE SUPERIOR QUE CONTIENE ESENCIALMENTE (IV) Y (B2), UNA MEZCLA (VIII) QUE CONTIENE (I) Y (V) COMO RESIDUO EN LA PARTE INFERIOR; Y (C) UNA MEZCLA (VIII) SE SOMETE A DESTILACION, PRODUCIENDO (C1) (I) COMO RESIDUO EN LA PARTE SUPERIOR Y (C2) UN RESIDUO EN LA PARTE INFERIOR QUE CONTIENE LA PARTE ESENCIAL DE (V).
ES98908025T 1997-02-07 1998-01-30 Procedimiento para la obtencion de hexametilendiamina a partir de mezclas, que contienen hexametilendiamina. Expired - Lifetime ES2175682T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19704612A DE19704612A1 (de) 1997-02-07 1997-02-07 Verfahren zur Gewinnung von Hexamethylendiamin aus Hexamethylendiamin enthaltenden Mischungen

Publications (1)

Publication Number Publication Date
ES2175682T3 true ES2175682T3 (es) 2002-11-16

Family

ID=7819564

Family Applications (1)

Application Number Title Priority Date Filing Date
ES98908025T Expired - Lifetime ES2175682T3 (es) 1997-02-07 1998-01-30 Procedimiento para la obtencion de hexametilendiamina a partir de mezclas, que contienen hexametilendiamina.

Country Status (15)

Country Link
US (1) US6139693A (es)
EP (1) EP0961767B1 (es)
JP (1) JP2001511166A (es)
KR (1) KR100527321B1 (es)
CN (1) CN1227216C (es)
AR (1) AR011635A1 (es)
AU (1) AU6618098A (es)
BR (2) BR9807166A (es)
CA (1) CA2280889C (es)
DE (2) DE19704612A1 (es)
ES (1) ES2175682T3 (es)
ID (1) ID23371A (es)
MY (1) MY127867A (es)
TW (1) TW512139B (es)
WO (1) WO1998034903A1 (es)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR9711729A (pt) * 1996-09-10 1999-08-24 Basf Ag Processo para separar 2-aminometilciclopentilamina de uma mistura compreendendo hexametilenodiamina e 2-aminometilciclopentilamina
DE19839338A1 (de) 1998-08-28 2000-03-02 Basf Ag Verbessertes Verfahren zur gleizeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin
DE10029187A1 (de) * 2000-06-19 2001-12-20 Basf Ag Verfahren zur Abtrennung von 6-Aminocapronitril aus Gemischen, die 6-Aminocapronitril, Adipodinitril und Hexamethylendiamin enthalten
WO2003042159A1 (de) * 2001-11-16 2003-05-22 Basf Aktiengesellschaft Verfahren zur isolierung von aminen aus wässrigen lösungen
US6599398B1 (en) * 2002-07-17 2003-07-29 E. I. Du Pont De Nemours And Company Recovery of adiponitrile from a mixture of adiponitrile, aminocapronitrile and hexamethylenediamine
US6887352B2 (en) * 2003-03-07 2005-05-03 Invista North America S.A.R.L. Distillative method for separating hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine
FR2857965B1 (fr) * 2003-07-25 2005-08-26 Rhodia Polyamide Intermediates Procede de fabrication et de separation de composes dinitriles
US7468119B2 (en) * 2004-09-10 2008-12-23 Invista North America S.A.R.L. Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine
US7208632B2 (en) * 2004-09-10 2007-04-24 Invista North America S.A R.L. Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine
FR2902425B1 (fr) * 2006-06-20 2008-07-18 Rhodia Recherches & Tech Procede de fabrication de diamines primaires
FR2922207B1 (fr) * 2007-10-11 2009-12-04 Rhodia Operations Procede de purification d'hexamethylene diamine
CN102482198B (zh) 2009-07-31 2016-06-15 陶氏环球技术有限责任公司 将还原性氨化反应溶剂和杂质与一种或多种脂肪族二胺分离的方法
KR20200128086A (ko) * 2018-02-27 2020-11-11 바스프 에스이 지방족 1차 디아민을 포함하는 혼합물로부터 알칸올아민을 분리하는 방법
WO2025119889A1 (en) 2023-12-07 2025-06-12 Basf Se Process for manufacturing an aliphatic diamine

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2208598A (en) * 1938-09-24 1940-07-23 Du Pont Aliphatic amino-nitriles and process of producing them
DE848654C (de) * 1950-08-19 1952-09-08 Basf Ag Verfahren zur Herstellung von partiellen Hydrierungsprodukten des Adipinsaeuredinitrils
GB731819A (en) * 1951-04-11 1955-06-15 Du Pont Improvements in or relating to the production of hexamethylene diamine and salts thereof
DE954416C (de) * 1952-11-04 1956-12-20 Basf Ag Verfahren zur Herstellung von Aminonitrilen und Diaminen
US2762835A (en) * 1953-03-12 1956-09-11 Celanese Corp Preparation of amino nitriles
DE1204681B (de) * 1959-04-15 1965-11-11 Monsanto Co Verfahren zur Entfernung geringer Mengen ungesaettigter Verbindungen aus raffiniertem Hexamethylendiamin
US3775258A (en) * 1972-04-27 1973-11-27 Du Pont Canada Purification of adiponitrile
US4282381A (en) * 1980-08-21 1981-08-04 E. I. Du Pont De Nemours And Company Process for purifying hexamethylenediamine
US4389348A (en) * 1981-10-26 1983-06-21 Allied Corporation Selective hydrogenation of dinitrile to omega-aminonitrile and supported rhodium-containing catalyst therefor
DE3300341A1 (de) * 1983-01-07 1984-07-12 Chemische Werke Hüls AG, 4370 Marl Aliphatische ether des cyclododecen-2-ols, verfahren zu ihrer herstellung sowie ihre verwendung zur herstellung von riechstoffkompositionen
US4601859A (en) * 1984-05-04 1986-07-22 Allied Corporation Selective hydrogenation of aliphatic dinitriles to omega-aminonitriles in ammonia with supported, finely dispersed rhodium-containing catalyst
US4803304A (en) * 1987-04-15 1989-02-07 E. I. Du Pont De Nemours And Company Recovery of bis(hexamethylene)triamine
US5133838A (en) * 1991-02-28 1992-07-28 E. I. Du Pont De Nemours And Company Purification of 6-aminocapronitrile
US5151543A (en) * 1991-05-31 1992-09-29 E. I. Du Pont De Nemours And Company Selective low pressure hydrogenation of a dinitrile to an aminonitrile
JPH06501033A (ja) * 1991-07-12 1994-01-27 ギスト　ブロカデス　ナムローゼ　フェンノートシャップ 血清アルブミンの精製方法
DE4235466A1 (de) * 1992-10-21 1994-04-28 Bayer Ag Verfahren zur Herstellung von (cyclo)aliphatischen Aminonitrilen
DE4446893A1 (de) * 1994-12-27 1996-07-04 Basf Ag Verfahren zur Herstellung von aliphatischen alpha,omega-Aminonitrilen
DE19500222A1 (de) * 1995-01-05 1996-07-11 Basf Ag Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin
DE19548289A1 (de) * 1995-12-22 1997-06-26 Basf Ag Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin
US5961788A (en) * 1998-10-09 1999-10-05 E. I. Du Pont De Nemours And Company Sequential distillation process for removing tetrahydroazepine from aminocapronitrile and/or hexamethylenediamine

Also Published As

Publication number Publication date
CA2280889A1 (en) 1998-08-13
EP0961767B1 (de) 2002-04-10
MY127867A (en) 2006-12-29
CN1251568A (zh) 2000-04-26
EP0961767A1 (de) 1999-12-08
WO1998034903A1 (de) 1998-08-13
CA2280889C (en) 2005-07-19
ID23371A (id) 2000-04-20
DE19704612A1 (de) 1998-08-13
KR100527321B1 (ko) 2005-11-09
BR9807196B1 (pt) 2009-01-13
AR011635A1 (es) 2000-08-30
TW512139B (en) 2002-12-01
KR20000070891A (ko) 2000-11-25
JP2001511166A (ja) 2001-08-07
DE59803738D1 (de) 2002-05-16
BR9807166A (pt) 2000-01-25
BR9807196A (pt) 2000-05-23
CN1227216C (zh) 2005-11-16
US6139693A (en) 2000-10-31
AU6618098A (en) 1998-08-26

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